CN102264776B - 使用原位制备的氟化离聚物的分散颗粒通过含水聚合制备氟化离聚物 - Google Patents

使用原位制备的氟化离聚物的分散颗粒通过含水聚合制备氟化离聚物 Download PDF

Info

Publication number
CN102264776B
CN102264776B CN200980152389.9A CN200980152389A CN102264776B CN 102264776 B CN102264776 B CN 102264776B CN 200980152389 A CN200980152389 A CN 200980152389A CN 102264776 B CN102264776 B CN 102264776B
Authority
CN
China
Prior art keywords
fluorinated
fluorinated ionomer
polymerization
particles
ionomer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN200980152389.9A
Other languages
English (en)
Chinese (zh)
Other versions
CN102264776A (zh
Inventor
R·M·阿滕
K·W·莱夫尤
R·B·劳埃德
C·J·内尔克
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
EIDP Inc
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Publication of CN102264776A publication Critical patent/CN102264776A/zh
Application granted granted Critical
Publication of CN102264776B publication Critical patent/CN102264776B/zh
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F214/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
    • C08F214/18—Monomers containing fluorine
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F14/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
    • C08F14/18—Monomers containing fluorine

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Polymerisation Methods In General (AREA)
CN200980152389.9A 2008-12-23 2009-12-23 使用原位制备的氟化离聚物的分散颗粒通过含水聚合制备氟化离聚物 Expired - Fee Related CN102264776B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US14012208P 2008-12-23 2008-12-23
US61/140,122 2008-12-23
PCT/US2009/069377 WO2010075497A1 (en) 2008-12-23 2009-12-23 Fluorinated ionomer produced by aqueous polymerization using dispersed particulate of fluorinated ionomer produced in situ

Publications (2)

Publication Number Publication Date
CN102264776A CN102264776A (zh) 2011-11-30
CN102264776B true CN102264776B (zh) 2014-04-30

Family

ID=41611328

Family Applications (1)

Application Number Title Priority Date Filing Date
CN200980152389.9A Expired - Fee Related CN102264776B (zh) 2008-12-23 2009-12-23 使用原位制备的氟化离聚物的分散颗粒通过含水聚合制备氟化离聚物

Country Status (5)

Country Link
US (1) US8436054B2 (https=)
EP (1) EP2367860B1 (https=)
JP (1) JP5758810B2 (https=)
CN (1) CN102264776B (https=)
WO (1) WO2010075497A1 (https=)

