CN102574994B - 生产聚酯醇的方法 - Google Patents

生产聚酯醇的方法 Download PDF

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Publication number
CN102574994B
CN102574994B CN201080036725.6A CN201080036725A CN102574994B CN 102574994 B CN102574994 B CN 102574994B CN 201080036725 A CN201080036725 A CN 201080036725A CN 102574994 B CN102574994 B CN 102574994B
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CN
China
Prior art keywords
zeolite
titanium
reaction
polyesterols
carried out
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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CN201080036725.6A
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English (en)
Chinese (zh)
Other versions
CN102574994A (zh
Inventor
L·格林格
V·弗洛卡
U·穆勒
M·布杜
U·马恩
E·古特里奇-豪克
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BASF SE
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BASF SE
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Publication of CN102574994A publication Critical patent/CN102574994A/zh
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Publication of CN102574994B publication Critical patent/CN102574994B/zh
Expired - Fee Related legal-status Critical Current
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78—Preparation processes
    • C08G63/82—Preparation processes characterised by the catalyst used
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/42—Polycondensates having carboxylic or carbonic ester groups in the main chain
    • C08G18/4236—Polycondensates having carboxylic or carbonic ester groups in the main chain containing only aliphatic groups
    • C08G18/4238—Polycondensates having carboxylic or carbonic ester groups in the main chain containing only aliphatic groups derived from dicarboxylic acids and dialcohols
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/16—Catalysts
    • C08G18/22—Catalysts containing metal compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
    • C08G63/06—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from hydroxycarboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
    • C08G63/12—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78—Preparation processes
    • C08G63/82—Preparation processes characterised by the catalyst used
    • C08G63/823—Preparation processes characterised by the catalyst used for the preparation of polylactones or polylactides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78—Preparation processes
    • C08G63/82—Preparation processes characterised by the catalyst used
    • C08G63/85—Germanium, tin, lead, arsenic, antimony, bismuth, titanium, zirconium, hafnium, vanadium, niobium, tantalum, or compounds thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78—Preparation processes
    • C08G63/82—Preparation processes characterised by the catalyst used
    • C08G63/87—Non-metals or inter-compounds thereof

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Polyesters Or Polycarbonates (AREA)
CN201080036725.6A 2009-08-20 2010-08-16 生产聚酯醇的方法 Expired - Fee Related CN102574994B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP09168315.1 2009-08-20
EP09168315 2009-08-20
PCT/EP2010/061895 WO2011020815A1 (de) 2009-08-20 2010-08-16 Verfahren zur herstellung von polyesteralkoholen

Publications (2)

Publication Number Publication Date
CN102574994A CN102574994A (zh) 2012-07-11
CN102574994B true CN102574994B (zh) 2014-12-24

Family

ID=42711161

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201080036725.6A Expired - Fee Related CN102574994B (zh) 2009-08-20 2010-08-16 生产聚酯醇的方法

Country Status (8)

Country Link
US (2) US20120149862A1 (enExample)
EP (1) EP2467414B1 (enExample)
JP (1) JP5680084B2 (enExample)
KR (1) KR20120058559A (enExample)
CN (1) CN102574994B (enExample)
ES (1) ES2465073T3 (enExample)
PT (1) PT2467414E (enExample)
WO (1) WO2011020815A1 (enExample)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2017085158A1 (en) 2015-11-18 2017-05-26 Basf Se Polyester polyols with enhanced solubility
CN106064822B (zh) * 2016-05-30 2018-03-23 中国科学院大连化学物理研究所 一种mww/mel共结晶分子筛及其合成方法
JP7171691B2 (ja) * 2017-07-05 2022-11-15 ビーエーエスエフ ソシエタス・ヨーロピア ポリエステロール合成のための触媒
KR20220032056A (ko) 2019-06-18 2022-03-15 킨트라 파이버스 인코포레이티드 폴리에스테르 중합체 나노복합체
IL303916B2 (en) * 2020-12-23 2025-08-01 Kintra Fibers Inc Polyester polymer nanocomposites

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008037400A1 (en) * 2006-09-29 2008-04-03 Dow Global Technologies Inc. Process for the preparation of polyester polyols

