CN102568855A - 碳材料负载二氧化锰纳米线阵列复合材料及其制备方法 - Google Patents
碳材料负载二氧化锰纳米线阵列复合材料及其制备方法 Download PDFInfo
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- CN102568855A CN102568855A CN2012100629457A CN201210062945A CN102568855A CN 102568855 A CN102568855 A CN 102568855A CN 2012100629457 A CN2012100629457 A CN 2012100629457A CN 201210062945 A CN201210062945 A CN 201210062945A CN 102568855 A CN102568855 A CN 102568855A
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- NUJOXMJBOLGQSY-UHFFFAOYSA-N manganese dioxide Chemical compound O=[Mn]=O NUJOXMJBOLGQSY-UHFFFAOYSA-N 0.000 title claims abstract description 128
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 81
- 229910052799 carbon Inorganic materials 0.000 title claims abstract description 60
- 239000002131 composite material Substances 0.000 title claims abstract description 36
- 239000002070 nanowire Substances 0.000 title abstract description 8
- 238000004519 manufacturing process Methods 0.000 title abstract description 7
- 239000000463 material Substances 0.000 claims abstract description 65
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims abstract description 37
- 238000005406 washing Methods 0.000 claims abstract description 32
- 239000003575 carbonaceous material Substances 0.000 claims abstract description 26
- 239000012286 potassium permanganate Substances 0.000 claims abstract description 21
- 238000006479 redox reaction Methods 0.000 claims abstract description 20
- 238000003756 stirring Methods 0.000 claims abstract description 16
- 238000001035 drying Methods 0.000 claims abstract description 15
- 239000007788 liquid Substances 0.000 claims abstract description 14
- 238000000034 method Methods 0.000 claims abstract description 12
- 238000000926 separation method Methods 0.000 claims abstract description 9
- 239000002994 raw material Substances 0.000 claims abstract description 5
- 239000007787 solid Substances 0.000 claims description 42
- 239000008367 deionised water Substances 0.000 claims description 28
- 229910021641 deionized water Inorganic materials 0.000 claims description 28
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 28
- 239000011259 mixed solution Substances 0.000 claims description 22
- 238000002360 preparation method Methods 0.000 claims description 21
- 229910021389 graphene Inorganic materials 0.000 claims description 14
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 12
- 239000000243 solution Substances 0.000 claims description 12
- 238000004140 cleaning Methods 0.000 claims description 9
- 238000000967 suction filtration Methods 0.000 claims description 9
- 229910002804 graphite Inorganic materials 0.000 claims description 7
- 239000010439 graphite Substances 0.000 claims description 7
- 229920000049 Carbon (fiber) Polymers 0.000 claims description 6
- 239000004917 carbon fiber Substances 0.000 claims description 6
- 239000002134 carbon nanofiber Substances 0.000 claims description 6
- 239000012295 chemical reaction liquid Substances 0.000 claims description 6
- LLYXJBROWQDVMI-UHFFFAOYSA-N 2-chloro-4-nitrotoluene Chemical compound CC1=CC=C([N+]([O-])=O)C=C1Cl LLYXJBROWQDVMI-UHFFFAOYSA-N 0.000 claims description 4
- 239000004567 concrete Substances 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 238000007599 discharging Methods 0.000 abstract description 5
- 239000002114 nanocomposite Substances 0.000 abstract description 5
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 abstract description 3
- 239000003054 catalyst Substances 0.000 abstract description 3
