CN102232064B - 从羰基化合物和氢氰酸制备羧酸酰胺的方法 - Google Patents

从羰基化合物和氢氰酸制备羧酸酰胺的方法 Download PDF

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Publication number
CN102232064B
CN102232064B CN200980148070.9A CN200980148070A CN102232064B CN 102232064 B CN102232064 B CN 102232064B CN 200980148070 A CN200980148070 A CN 200980148070A CN 102232064 B CN102232064 B CN 102232064B
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acid
reaction
carbonyl compound
meth
carried out
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English (en)
Chinese (zh)
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CN102232064A (zh
Inventor
A·迈
M·克斯特纳
J·贝克尔
J·沙伦贝格
H·西格特
B·福格尔
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Roma Chemical Co ltd
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Evonik Roehm GmbH
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/06—Preparation of carboxylic acid amides from nitriles by transformation of cyano groups into carboxamide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/06—Preparation of carboxylic acid amides from nitriles by transformation of cyano groups into carboxamide groups
    • C07C231/065—By hydration using metals or metallic ions as catalyst
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/14—Preparation of carboxylic acid amides by formation of carboxamide groups together with reactions not involving the carboxamide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN200980148070.9A 2008-12-01 2009-10-29 从羰基化合物和氢氰酸制备羧酸酰胺的方法 Expired - Fee Related CN102232064B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102008044218.6 2008-12-01
DE102008044218A DE102008044218A1 (de) 2008-12-01 2008-12-01 Verfahren zur Herstellung von einem Carbonsäureamid aus einer Carbonylverbindung und Blausäure
PCT/EP2009/064279 WO2010063520A1 (de) 2008-12-01 2009-10-29 Verfahren zur herstellung von einem carbonsäureamid aus einer carbonylverbindung und blausäure

Publications (2)

Publication Number Publication Date
CN102232064A CN102232064A (zh) 2011-11-02
CN102232064B true CN102232064B (zh) 2014-11-05

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CN200980148070.9A Expired - Fee Related CN102232064B (zh) 2008-12-01 2009-10-29 从羰基化合物和氢氰酸制备羧酸酰胺的方法

Country Status (14)

Country Link
US (1) US8975440B2 (enExample)
EP (1) EP2352720B1 (enExample)
JP (1) JP5757874B2 (enExample)
KR (1) KR101696940B1 (enExample)
CN (1) CN102232064B (enExample)
BR (1) BRPI0922626A2 (enExample)
CA (1) CA2745498A1 (enExample)
DE (1) DE102008044218A1 (enExample)
MX (1) MX2011005476A (enExample)
MY (1) MY159638A (enExample)
RU (1) RU2552619C9 (enExample)
SG (1) SG171871A1 (enExample)
TW (1) TWI471291B (enExample)
WO (1) WO2010063520A1 (enExample)

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MX2008014641A (es) * 2006-05-15 2008-11-27 Evonik Roehm Gmbh Proceso para preparar esteres alfa-hidroxicarboxilicos.
DE102006055428A1 (de) * 2006-11-22 2008-05-29 Evonik Röhm Gmbh Verfahren zur Herstellung von (Meth)acrylsäure
DE102006055430A1 (de) 2006-11-22 2008-05-29 Evonik Röhm Gmbh Verfahren zur Herstellung von Carbonsäureamiden durch Hydrolyse von Carbonsäurenitrilen in Gegenwart eines Mangandioxid umfassenden Katalysators
DE102008001319A1 (de) * 2008-04-22 2009-10-29 Evonik Röhm Gmbh Katalysator zur Umsetzung von Carbonsäurenitrilen
BR112013018092B1 (pt) 2011-02-23 2021-04-27 Evonik Operations Gmbh Método para produção de 2-hidróxi-4-(metiltio) butano nitrila a partir de 3- (metiltio) propanal e cianeto de hidrogênio, e uso de um produto de reação, que contém mmp-cianidrina
CN102295571B (zh) * 2011-06-01 2016-04-27 郭建行 甲醇或甲醛氨氧化合成酰胺的方法
US10227284B2 (en) 2014-09-10 2019-03-12 Evonik Roehm Gmbh Method for preparing alpha-hydroxycarboxylic acid esters in which ammonia is recycled
DE102016210285A1 (de) 2016-06-10 2017-12-14 Evonik Röhm Gmbh Verfahren zur Herstellung von Methacrylaten und Methacrylsäure
EP3392237B1 (de) 2017-04-21 2019-10-02 Evonik Degussa GmbH Verfahren zur herstellung von acroleincyanhydrinen
EP3604222A1 (en) * 2018-07-30 2020-02-05 Evonik Operations GmbH Process for the purification of hydrogen cyanide
CN112495391B (zh) * 2020-12-21 2021-09-14 中国科学院山西煤炭化学研究所 一种适用于乙腈水合反应制备乙酰胺的负载型复合金属催化剂及其制备方法和应用
US12492133B2 (en) * 2021-11-17 2025-12-09 Lg Chem, Ltd. Method for purifying of waste water
EP4452919A1 (de) 2021-12-23 2024-10-30 Röhm GmbH Verfahren zur herstellung von alkylmethacrylaten mit verbesserter ausbeute und verminderten emissionen flüchtiger organischer verbindungen
WO2023169810A1 (de) 2022-03-11 2023-09-14 Röhm Gmbh Verfahren zur herstellung von alpha-hydroxyisobuttersäuremethylester und dessen anwendung in der elektronik-industrie

