CN102197064B - 使用高纯度4,4'-二氟二苯甲酮制备聚(芳基醚酮)的改进方法 - Google Patents
使用高纯度4,4'-二氟二苯甲酮制备聚(芳基醚酮)的改进方法 Download PDFInfo
- Publication number
- CN102197064B CN102197064B CN200980142463.9A CN200980142463A CN102197064B CN 102197064 B CN102197064 B CN 102197064B CN 200980142463 A CN200980142463 A CN 200980142463A CN 102197064 B CN102197064 B CN 102197064B
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- China
- Prior art keywords
- difluorobenzophenone
- dfbp
- poly
- ether ketone
- aryl ether
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/34—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives
- C08G65/38—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols
- C08G65/40—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols from phenols (I) and other compounds (II), e.g. OH-Ar-OH + X-Ar-X, where X is halogen atom, i.e. leaving group
- C08G65/4012—Other compound (II) containing a ketone group, e.g. X-Ar-C(=O)-Ar-X for polyetherketones
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D7/00—Carbonates of sodium, potassium or alkali metals in general
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C315/00—Preparation of sulfones; Preparation of sulfoxides
- C07C315/06—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/78—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/34—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives
- C08G65/38—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols
- C08G65/40—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols from phenols (I) and other compounds (II), e.g. OH-Ar-OH + X-Ar-X, where X is halogen atom, i.e. leaving group
- C08G65/4087—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols from phenols (I) and other compounds (II), e.g. OH-Ar-OH + X-Ar-X, where X is halogen atom, i.e. leaving group characterised by the catalyst used
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/34—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives
- C08G65/38—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols
- C08G65/40—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols from phenols (I) and other compounds (II), e.g. OH-Ar-OH + X-Ar-X, where X is halogen atom, i.e. leaving group
- C08G65/4093—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols from phenols (I) and other compounds (II), e.g. OH-Ar-OH + X-Ar-X, where X is halogen atom, i.e. leaving group characterised by the process or apparatus used
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G8/00—Condensation polymers of aldehydes or ketones with phenols only
- C08G8/02—Condensation polymers of aldehydes or ketones with phenols only of ketones
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G2261/00—Macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain of the macromolecule
- C08G2261/30—Monomer units or repeat units incorporating structural elements in the main chain
- C08G2261/34—Monomer units or repeat units incorporating structural elements in the main chain incorporating partially-aromatic structural elements in the main chain
- C08G2261/344—Monomer units or repeat units incorporating structural elements in the main chain incorporating partially-aromatic structural elements in the main chain containing heteroatoms
- C08G2261/3444—Polyethersulfones
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
- C08G75/20—Polysulfones
- C08G75/23—Polyethersulfones
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Polyethers (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Applications Claiming Priority (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10809608P | 2008-10-24 | 2008-10-24 | |
