CN102256922B - 通过醇蒸气汽提制备羧酸酯 - Google Patents

通过醇蒸气汽提制备羧酸酯 Download PDF

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Publication number
CN102256922B
CN102256922B CN200980150480.7A CN200980150480A CN102256922B CN 102256922 B CN102256922 B CN 102256922B CN 200980150480 A CN200980150480 A CN 200980150480A CN 102256922 B CN102256922 B CN 102256922B
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CN
China
Prior art keywords
alcohol
acid
reactor
reaction mixture
vapor
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Expired - Fee Related
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CN200980150480.7A
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English (en)
Chinese (zh)
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CN102256922A (zh
Inventor
J·彼得斯
W·迪斯特多尔夫
K·弗里泽
T·沙福尔
O·贝
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BASF SE
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BASF SE
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D19/00—Degasification of liquids
    • B01D19/0005—Degasification of liquids with one or more auxiliary substances
    • B01D19/001—Degasification of liquids with one or more auxiliary substances by bubbling steam through the liquid
    • B01D19/0015—Degasification of liquids with one or more auxiliary substances by bubbling steam through the liquid in contact columns containing plates, grids or other filling elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/36—Azeotropic distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/38—Steam distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN200980150480.7A 2008-12-16 2009-12-15 通过醇蒸气汽提制备羧酸酯 Expired - Fee Related CN102256922B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP08171795 2008-12-16
EP08171795.1 2008-12-16
PCT/EP2009/067179 WO2010076194A1 (de) 2008-12-16 2009-12-15 Herstellung von carbonsäureestern unter strippen mit alkohol-dampf

Publications (2)

Publication Number Publication Date
CN102256922A CN102256922A (zh) 2011-11-23
CN102256922B true CN102256922B (zh) 2015-09-09

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN200980150480.7A Expired - Fee Related CN102256922B (zh) 2008-12-16 2009-12-15 通过醇蒸气汽提制备羧酸酯

Country Status (9)

Country Link
US (1) US8901344B2 (enExample)
EP (1) EP2379482B1 (enExample)
JP (1) JP5698146B2 (enExample)
KR (1) KR101733814B1 (enExample)
CN (1) CN102256922B (enExample)
CA (1) CA2746571C (enExample)
ES (1) ES2554170T3 (enExample)
MY (1) MY157837A (enExample)
WO (1) WO2010076194A1 (enExample)

Families Citing this family (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102001948B (zh) * 2010-10-18 2015-04-15 华侨大学 一种酯化合成对苯二甲酸二异辛酯的方法
CN102295564B (zh) * 2011-07-25 2013-07-10 浙江庆安化工有限公司 一种dop连续化生产工艺
CN103822937A (zh) * 2012-11-16 2014-05-28 哈尔滨飞机工业集团有限责任公司 三氯乙烯槽液沸点测试方法
CN103113231A (zh) * 2013-02-27 2013-05-22 寿光市鲁源盐化有限公司 二烯丙基二甘醇碳酸酯的合成方法
TWI466863B (zh) * 2013-03-21 2015-01-01 Chang Chun Plastics Co Ltd 對苯二甲酸二（２－乙基己酯）之製造方法
CN104418747B (zh) * 2013-08-22 2016-08-10 中国科学院大连化学物理研究所 一种制备邻苯二甲酸二（2-丙基庚）酯的方法
TWI686444B (zh) 2014-09-04 2020-03-01 德商巴斯夫歐洲公司 包含聚合二羧酸酯的塑化劑組成物
CN105111074B (zh) * 2015-07-20 2018-02-13 浙江大学 一种碱减量废水固体残渣甲酯化回收利用方法
CN105111075A (zh) * 2015-08-28 2015-12-02 华东理工大学 邻苯二甲酸酯类增塑剂连续生产新工艺
KR101663586B1 (ko) 2016-04-28 2016-10-10 애경유화주식회사 차별화 된 반응 온도 제어를 이용하여 반응 전환 속도를 높인 디옥틸테레프탈레이트의 제조방법
WO2019185409A1 (de) 2018-03-29 2019-10-03 Basf Se Pvc-zusammensetzung, enthaltend wenigstens einen weichmacher der wenigstens eine carbonsäureestergruppe aufweist und wenigstens eine carbodiimidverbindung
KR102506500B1 (ko) * 2018-11-29 2023-03-06 주식회사 엘지화학 디알킬 테레프탈레이트계 조성물의 제조방법
JP7342320B2 (ja) * 2019-04-04 2023-09-12 エルジー・ケム・リミテッド エステル系組成物の製造方法及び製造システム
US11512166B2 (en) 2019-04-04 2022-11-29 Lg Chem, Ltd. Method and system for manufacturing ester-based composition
KR102489172B1 (ko) * 2019-07-04 2023-01-18 주식회사 엘지화학 디에스터계 물질의 제조 유닛 및 이를 포함하는 디에스터계 물질의 제조 시스템
KR102489171B1 (ko) * 2019-07-04 2023-01-18 주식회사 엘지화학 디에스터계 물질의 제조 유닛 및 이를 포함하는 디에스터계 물질의 제조 시스템
KR102489173B1 (ko) * 2019-07-04 2023-01-18 주식회사 엘지화학 열교환 시스템 및 이를 포함하는 디에스터계 조성물 제조 시스템
KR102488351B1 (ko) * 2019-07-04 2023-01-13 주식회사 엘지화학 디에스터계 물질의 연속식 제조방법
KR102489174B1 (ko) * 2019-07-04 2023-01-18 주식회사 엘지화학 디에스터계 조성물의 제조 시스템 및 방법
CN112239405B (zh) * 2019-07-17 2023-05-02 中国石油化工股份有限公司 2,6-萘二甲酸二甲酯的合成方法
KR102501597B1 (ko) * 2019-09-25 2023-02-20 주식회사 엘지화학 디에스테르계 조성물의 제조 시스템 및 제조방법
KR102595882B1 (ko) * 2019-09-25 2023-10-30 주식회사 엘지화학 디에스터계 조성물의 제조 시스템 및 제조방법
EP4036075B1 (en) * 2019-09-27 2024-10-30 Lg Chem, Ltd. Method for preparing diester-based material
CN110938000A (zh) * 2019-12-09 2020-03-31 江苏国胶新材料有限公司 一种丙烯酸异辛酯的生产工艺方法
JP2023534443A (ja) * 2020-09-24 2023-08-09 エルジー・ケム・リミテッド エステル系組成物の製造方法
US20240010937A1 (en) * 2022-07-07 2024-01-11 Uop Llc Process for recovery of pyrolysis oil extraction solvent