Families Citing this family (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014084399A1 (ja) 2012-11-30 2014-06-05 ダイキン工業株式会社 ポリテトラフルオロエチレン水性分散液及びポリテトラフルオロエチレンファインパウダー
CN111040058B (zh) 2012-11-30 2022-10-25 大金工业株式会社 聚四氟乙烯水性分散液的制造方法
EP2927248B1 (en) * 2012-11-30 2018-06-13 Daikin Industries, Ltd. Production method for polytetrafluoroethylene aqueous dispersion
JP6225683B2 (ja) * 2013-05-17 2017-11-08 ダイキン工業株式会社 フルオロポリマー水性分散液の製造方法
US10717861B2 (en) * 2015-04-28 2020-07-21 Dankook University Cheonan Campus Industry Academic Cooperation Foundation Perfluorinated ionomer nanoparticle dispersion solution, and preparation method therefor
EP3760649B1 (en) 2018-03-01 2024-01-24 Daikin Industries, Ltd. Method for manufacturing fluoropolymer
JPWO2019181435A1 (ja) 2018-03-22 2021-03-18 富士フイルム株式会社 ろ過装置、精製装置、薬液の製造方法
WO2020105651A1 (ja) 2018-11-19 2020-05-28 ダイキン工業株式会社 変性ポリテトラフルオロエチレンの製造方法及び組成物
TWI821458B (zh) 2018-11-19 2023-11-11 日商大金工業股份有限公司 組成物及拉伸體
JP7417129B2 (ja) 2019-04-26 2024-01-18 ダイキン工業株式会社 水の処理方法および組成物
JP7389366B2 (ja) 2019-04-26 2023-11-30 ダイキン工業株式会社 フルオロポリマー水性分散液の製造方法、排水の処理方法、及び、フルオロポリマー水性分散液
JP7231868B2 (ja) 2019-09-05 2023-03-02 ダイキン工業株式会社 組成物およびその製造方法
WO2021045165A1 (ja) 2019-09-05 2021-03-11 ダイキン工業株式会社 パーフルオロエラストマーの製造方法および組成物
WO2021100836A1 (ja) 2019-11-19 2021-05-27 ダイキン工業株式会社 フルオロポリマーの製造方法、ポリテトラフルオロエチレンの製造方法、パーフルオロエラストマーの製造方法および組成物
WO2022107894A1 (ja) 2020-11-19 2022-05-27 ダイキン工業株式会社 ポリテトラフルオロエチレンの製造方法およびポリテトラフルオロエチレンを含有する組成物
EP4249517A4 (en) 2020-11-19 2024-10-16 Daikin Industries, Ltd. PROCESS FOR PRODUCING AN AQUEOUS DISPERSION OF FLUORINE-CONTAINING ELASTOMER, AND COMPOSITION
JP7549257B2 (ja) 2020-11-19 2024-09-11 ダイキン工業株式会社 パーフルオロエラストマー水性分散液の製造方法、組成物、架橋性組成物および架橋物
KR20230150868A (ko) 2021-03-10 2023-10-31 다이킨 고교 가부시키가이샤 도료 조성물, 도포막, 적층체 및 도장 물품
JPWO2022244784A1 (https=) 2021-05-19 2022-11-24
JP7741413B2 (ja) 2021-06-11 2025-09-18 ダイキン工業株式会社 含フッ素エラストマー水性分散液の製造方法、組成物および水性分散液
WO2023277139A1 (ja) 2021-06-30 2023-01-05 ダイキン工業株式会社 フルオロポリマー組成物の製造方法およびフルオロポリマー組成物
WO2023277140A1 (ja) 2021-06-30 2023-01-05 ダイキン工業株式会社 高純度フルオロポリマー含有組成物の製造方法および高純度フルオロポリマー含有組成物
EP4497762A4 (en) 2022-03-23 2026-03-18 Daikin Ind Ltd PROCESS FOR PRODUCING FLUORIDED POLYMER, AND COMPOSITION
CN119095910A (zh) 2022-04-28 2024-12-06 大金工业株式会社 含有氟橡胶的组合物
JP7787462B2 (ja) 2022-04-28 2025-12-17 ダイキン工業株式会社 フルオロポリマーの製造方法
CN119072500A (zh) 2022-04-28 2024-12-03 大金工业株式会社 含有氟树脂的组合物的制造方法和含有氟树脂的组合物
WO2024154773A1 (ja) 2023-01-18 2024-07-25 ダイキン工業株式会社 テトラフルオロエチレン系ポリマー組成物、電気化学デバイス用バインダー、電極合剤、電極、及び、二次電池
EP4456182A4 (en) 2023-01-18 2025-09-03 Daikin Ind Ltd MIXTURE FOR ELECTROCHEMICAL DEVICE, MIXTURE SHEET FOR ELECTROCHEMICAL DEVICE, ELECTRODE AND ELECTROCHEMICAL DEVICE
JP7820661B2 (ja) 2023-08-14 2026-02-26 ダイキン工業株式会社 フルオロポリマー水性分散液の製造方法およびフルオロポリマー水性分散液
JP7689278B2 (ja) 2023-08-28 2025-06-06 ダイキン工業株式会社 水溶性含フッ素ポリマーの回収方法