| US10809708P | 2008-10-24 | 2008-10-24 | |
| US61/108,096 | 2008-10-24 | ||
| US61/108,097 | 2008-10-24 | ||
| US14020508P | 2008-12-23 | 2008-12-23 | |
| US61/140,205 | 2008-12-23 | ||
| PCT/EP2009/064008 WO2010046483A1 (en) | 2008-10-24 | 2009-10-23 | Improved process for preparing a poly(aryl ether ketone) using a high purity 4,4'-difluorobenzophenone |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102197064A CN102197064A (zh) | 2011-09-21 |
| CN102197064B true CN102197064B (zh) | 2014-08-13 |
Family
ID=41445399
Family Applications (6)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200980151189.1A Expired - Fee Related CN102257033B (zh) | 2008-10-24 | 2009-10-23 | 用于制造聚(芳基醚酮)的改进的方法以及用于提供适合于制造聚(芳基醚酮)的碳酸钠的改进的方法 |
| CN200980142309.1A Active CN102203165B (zh) | 2008-10-24 | 2009-10-23 | 高纯度二苯砜、其制备以及用于制备聚(芳基醚酮)的用途 |
| CN200980151210.8A Active CN102257034B (zh) | 2008-10-24 | 2009-10-23 | 在碳酸钠的存在下制造聚(芳基醚酮)的方法 |
| CN201910088673.XA Pending CN109912794A (zh) | 2008-10-24 | 2009-10-23 | 高纯度二苯砜、其制备以及用于制备聚(芳基醚酮)的用途 |
| CN200980142463.9A Active CN102197064B (zh) | 2008-10-24 | 2009-10-23 | 使用高纯度4,4'-二氟二苯甲酮制备聚(芳基醚酮)的改进方法 |
| CN201610339978.XA Active CN106167545B (zh) | 2008-10-24 | 2009-10-23 | 高纯度二苯砜、其制备以及用于制备聚(芳基醚酮)的用途 |
Family Applications Before (4)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200980151189.1A Expired - Fee Related CN102257033B (zh) | 2008-10-24 | 2009-10-23 | 用于制造聚(芳基醚酮)的改进的方法以及用于提供适合于制造聚(芳基醚酮)的碳酸钠的改进的方法 |
| CN200980142309.1A Active CN102203165B (zh) | 2008-10-24 | 2009-10-23 | 高纯度二苯砜、其制备以及用于制备聚(芳基醚酮)的用途 |
| CN200980151210.8A Active CN102257034B (zh) | 2008-10-24 | 2009-10-23 | 在碳酸钠的存在下制造聚(芳基醚酮)的方法 |
| CN201910088673.XA Pending CN109912794A (zh) | 2008-10-24 | 2009-10-23 | 高纯度二苯砜、其制备以及用于制备聚(芳基醚酮)的用途 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610339978.XA Active CN106167545B (zh) | 2008-10-24 | 2009-10-23 | 高纯度二苯砜、其制备以及用于制备聚(芳基醚酮)的用途 |
Country Status (8)
| Country | Link |
|---|---|
| US (7) | US9175136B2 (OSRAM) |
| EP (5) | EP2342261A1 (OSRAM) |
| JP (5) | JP5606443B2 (OSRAM) |
| CN (6) | CN102257033B (OSRAM) |
| AU (1) | AU2009306298A1 (OSRAM) |
| CA (3) | CA2741016C (OSRAM) |
| RU (1) | RU2011120794A (OSRAM) |
| WO (4) | WO2010046482A1 (OSRAM) |
Families Citing this family (49)
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|---|---|---|---|---|
| CN102257033B (zh) * | 2008-10-24 | 2014-01-29 | 索维高级聚合物股份有限公司 | 用于制造聚(芳基醚酮)的改进的方法以及用于提供适合于制造聚(芳基醚酮)的碳酸钠的改进的方法 |
| CN101580583B (zh) * | 2009-06-26 | 2011-03-30 | 金发科技股份有限公司 | 采用四元共聚技术制备聚芳醚酮类共聚物的方法 |
| KR20120032014A (ko) | 2009-07-24 | 2012-04-04 | 인비스타 테크놀러지스 에스.에이.알.엘. | 이온성 액체를 사용하는 합성 방법 |
| JP5316727B1 (ja) * | 2011-09-21 | 2013-10-16 | 東レ株式会社 | 環式ポリフェニレンエーテルエーテルケトン組成物の回収方法およびそれを用いたポリフェニレンエーテルエーテルケトンの製造方法 |
| WO2014097564A1 (ja) * | 2012-12-21 | 2014-06-26 | 東レ株式会社 | 環式ポリフェニレンエーテルエーテルケトン組成物および線状ポリフェニレンエーテルエーテルケトンの製造方法、ポリフェニレンエーテルエーテルケトンの製造方法 |
| JP6221311B2 (ja) * | 2013-04-05 | 2017-11-01 | 東レ株式会社 | ポリフェニレンエーテルエーテルケトンの製造方法 |
| US20160075833A1 (en) * | 2013-05-02 | 2016-03-17 | Basf Se | Polyarylethersulfone copolymers |
| JP6169255B2 (ja) * | 2013-05-02 | 2017-07-26 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | ポリアリールエーテルスルホンコポリマー |
| GB201311376D0 (en) | 2013-06-26 | 2013-08-14 | Victrex Mfg Ltd | Polymetric Materials |
| GB2526243B (en) | 2014-02-24 | 2021-07-14 | Victrex Mfg Ltd | Polymeric materials |