- 229910001416 lithium ion Inorganic materials 0.000 abstract description 3
- 238000005516 engineering process Methods 0.000 abstract description 2
- 238000002156 mixing Methods 0.000 abstract description 2
- 239000000969 carrier Substances 0.000 abstract 1
- 238000009792 diffusion process Methods 0.000 abstract 1
- 239000011149 active material Substances 0.000 description 6
- 238000011065 in-situ storage Methods 0.000 description 4
- 239000000126 substance Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 230000005518 electrochemistry Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 239000002243 precursor Substances 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 238000005054 agglomeration Methods 0.000 description 1
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- 230000008021 deposition Effects 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000002389 environmental scanning electron microscopy Methods 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000002105 nanoparticle Substances 0.000 description 1
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/13—Energy storage using capacitors
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- Carbon And Carbon Compounds (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
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Cited By (17)
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---|---|---|---|---|
CN104599857A (zh) * | 2015-01-22 | 2015-05-06 | 武汉理工大学 | 多孔石墨烯/MnO2管中线结构同轴纳米线及其制备方法和应用 |
CN104993143A (zh) * | 2015-05-25 | 2015-10-21 | 西北工业大学 | 一种自支撑锂离子电池负极材料的制备方法 |
CN105289581A (zh) * | 2015-10-16 | 2016-02-03 | 上海纳米技术及应用国家工程研究中心有限公司 | 一种硫酸处理的碳纳米管担载氧化锰基催化剂及制备 |
CN105289583A (zh) * | 2015-10-30 | 2016-02-03 | 上海纳米技术及应用国家工程研究中心有限公司 | 一种碳纳米球担载氧化锰基催化剂的制备方法 |
CN105435740A (zh) * | 2015-11-18 | 2016-03-30 | 福建翔丰华新能源材料有限公司 | 一种负载二氧化锰的活性炭甲醛吸附剂的制备方法 |
CN105609319A (zh) * | 2016-01-29 | 2016-05-25 | 西北师范大学 | 用于超级电容器电极材料的片状碳化钛负载二氧化锰复合材料及其制备 |
CN105858828A (zh) * | 2016-06-03 | 2016-08-17 | 华东师范大学 | 一种不对称流动式电极的脱盐装置 |
CN106925034A (zh) * | 2017-04-27 | 2017-07-07 | 福州大学 | 一种脱硝功能聚苯硫醚复合滤料的制备方法 |
CN108144425A (zh) * | 2018-03-03 | 2018-06-12 | 深圳市太鸟科技有限公司 | 一种三维石墨烯碳基复合脱硫材料及其制备方法 |
CN108400018A (zh) * | 2018-01-10 | 2018-08-14 | 青岛大学 | 一种浒苔活性炭复合二氧化锰超级电容器电极材料的制备方法 |
CN109346717A (zh) * | 2018-09-11 | 2019-02-15 | 三峡大学 | 一种自支撑NaxMnO2阵列钠离子电池正极材料及其制备方法 |
CN109647538A (zh) * | 2018-12-11 | 2019-04-19 | 天津工业大学 | 一种二氧化锰负载型催化剂的制备方法 |
CN110176363A (zh) * | 2019-05-14 | 2019-08-27 | 扬州大学 | 多孔碳负载二氧化锰纳米材料的制备方法 |
US10580591B2 (en) | 2013-11-05 | 2020-03-03 | The Regents Of California, Riverside | Metal-oxide anchored graphene and carbon-nanotube hybrid foam |
CN111744470A (zh) * | 2020-07-08 | 2020-10-09 | 武汉理工大学 | 一种原位负载阵列式活性成分的碳纤维基脱硝催化剂及其制备方法 |
CN112375545A (zh) * | 2020-11-16 | 2021-02-19 | 桂林电子科技大学 | 一种二氧化锰-三聚氰胺甲醛树脂双壳层复合相变材料及其制备方法 |
CN114805882A (zh) * | 2021-05-28 | 2022-07-29 | 惠州市纵胜电子材料有限公司 | 一种高强度抗静电3d片材及其制备方法 |
Citations (4)
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CN1935355A (zh) * | 2006-09-07 | 2007-03-28 | 山东大学 | 二氧化锰/碳纳米管复合吸附剂及其制备方法 |
CN101281821A (zh) * | 2008-05-20 | 2008-10-08 | 中山大学 | 纳米丝状二氧化锰负载炭气凝胶及其制备方法与应用 |
CN101923960A (zh) * | 2010-08-18 | 2010-12-22 | 东华大学 | 一种瓣状二氧化锰纳米晶包覆碳纳米管复合电极材料的制备方法 |
CN102354611A (zh) * | 2011-08-31 | 2012-02-15 | 燕山大学 | 一种石墨烯/二氧化锰纳米复合材料及制备方法 |
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2012
- 2012-03-12 CN CN201210062945.7A patent/CN102568855B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1935355A (zh) * | 2006-09-07 | 2007-03-28 | 山东大学 | 二氧化锰/碳纳米管复合吸附剂及其制备方法 |