Family Cites Families (71)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2559752A (en) 1951-03-06 1951-07-10 Du Pont Aqueous colloidal dispersions of polymers
US2713593A (en) 1953-12-21 1955-07-19 Minnesota Mining & Mfg Fluorocarbon acids and derivatives
US3037953A (en) 1961-04-26 1962-06-05 Du Pont Concentration of aqueous colloidal dispersions of polytetrafluoroethylene
US3271341A (en) 1961-08-07 1966-09-06 Du Pont Aqueous colloidal dispersions of polymer
US3282875A (en) 1964-07-22 1966-11-01 Du Pont Fluorocarbon vinyl ether polymers
US3291843A (en) 1963-10-08 1966-12-13 Du Pont Fluorinated vinyl ethers and their preparation
US3391099A (en) 1966-04-25 1968-07-02 Du Pont Polymerization process
GB1292268A (en) 1970-02-16 1972-10-11 Bitterfeld Chemie Process for the dimerisation of hexafluoropropene epoxide
US3704272A (en) 1970-09-15 1972-11-28 Du Pont Concentration of polytetrafluoroethylene aqueous dispersion
US4358545A (en) 1980-06-11 1982-11-09 The Dow Chemical Company Sulfonic acid electrolytic cell having flourinated polymer membrane with hydration product less than 22,000
JPS5816622U (ja) 1981-07-23 1983-02-01 株式会社リコー カメラシステムにおける信号伝達装置
US4380618A (en) 1981-08-21 1983-04-19 E. I. Du Pont De Nemours And Company Batch polymerization process
US4552631A (en) 1983-03-10 1985-11-12 E. I. Du Pont De Nemours And Company Reinforced membrane, electrochemical cell and electrolysis process
DE3486428T2 (de) 1983-12-26 1996-10-10 Daikin Ind Ltd Halogen enthaltendes Polyether
US4621116A (en) 1984-12-07 1986-11-04 E. I. Du Pont De Nemours And Company Process for copolymerization of tetrafluoroethylene in the presence of a dispersing agent comprising a perfluoroalkoxybenzene sulfonic acid or salt
US4743658A (en) 1985-10-21 1988-05-10 E. I. Du Pont De Nemours And Company Stable tetrafluoroethylene copolymers
US4940525A (en) 1987-05-08 1990-07-10 The Dow Chemical Company Low equivalent weight sulfonic fluoropolymers
US4952630A (en) 1987-12-31 1990-08-28 E. I. Du Pont De Nemours And Company Modified polytetrafluoroethylene resins and blends thereof
JP3172983B2 (ja) 1993-09-20 2001-06-04 ダイキン工業株式会社 ビニリデンフルオライド系重合体の水性分散液およびその製法
US5422411A (en) 1993-09-21 1995-06-06 Ballard Power Systems Inc. Trifluorostyrene and substituted trifluorostyrene copolymeric compositions and ion-exchange membranes formed therefrom
US5637748A (en) 1995-03-01 1997-06-10 E. I. Du Pont De Nemours And Company Process for synthesizing fluorinated nitrile compounds
JP3346090B2 (ja) 1995-03-31 2002-11-18 ダイキン工業株式会社 ポリテトラフルオロエチレン水性分散液組成物及びその用途
US5688884A (en) 1995-08-31 1997-11-18 E. I. Du Pont De Nemours And Company Polymerization process
US5789508A (en) 1995-08-31 1998-08-04 E. I. Du Pont De Nemours And Company Polymerization process
US5763552A (en) 1996-07-26 1998-06-09 E. I. Du Pont De Nemours And Company Hydrogen-containing flourosurfacant and its use in polymerization
US5866711A (en) 1996-09-13 1999-02-02 E. I. Du Pont De Nemours And Company Fluorocyanate and fluorocarbamate monomers and polymers thereof
US5969067A (en) 1996-09-13 1999-10-19 E.I. Dupont De Nemours And Company Phosphorus-containing fluoromonomers and polymers thereof
CN1233267A (zh) 1996-10-15 1999-10-27 纳幕尔杜邦公司 含有高度氟化的离子交换聚合物颗粒的组合物
CN1154633C (zh) 1997-03-31 2004-06-23 大金工业株式会社 卤代乙烯醚类磺酸衍生物的制法
JP4150867B2 (ja) * 1998-05-13 2008-09-17 ダイキン工業株式会社 燃料電池に使用するのに適した固体高分子電解質用材料
US6395848B1 (en) 1999-05-20 2002-05-28 E. I. Du Pont De Nemours And Company Polymerization of fluoromonomers
US6482979B1 (en) 1999-12-22 2002-11-19 Dyneon Llc Perfluorinated acid fluorides and preparation thereof
JP4779184B2 (ja) * 2000-02-16 2011-09-28 ダイキン工業株式会社 フッ素系アイオノマー共重合体の製造法
JP4759782B2 (ja) * 2000-02-16 2011-08-31 ダイキン工業株式会社 フッ素系アイオノマーの精製・濃縮方法
EP1283225B1 (en) 2000-02-16 2006-05-03 Daikin Industries, Ltd. Process for producing fluoroionomer, method for purification and concentration of the ionomer, and method of film formation
US6737489B2 (en) 2001-05-21 2004-05-18 3M Innovative Properties Company Polymers containing perfluorovinyl ethers and applications for such polymers
US7045571B2 (en) 2001-05-21 2006-05-16 3M Innovative Properties Company Emulsion polymerization of fluorinated monomers
US7094851B2 (en) * 2001-12-06 2006-08-22 Gore Enterprise Holdings, Inc. Low equivalent weight ionomer
