CN102040726B - 一种高性能油墨树脂的制备方法 - Google Patents
一种高性能油墨树脂的制备方法 Download PDFInfo
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- CN102040726B CN102040726B CN 201010507483 CN201010507483A CN102040726B CN 102040726 B CN102040726 B CN 102040726B CN 201010507483 CN201010507483 CN 201010507483 CN 201010507483 A CN201010507483 A CN 201010507483A CN 102040726 B CN102040726 B CN 102040726B
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- 229920005989 resin Polymers 0.000 title claims abstract description 37
- 239000011347 resin Substances 0.000 title claims abstract description 37
- 238000002360 preparation method Methods 0.000 title claims abstract description 24
- 238000007639 printing Methods 0.000 title abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 40
- 150000002148 esters Chemical class 0.000 claims abstract description 38
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 36
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims abstract description 29
- 238000006243 chemical reaction Methods 0.000 claims abstract description 23
- 239000004814 polyurethane Substances 0.000 claims abstract description 14
- 229920002635 polyurethane Polymers 0.000 claims abstract description 14
- 229920001730 Moisture cure polyurethane Polymers 0.000 claims abstract description 10
- 239000000203 mixture Substances 0.000 claims description 32
- 239000000178 monomer Substances 0.000 claims description 26
- 239000003999 initiator Substances 0.000 claims description 18
- 239000002904 solvent Substances 0.000 claims description 18
- 238000003756 stirring Methods 0.000 claims description 16
- 239000000243 solution Substances 0.000 claims description 14
- BAPJBEWLBFYGME-UHFFFAOYSA-N Methyl acrylate Chemical compound COC(=O)C=C BAPJBEWLBFYGME-UHFFFAOYSA-N 0.000 claims description 12
- JOYRKODLDBILNP-UHFFFAOYSA-N urethane group Chemical group NC(=O)OCC JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 11
- 238000006116 polymerization reaction Methods 0.000 claims description 11
- VVWRJUBEIPHGQF-UHFFFAOYSA-N propan-2-yl n-propan-2-yloxycarbonyliminocarbamate Chemical group CC(C)OC(=O)N=NC(=O)OC(C)C VVWRJUBEIPHGQF-UHFFFAOYSA-N 0.000 claims description 10
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims description 10
- 229920002554 vinyl polymer Polymers 0.000 claims description 10
- 238000010792 warming Methods 0.000 claims description 10
- 238000012856 packing Methods 0.000 claims description 9
- 229920002125 Sokalan® Polymers 0.000 claims description 8
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 claims description 8
- 238000001816 cooling Methods 0.000 claims description 8
- 229920001577 copolymer Polymers 0.000 claims description 8
- 239000004584 polyacrylic acid Substances 0.000 claims description 8
- DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical compound CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 claims description 8
- 239000004721 Polyphenylene oxide Substances 0.000 claims description 6
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims description 6
- 238000010790 dilution Methods 0.000 claims description 6
- 239000012895 dilution Substances 0.000 claims description 6
- 150000002009 diols Chemical class 0.000 claims description 6
- 150000002334 glycols Chemical class 0.000 claims description 6
- 229920000728 polyester Polymers 0.000 claims description 6
- 229920000570 polyether Polymers 0.000 claims description 6
- JIGUQPWFLRLWPJ-UHFFFAOYSA-N Ethyl acrylate Chemical compound CCOC(=O)C=C JIGUQPWFLRLWPJ-UHFFFAOYSA-N 0.000 claims description 5
- 238000005516 engineering process Methods 0.000 claims description 5
- PNJWIWWMYCMZRO-UHFFFAOYSA-N pent‐4‐en‐2‐one Natural products CC(=O)CC=C PNJWIWWMYCMZRO-UHFFFAOYSA-N 0.000 claims description 5
- OMIGHNLMNHATMP-UHFFFAOYSA-N 2-hydroxyethyl prop-2-enoate Chemical group OCCOC(=O)C=C OMIGHNLMNHATMP-UHFFFAOYSA-N 0.000 claims description 4
- UPMLOUAZCHDJJD-UHFFFAOYSA-N 4,4'-Diphenylmethane Diisocyanate Chemical compound C1=CC(N=C=O)=CC=C1CC1=CC=C(N=C=O)C=C1 UPMLOUAZCHDJJD-UHFFFAOYSA-N 0.000 claims description 4
- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical compound CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 claims description 4