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DE1003714B (de) 1956-01-25 1957-03-07 Glanzstoff Ag Verfahren zum Abbau von Polyaethylenterephthalat zu Terephthalsaeuredimethylester
DE2904184A1 (de) 1978-03-17 1979-09-20 Gaf Corp Formmasse und die daraus hergestellten spritzguss-formkoerper
IT1222868B (it) 1987-10-12 1990-09-12 Montedipe Spa Metodo per la preparazione di titanio silicaliti
US5244650A (en) 1989-06-29 1993-09-14 Engelhard Corporation Large-pored molecular sieves with charged octahedral titanium and charged tetrahedral aluminum sites
US5051528A (en) 1990-04-24 1991-09-24 Eastman Kodak Company Recovery process for ethylene glycol and dimethylterephthalate
US5187216A (en) * 1991-04-18 1993-02-16 Eastman Kodak Company Process for the preparation of crystalline copolyesters
JPH0543674A (ja) * 1991-08-09 1993-02-23 Kuraray Co Ltd ポリエーテルエステルポリオールの製造法
US5143984A (en) * 1992-01-21 1992-09-01 Eastman Kodak Company Process to prepare high molecule weight polyester
JP3231094B2 (ja) * 1992-10-09 2001-11-19 ハリマ化成株式会社 親水性ポリエステルジオールおよびその製造方法
US5502240A (en) * 1995-06-09 1996-03-26 Aristech Chemical Corporation Esterification process using a titamium zeolite catalyst
DE19638549A1 (de) * 1996-09-20 1998-03-26 Zimmer Ag Zeolith-Katalysator zur Polykondensation von Polyester
US5952455A (en) * 1996-10-11 1999-09-14 Kyowa Hakko Kogyo Co., Ltd. Process for producing polyhydroxycarboxylic acid
DE19717320A1 (de) * 1997-04-24 1998-10-29 Basf Ag Einstufiges Verfahren zur Herstellung von Glykolmonoethern aus Olefinen
JP2001172379A (ja) * 1999-12-17 2001-06-26 Toray Ind Inc ゼオライトを用いたポリエステルの製造装置及びその製造方法
JP2001200035A (ja) * 2000-01-20 2001-07-24 Kyowa Yuka Kk ポリエステルポリオール
JP2002013025A (ja) * 2000-06-28 2002-01-18 Toray Ind Inc ポリエステル繊維の製造方法
WO2004050741A1 (en) * 2002-12-03 2004-06-17 Dow Global Technologies Inc. Sulfonate-functional polyester polyols
WO2005042587A1 (ja) 2003-10-31 2005-05-12 Kowa Co., Ltd. セルロースiiリン酸エステル及びそれを用いた金属吸着材
DE102005014032A1 (de) 2005-03-23 2006-09-28 Basf Ag Zwei-stufiges Verfahren zur Herstellung von Polyesterolen
DE102008004343A1 (de) 2007-01-19 2008-07-24 Basf Se Verfahren zur Herstellung von Polyesteralkoholen
JP5577013B2 (ja) * 2007-06-06 2014-08-20 三井化学株式会社 無溶剤型ラミネート接着剤および複合フィルムの製造方法
WO2010035579A1 (ja) * 2008-09-25 2010-04-01 Dic株式会社 ポリウレタン樹脂組成物及びその成形品
DE102009005712A1 (de) * 2009-01-22 2010-07-29 Bayer Materialscience Ag Polyurethanvergussmassen

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008037400A1 (en) * 2006-09-29 2008-04-03 Dow Global Technologies Inc. Process for the preparation of polyester polyols

Also Published As

Publication number Publication date
EP2467414A1 (de) 2012-06-27
EP2467414B1 (de) 2014-04-16
US20150011792A1 (en) 2015-01-08
JP5680084B2 (ja) 2015-03-04
JP2013502475A (ja) 2013-01-24
PT2467414E (pt) 2014-06-09
WO2011020815A1 (de) 2011-02-24
ES2465073T3 (es) 2014-06-05
CN102574994A (zh) 2012-07-11
US20120149862A1 (en) 2012-06-14
US9133093B2 (en) 2015-09-15
KR20120058559A (ko) 2012-06-07

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C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20141224

Termination date: 20160816