BR0215428A (pt) 2002-01-04 2004-12-14 Du Pont Dispersão aquosa, composição de revestimento da dispersão aquosa, substratos revestidos e filme auto-sustentado
US6833418B2 (en) 2002-04-05 2004-12-21 3M Innovative Properties Company Dispersions containing perfluorovinyl ether homopolymers and use thereof
US6822059B2 (en) 2002-04-05 2004-11-23 3M Innovative Properties Company Dispersions containing bicomponent fluoropolymer particles and use thereof
US6902839B2 (en) 2002-05-31 2005-06-07 Korea Advanced Institute Of Science And Technology Polymer electrolyte membrane for fuel cell and method for producing the same
JP4096764B2 (ja) 2002-06-17 2008-06-04 ダイキン工業株式会社 含フッ素結晶性ポリマー分散体製造方法
DE10228103A1 (de) 2002-06-24 2004-01-15 Bayer Cropscience Ag Fungizide Wirkstoffkombinationen
US6841616B2 (en) 2003-03-28 2005-01-11 Arkema Inc. Polymerization of halogen-containing monomers using siloxane surfactant
JP2004358397A (ja) 2003-06-05 2004-12-24 Daikin Ind Ltd 界面活性剤、含フッ素重合体の製造方法及び含フッ素重合体水性分散液
JP2004359870A (ja) 2003-06-05 2004-12-24 Daikin Ind Ltd 界面活性剤、含フッ素重合体の製造方法及び含フッ素重合体水性分散液
US7589234B2 (en) 2003-07-02 2009-09-15 Daikin Industries, Ltd. Fluoroalkyl carboxylic acid derivative, method for producing fluorine-containing polymer, and aqueous dispersion of fluorine-containing polymer
US7557164B2 (en) 2003-08-19 2009-07-07 E. I. Du Pont De Nemours And Company Membranes of fluorinated ionomer blended with nonionomeric fluoropolymers for electrochemical cells
US20050090613A1 (en) 2003-10-22 2005-04-28 Daikin Industries, Ltd. Process for preparing fluorine-containing polymer latex
US7071271B2 (en) 2003-10-30 2006-07-04 3M Innovative Properties Company Aqueous emulsion polymerization of functionalized fluoromonomers
ATE529451T1 (de) 2003-11-17 2011-11-15 3M Innovative Properties Co Wässrige ptfe-dispersionen mit einem niedrigen gehalt an fluorierten emulgatoren
JP2005320501A (ja) 2004-04-07 2005-11-17 Daikin Ind Ltd 含フッ素エラストマー重合体の製造方法
RU2346996C2 (ru) 2004-06-29 2009-02-20 ЮРОПИЭН НИКЕЛЬ ПиЭлСи Усовершенствованное выщелачивание основных металлов
US20060014887A1 (en) 2004-07-19 2006-01-19 3M Innovative Properties Company Method of hydrolyzing a dispersion of ionic fluoropolymer
GB0511779D0 (en) * 2005-06-10 2005-07-20 3M Innovative Properties Co Aqueous emulsion polymerization of fluorinated monomers in the presence of a partially fluorinated oligomer as an emulsifier
US7930013B2 (en) 2005-06-29 2011-04-19 Compumedics Limited Sensor assembly with conductive bridge
GB0514387D0 (en) 2005-07-15 2005-08-17 3M Innovative Properties Co Aqueous emulsion polymerization of fluorinated monomers using a perfluoropolyether surfactant
GB0514398D0 (en) 2005-07-15 2005-08-17 3M Innovative Properties Co Aqueous emulsion polymerization of fluorinated monomers using a fluorinated surfactant
US7671112B2 (en) 2005-07-15 2010-03-02 3M Innovative Properties Company Method of making fluoropolymer dispersion
CN100558753C (zh) 2005-10-17 2009-11-11 旭硝子株式会社 聚四氟乙烯水性乳化液、由其制得的聚四氟乙烯细粉和多孔体
WO2007046377A1 (ja) 2005-10-20 2007-04-26 Asahi Glass Company, Limited 溶融成形可能なフッ素樹脂の製造方法
JP5141256B2 (ja) 2005-10-20 2013-02-13 旭硝子株式会社 ポリテトラフルオロエチレン水性分散液およびその製品
EP1942118B1 (en) 2005-10-26 2013-09-11 Asahi Glass Company, Limited Fluororesin with low fluorine-containing emulsifier residual and method for producing same
TW200801513A (en) 2006-06-29 2008-01-01 Fermiscan Australia Pty Ltd Improved process
WO2008001894A1 (fr) * 2006-06-30 2008-01-03 Daikin Industries, Ltd. Procédé de production de polymère contenant du fluor
EP2079766B1 (en) 2006-11-09 2011-05-18 E.I. Du Pont De Nemours And Company Aqueous polymerization of fluorinated monomer using polymerization agent comprising high molecular weight fluoropolyether acid or salt and fluoropolyether acid or salt surfactant
JP5439186B2 (ja) 2006-11-09 2014-03-12 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー フルオロポリエーテル酸または塩および炭化水素系界面活性剤を含む重合剤を用いるフッ素化モノマーの水性重合
US7989566B2 (en) 2008-01-22 2011-08-02 Dupont Performance Elastomers Llc Process for producing fluoropolymers
US8153738B2 (en) 2008-12-23 2012-04-10 E I Du Pont De Nemours And Company Fluoropolymer produced by aqueous polymerization using dispersed particulate of fluorinated ionomer
WO2010075495A1 (en) 2008-12-23 2010-07-01 E. I. Du Pont De Nemours And Company Fluorinated ionomer produced by aqueous polymerization using dispersed particulate of fluorinated ionomer