CN101281821A (zh) * | 2008-05-20 | 2008-10-08 | 中山大学 | 纳米丝状二氧化锰负载炭气凝胶及其制备方法与应用 |
CN101923960A (zh) * | 2010-08-18 | 2010-12-22 | 东华大学 | 一种瓣状二氧化锰纳米晶包覆碳纳米管复合电极材料的制备方法 |
CN102354611A (zh) * | 2011-08-31 | 2012-02-15 | 燕山大学 | 一种石墨烯/二氧化锰纳米复合材料及制备方法 |
Cited By (24)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US10580591B2 (en) | 2013-11-05 | 2020-03-03 | The Regents Of California, Riverside | Metal-oxide anchored graphene and carbon-nanotube hybrid foam |
CN104599857A (zh) * | 2015-01-22 | 2015-05-06 | 武汉理工大学 | 多孔石墨烯/MnO2管中线结构同轴纳米线及其制备方法和应用 |
CN104599857B (zh) * | 2015-01-22 | 2017-07-11 | 武汉理工大学 | 多孔石墨烯/MnO2管中线结构同轴纳米线及其制备方法和应用 |
CN104993143A (zh) * | 2015-05-25 | 2015-10-21 | 西北工业大学 | 一种自支撑锂离子电池负极材料的制备方法 |
CN105289581A (zh) * | 2015-10-16 | 2016-02-03 | 上海纳米技术及应用国家工程研究中心有限公司 | 一种硫酸处理的碳纳米管担载氧化锰基催化剂及制备 |
CN105289583A (zh) * | 2015-10-30 | 2016-02-03 | 上海纳米技术及应用国家工程研究中心有限公司 | 一种碳纳米球担载氧化锰基催化剂的制备方法 |
CN105435740A (zh) * | 2015-11-18 | 2016-03-30 | 福建翔丰华新能源材料有限公司 | 一种负载二氧化锰的活性炭甲醛吸附剂的制备方法 |
CN105609319B (zh) * | 2016-01-29 | 2019-01-22 | 西北师范大学 | 用于超级电容器电极材料的片状碳化钛负载二氧化锰复合材料及其制备 |
CN105609319A (zh) * | 2016-01-29 | 2016-05-25 | 西北师范大学 | 用于超级电容器电极材料的片状碳化钛负载二氧化锰复合材料及其制备 |
CN105858828A (zh) * | 2016-06-03 | 2016-08-17 | 华东师范大学 | 一种不对称流动式电极的脱盐装置 |
CN106925034A (zh) * | 2017-04-27 | 2017-07-07 | 福州大学 | 一种脱硝功能聚苯硫醚复合滤料的制备方法 |
CN106925034B (zh) * | 2017-04-27 | 2018-12-25 | 福州大学 | 一种脱硝功能聚苯硫醚复合滤料的制备方法 |
CN108400018A (zh) * | 2018-01-10 | 2018-08-14 | 青岛大学 | 一种浒苔活性炭复合二氧化锰超级电容器电极材料的制备方法 |
CN108144425A (zh) * | 2018-03-03 | 2018-06-12 | 深圳市太鸟科技有限公司 | 一种三维石墨烯碳基复合脱硫材料及其制备方法 |
CN108144425B (zh) * | 2018-03-03 | 2021-02-09 | 深圳市太鸟科技有限公司 | 一种三维石墨烯碳基复合脱硫材料及其制备方法 |
CN109346717A (zh) * | 2018-09-11 | 2019-02-15 | 三峡大学 | 一种自支撑NaxMnO2阵列钠离子电池正极材料及其制备方法 |
CN109346717B (zh) * | 2018-09-11 | 2021-06-18 | 三峡大学 | 一种自支撑NaxMnO2阵列钠离子电池正极材料及其制备方法 |
CN109647538A (zh) * | 2018-12-11 | 2019-04-19 | 天津工业大学 | 一种二氧化锰负载型催化剂的制备方法 |
CN110176363A (zh) * | 2019-05-14 | 2019-08-27 | 扬州大学 | 多孔碳负载二氧化锰纳米材料的制备方法 |
CN111744470A (zh) * | 2020-07-08 | 2020-10-09 | 武汉理工大学 | 一种原位负载阵列式活性成分的碳纤维基脱硝催化剂及其制备方法 |
CN111744470B (zh) * | 2020-07-08 | 2023-09-19 | 武汉理工大学 | 一种原位负载阵列式活性成分的碳纤维基脱硝催化剂及其制备方法 |
CN112375545A (zh) * | 2020-11-16 | 2021-02-19 | 桂林电子科技大学 | 一种二氧化锰-三聚氰胺甲醛树脂双壳层复合相变材料及其制备方法 |
CN112375545B (zh) * | 2020-11-16 | 2021-07-02 | 桂林电子科技大学 | 一种二氧化锰-三聚氰胺甲醛树脂双壳层复合相变材料及其制备方法 |
CN114805882A (zh) * | 2021-05-28 | 2022-07-29 | 惠州市纵胜电子材料有限公司 | 一种高强度抗静电3d片材及其制备方法 |
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Effective date of registration: 20240115 Address after: 516199 Luo Yang Zhen Ji Ma Di Cun Mai Dong, Boluo County, Huizhou City, Guangdong Province Patentee after: HUIZHOU JINLONGYU CABLE INDUSTRIAL DEVELOPMENT CO.,LTD. Address before: 401329 Building 1, No. 21, Fengsheng Road, Jinfeng Town, high tech Zone, Jiulongpo District, Chongqing Patentee before: Chongqing jintianyi New Energy Technology Co.,Ltd. Patentee before: HUIZHOU JINLONGYU CABLE INDUSTRIAL DEVELOPMENT CO.,LTD. |
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Effective date of registration: 20240816 Address after: Room 1101, Office Building 2, Jinlongyu Industrial Park, No. 288 Jihua Road, Shuijing Community, Jihua Street, Longgang District, Shenzhen City, Guangdong Province 518000 Patentee after: Jinlongyu New Energy (Shenzhen) Co.,Ltd. Country or region after: China Address before: 516199 Luo Yang Zhen Ji Ma Di Cun Mai Dong, Boluo County, Huizhou City, Guangdong Province Patentee before: HUIZHOU JINLONGYU CABLE INDUSTRIAL DEVELOPMENT CO.,LTD. Country or region before: China |
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