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2503195C3 (de) 1975-01-27 1984-10-18 Henkel KGaA, 4000 Düsseldorf Verfahren und Vorrichtung zur kontinuierlichen katalytischen Veresterung von Fettsäuren mit Alkoholen
DE3809417A1 (de) 1988-03-21 1989-10-12 Henkel Kgaa Verfahren zur kontinuierlichen veresterung von fettsaeuren
GB8618888D0 (en) * 1986-08-01 1986-09-10 Davy Mckee Ltd Process
IN171820B (enExample) * 1989-12-22 1993-01-16 Lever Hindustan Ltd
GB9102513D0 (en) 1991-02-06 1991-03-27 Exxon Chemical Patents Inc Hydrocarbon production
US5324853A (en) 1993-01-19 1994-06-28 Exxon Chemical Patents Inc. Process for the production of plasticizer and polyolesters
DE4339713A1 (de) 1993-11-22 1995-05-24 Basf Ag Verfahren zur Oligomerisierung von Olefinen zu hochlinearen Oligomeren und Katalysatoren dafür
EP0835860B1 (de) 1996-10-14 2001-06-13 Bayer Ag Verfahren zur Herstellung von Estern oder Alkoholaten unter Abtrennung von Wasser
JPH11189569A (ja) * 1997-12-25 1999-07-13 Mitsubishi Chemical Corp ジアルキルフタレートの製造方法
DE19955593A1 (de) 1999-11-18 2001-05-23 Basf Ag C13-Alkoholgemisch und funktionalisiertes C13-Alkoholgemisch
US6271410B1 (en) * 2000-06-06 2001-08-07 Creanova Inc. Higher alkyl esters of cyanoacetic acid
DE10043545A1 (de) * 2000-09-05 2002-03-14 Oxeno Olefinchemie Gmbh Verfahren zur Herstellung von Carbonsäureestern
TWI324592B (en) * 2002-11-28 2010-05-11 Sulzer Chemtech Ag A method for the esterification of a fatty acid
JP2007153814A (ja) * 2005-12-06 2007-06-21 Mitsubishi Chemicals Corp ジカルボン酸ジエステルの製造方法
US8273924B2 (en) 2007-08-31 2012-09-25 Basf Se Method for producing 1,2-propandiol by low-pressure hydrogenation of glycerine
BRPI0815783A2 (pt) 2007-08-31 2015-02-24 Basf Se Processo para a preparação de 1,2-propanodiol.
KR20100098631A (ko) 2007-11-13 2010-09-08 오스람 게젤샤프트 미트 베쉬랭크터 하프퉁 고압 방전 램프를 동작시키기 위한 회로 어레인지먼트와 방법
EP2107064A1 (de) 2008-04-02 2009-10-07 Basf Se Verfahren zur Herstellung von Triamiden aus Ammoniak und Amido-Dichloriden
US20110028579A1 (en) 2008-04-01 2011-02-03 Base Se Process for lightening the color of polyisocyanates with ozone-containing gas

Also Published As

Publication number Publication date
KR101733814B1 (ko) 2017-05-08
CN102256922A (zh) 2011-11-23
WO2010076194A1 (de) 2010-07-08
EP2379482B1 (de) 2015-08-26
MY157837A (en) 2016-07-29
JP5698146B2 (ja) 2015-04-08
CA2746571C (en) 2017-08-22
JP2012512231A (ja) 2012-05-31
CA2746571A1 (en) 2010-07-08
US20110301377A1 (en) 2011-12-08
EP2379482A1 (de) 2011-10-26
ES2554170T3 (es) 2015-12-16
KR20110101206A (ko) 2011-09-15
US8901344B2 (en) 2014-12-02

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Termination date: 20171215