Also Published As

Publication number Publication date
WO2010075497A1 (en) 2010-07-01
EP2367860B1 (en) 2016-04-27
JP5758810B2 (ja) 2015-08-05
CN102264776A (zh) 2011-11-30
US8436054B2 (en) 2013-05-07
JP2012513535A (ja) 2012-06-14
US20100160465A1 (en) 2010-06-24
EP2367860A1 (en) 2011-09-28

Similar Documents

Publication Publication Date Title
CN102264776B (zh) 使用原位制备的氟化离聚物的分散颗粒通过含水聚合制备氟化离聚物
CN102264775B (zh) 使用原位制备的氟化离聚物的分散颗粒通过含水聚合制备含氟聚合物
EP3091039B1 (en) Fluoropolymer produced by aqueous polymerization using dispersed particulate of fluorinated ionomer
US8835547B2 (en) Fluoropolymer particles having a nucleus of fluorinated ionomer
CN102027023B (zh) 使用氟聚醚酸或盐的混合物的氟化单体含水聚合反应
US20120077931A1 (en) Aqueous polymerization of fluorinated monomer using polymerization agent comprising fluoropolyether acid or salt and short chain fluorosurfactant
CN102264774A (zh) 使用氟化离聚物的分散颗粒通过含水聚合制备的氟化离聚物
US8436053B2 (en) Fluorinated ionomer produced by aqueous polymerization using dispersed particulate of fluorinated ionomer

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20140430

Termination date: 20161223

CF01 Termination of patent right due to non-payment of annual fee