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EP0407811A2 (en) * 1989-07-14 1991-01-16 Mitsubishi Gas Chemical Company, Inc. Process for producing methyl methacrylate
US4987256A (en) * 1989-09-07 1991-01-22 Mitsubishi Gas Chemical Company, Inc. Process for production of α-hydroxycarboxylic acid amide
EP0433611A1 (en) * 1989-12-19 1991-06-26 Mitsubishi Gas Chemical Company, Inc. Process for producing alpha-hydroxyisobutyric acid amide
CN101180259A (zh) * 2005-05-20 2008-05-14 赢创罗姆有限责任公司 制备（甲基）丙烯酸烷基酯的方法

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US3562320A (en) 1967-04-25 1971-02-09 Escambia Chem Corp Process for producing methacrylic acid
JPS4812727B1 (enExample) * 1969-10-21 1973-04-23
DE2202660C3 (de) * 1972-01-20 1983-12-29 Skw Trostberg Ag, 8223 Trostberg Verfahren zur Entfernung von Cyanidionen aus Abwasser
DE2527120A1 (de) 1975-06-18 1976-12-30 Roehm Gmbh Verfahren zur herstellung von alpha-hydroxyisobutyramid aus acetoncyanhydrin
US4950801A (en) 1989-01-19 1990-08-21 Mitsubishi Gas Chemical Company, Inc. Process for producing alpha-hydroxycarboxylic acid amide
JP2893730B2 (ja) 1989-07-04 1999-05-24 三菱瓦斯化学株式会社 メタクリル酸メチルの製造法
US5387715A (en) 1991-12-03 1995-02-07 Mitsui Toatsu Chemicals, Inc. Process for producing α-hydroxy-isobutyramide
JPH06172283A (ja) 1992-12-02 1994-06-21 Mitsui Toatsu Chem Inc α−ヒドロキシイソ酪酸アミドの製造方法
KR960000850A (ko) 1994-06-06 1996-01-25 사토 아키오 메타크릴산메틸의 연속제조방법
GB9719060D0 (en) 1997-09-09 1997-11-12 Ici Plc Polymer composition
JPH11255710A (ja) 1998-03-11 1999-09-21 Mitsubishi Gas Chem Co Inc メタクリル酸メチルの製造方法
JPH11319558A (ja) 1998-05-13 1999-11-24 Mitsubishi Gas Chem Co Inc シアンヒドリンの水和触媒
JP2002371046A (ja) * 2001-06-11 2002-12-26 Showa Denko Kk ２−ヒドロキシカルボン酸アミドの製法
DE102005023976A1 (de) 2005-05-20 2006-11-23 Röhm Gmbh Verfahren zur Umesterung
MX2008014641A (es) 2006-05-15 2008-11-27 Evonik Roehm Gmbh Proceso para preparar esteres alfa-hidroxicarboxilicos.
DE102007011706A1 (de) * 2007-03-08 2008-09-11 Evonik Röhm Gmbh Verfahren zur Herstellung von Alpha-Hydroxycarbonsäuren
DE102006055430A1 (de) 2006-11-22 2008-05-29 Evonik Röhm Gmbh Verfahren zur Herstellung von Carbonsäureamiden durch Hydrolyse von Carbonsäurenitrilen in Gegenwart eines Mangandioxid umfassenden Katalysators
DE102006055427A1 (de) 2006-11-22 2008-05-29 Evonik Röhm Gmbh Verfahren zur Herstellung von Tetramethylglycolid
DE102006055428A1 (de) 2006-11-22 2008-05-29 Evonik Röhm Gmbh Verfahren zur Herstellung von (Meth)acrylsäure
DE102006055426A1 (de) 2006-11-22 2008-05-29 Evonik Röhm Gmbh Verfahren zur Herstellung von Alkyl(meth)acrylaten unter Verwendung einer enzymatischen Cyanhydrinhydrolyse
DE102008001319A1 (de) 2008-04-22 2009-10-29 Evonik Röhm Gmbh Katalysator zur Umsetzung von Carbonsäurenitrilen

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EP0407811A2 (en) * 1989-07-14 1991-01-16 Mitsubishi Gas Chemical Company, Inc. Process for producing methyl methacrylate
US4987256A (en) * 1989-09-07 1991-01-22 Mitsubishi Gas Chemical Company, Inc. Process for production of α-hydroxycarboxylic acid amide
EP0433611A1 (en) * 1989-12-19 1991-06-26 Mitsubishi Gas Chemical Company, Inc. Process for producing alpha-hydroxyisobutyric acid amide
CN101180259A (zh) * 2005-05-20 2008-05-14 赢创罗姆有限责任公司 制备（甲基）丙烯酸烷基酯的方法

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2-甲基-2-羟基丙腈水合工艺改进;甘宏宇等;《合成化学》;19981231;第6卷(第4期);第426—429页 *

Also Published As

Publication number Publication date
MX2011005476A (es) 2011-06-16
RU2552619C9 (ru) 2016-01-20
JP5757874B2 (ja) 2015-08-05
EP2352720A1 (de) 2011-08-10
TW201031622A (en) 2010-09-01
KR101696940B1 (ko) 2017-01-16
TWI471291B (zh) 2015-02-01
WO2010063520A9 (de) 2011-06-03
CA2745498A1 (en) 2010-06-10
KR20110090993A (ko) 2011-08-10
JP2012510485A (ja) 2012-05-10
RU2552619C2 (ru) 2015-06-10
CN102232064A (zh) 2011-11-02
SG171871A1 (en) 2011-07-28
US20110306784A1 (en) 2011-12-15
EP2352720B1 (de) 2017-12-20
RU2011126760A (ru) 2013-01-10
WO2010063520A1 (de) 2010-06-10
US20120232305A2 (en) 2012-09-13
DE102008044218A1 (de) 2010-06-02
US8975440B2 (en) 2015-03-10
BRPI0922626A2 (pt) 2016-01-05
MY159638A (en) 2017-01-13

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Address after: Darmstadt, Germany

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Granted publication date: 20141105

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