| GB201409128D0 (en) * | 2014-05-22 | 2014-07-09 | Ketonex Ltd | Method |
| WO2016028614A1 (en) | 2014-08-21 | 2016-02-25 | Ticona Llc | Composition containing a polyaryletherketone and low naphthenic liquid crystalline polymer |
| EP3183321A1 (en) | 2014-08-21 | 2017-06-28 | Ticona LLC | Polyaryletherketone composition |
| GB201415972D0 (en) | 2014-09-10 | 2014-10-22 | Ketonex Ltd | Process |
| JP6841759B2 (ja) * | 2014-12-19 | 2021-03-10 | メルク パテント ゲゼルシャフト ミット ベシュレンクテル ハフツングMerck Patent Gesellschaft mit beschraenkter Haftung | ビメソゲン化合物およびメソゲン性媒体 |
| JP2018502972A (ja) * | 2015-01-23 | 2018-02-01 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | 溶融重合法からのポリアリールエーテルの脱塩 |
| EP3247737B1 (de) * | 2015-01-23 | 2018-10-24 | Basf Se | Entsalzung von polyarylethern mittels schmelzeextraktion |
| EP3222651A1 (de) | 2016-03-21 | 2017-09-27 | Basf Se | Entsalzung von polyarylethern mittels schmelzeextraktion |
| GB2569512A (en) * | 2016-09-26 | 2019-06-19 | Victrex Mfg Ltd | Polymers and process for their manufacture |
| WO2018086873A1 (en) | 2016-11-11 | 2018-05-17 | Solvay Specialty Polymers Usa, Llc | Polyarylether ketone copolymer |
| JP7262387B2 (ja) | 2016-11-11 | 2023-04-21 | ソルベイ スペシャルティ ポリマーズ ユーエスエー, エルエルシー | ポリアリールエーテルケトンコポリマー |
| EP3559085B2 (en) * | 2016-12-21 | 2025-08-06 | Solvay Specialty Polymers USA, LLC | Poly(ether ketone ketone) polymers |
| WO2018115035A1 (en) | 2016-12-21 | 2018-06-28 | Solvay Specialty Polymers Usa, Llc | Poly(ether ketone ketone) polymers, corresponding synthesis methods and polymer compositions and articles made therefrom |
| EP3558918B1 (en) * | 2016-12-21 | 2021-11-10 | Solvay Specialty Polymers USA, LLC | Method for decreasing the concentration of a metal in a monomer composition comprising bis(benzoyl)benzene |
| WO2018115033A1 (en) | 2016-12-21 | 2018-06-28 | Solvay Specialty Polymers Usa, Llc | Poly(ether ketone ketone) polymers, corresponding synthesis methods and polymer compositions and articles made therefrom |
| CN110248984B (zh) | 2016-12-21 | 2022-03-04 | 索尔维特殊聚合物美国有限责任公司 | 聚(醚酮酮)聚合物、相应的合成方法和聚合物组合物以及由其制成的制品 |
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| CN111417670B (zh) | 2017-12-20 | 2024-05-17 | 索尔维特殊聚合物美国有限责任公司 | 制造PEEK-PEmEK共聚物的方法和由该方法获得的共聚物 |
| EP3810678A1 (en) * | 2018-06-21 | 2021-04-28 | Solvay Specialty Polymers USA, LLC. | Poly(ether ketone ketone) (pekk) polymer and composites |
| CN109061026B (zh) * | 2018-09-05 | 2020-12-25 | 九江天赐高新材料有限公司 | 一种对合成的peek样品进行分析检测的方法 |
| US10731001B2 (en) | 2018-11-09 | 2020-08-04 | Arkema France | Method for the recovery of compounds deriving from the synthesis of poly aryl ether ketone polymers |
| EP3650095B1 (en) | 2018-11-09 | 2025-09-03 | Arkema France | Method for the recovery of compounds deriving from the synthesis of aryl ether ketones by evaporation with a rotor |
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| US11845832B2 (en) | 2019-06-20 | 2023-12-19 | Solvay Specialty Polymers Usa, Llc | Method of making a PEEK-PEoEK copolymer and copolymer obtained from the method |
| WO2020254096A1 (en) | 2019-06-20 | 2020-12-24 | Solvay Specialty Polymers Usa, Llc | Peek-peodek copolymer and method of making the copolymer |
| WO2021001132A1 (en) | 2019-07-01 | 2021-01-07 | Solvay Specialty Polymers Usa, Llc | PEEK-PEoEK COPOLYMER POWDER AND METHOD OF PREPARING THE POWDER |
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| CN113912799B (zh) * | 2021-09-16 | 2022-05-10 | 吉林省中研高分子材料股份有限公司 | 聚醚醚酮及其制备方法 |
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