- 239000005057 Hexamethylene diisocyanate Substances 0.000 claims description 4
- DKPFZGUDAPQIHT-UHFFFAOYSA-N butyl acetate Chemical compound CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 claims description 4
- 239000003054 catalyst Substances 0.000 claims description 4
- 238000007865 diluting Methods 0.000 claims description 4
- RRAMGCGOFNQTLD-UHFFFAOYSA-N hexamethylene diisocyanate Chemical compound O=C=NCCCCCCN=C=O RRAMGCGOFNQTLD-UHFFFAOYSA-N 0.000 claims description 4
- NIMLQBUJDJZYEJ-UHFFFAOYSA-N isophorone diisocyanate Chemical compound CC1(C)CC(N=C=O)CC(C)(CN=C=O)C1 NIMLQBUJDJZYEJ-UHFFFAOYSA-N 0.000 claims description 4
- GWZMWHWAWHPNHN-UHFFFAOYSA-N 2-hydroxypropyl prop-2-enoate Chemical compound CC(O)COC(=O)C=C GWZMWHWAWHPNHN-UHFFFAOYSA-N 0.000 claims description 3
- ZMARGGQEAJXRFP-UHFFFAOYSA-N 1-hydroxypropan-2-yl 2-methylprop-2-enoate Chemical compound OCC(C)OC(=O)C(C)=C ZMARGGQEAJXRFP-UHFFFAOYSA-N 0.000 claims description 2
- DSCFFEYYQKSRSV-UHFFFAOYSA-N 1L-O1-methyl-muco-inositol Natural products COC1C(O)C(O)C(O)C(O)C1O DSCFFEYYQKSRSV-UHFFFAOYSA-N 0.000 claims description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims description 2
- OMPJBNCRMGITSC-UHFFFAOYSA-N Benzoylperoxide Chemical compound C=1C=CC=CC=1C(=O)OOC(=O)C1=CC=CC=C1 OMPJBNCRMGITSC-UHFFFAOYSA-N 0.000 claims description 2
- SOGAXMICEFXMKE-UHFFFAOYSA-N Butylmethacrylate Chemical compound CCCCOC(=O)C(C)=C SOGAXMICEFXMKE-UHFFFAOYSA-N 0.000 claims description 2
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 claims description 2
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims description 2
- 238000010526 radical polymerization reaction Methods 0.000 claims description 2
- 239000002994 raw material Substances 0.000 claims description 2
- 229920003023 plastic Polymers 0.000 abstract description 21
- 239000004033 plastic Substances 0.000 abstract description 21
- 239000000758 substrate Substances 0.000 abstract description 12
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- 229920006378 biaxially oriented polypropylene Polymers 0.000 abstract description 6
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- 230000001070 adhesive effect Effects 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 4
- 229920000058 polyacrylate Polymers 0.000 abstract description 3
- -1 polyethylene terephthalate Polymers 0.000 abstract description 3
- 238000007646 gravure printing Methods 0.000 abstract 3
- 239000004698 Polyethylene Substances 0.000 abstract 2
- 239000004417 polycarbonate Substances 0.000 abstract 2
- 229920000573 polyethylene Polymers 0.000 abstract 2
- 229920000139 polyethylene terephthalate Polymers 0.000 abstract 2
- 239000005020 polyethylene terephthalate Substances 0.000 abstract 2
- 239000004800 polyvinyl chloride Substances 0.000 abstract 2
- 229920000915 polyvinyl chloride Polymers 0.000 abstract 2
- 239000004952 Polyamide Substances 0.000 abstract 1
- 230000006978 adaptation Effects 0.000 abstract 1
- 238000004132 cross linking Methods 0.000 abstract 1
- 239000012948 isocyanate Substances 0.000 abstract 1
- 150000002513 isocyanates Chemical class 0.000 abstract 1
- 229920002647 polyamide Polymers 0.000 abstract 1
- 229920000515 polycarbonate Polymers 0.000 abstract 1
- 235000019441 ethanol Nutrition 0.000 description 27
- 239000007787 solid Substances 0.000 description 12
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 9
- 150000001875 compounds Chemical class 0.000 description 9
- 239000011230 binding agent Substances 0.000 description 7
- 239000000463 material Substances 0.000 description 6
- 238000009835 boiling Methods 0.000 description 5
- 239000002131 composite material Substances 0.000 description 5
- 239000003292 glue Substances 0.000 description 5
- 239000012046 mixed solvent Substances 0.000 description 5
- 206010013786 Dry skin Diseases 0.000 description 4
- 238000007599 discharging Methods 0.000 description 4
- 238000001035 drying Methods 0.000 description 4
- 238000011049 filling Methods 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 239000000049 pigment Substances 0.000 description 4
- 239000004576 sand Substances 0.000 description 4
- 238000011161 development Methods 0.000 description 3
- 230000007613 environmental effect Effects 0.000 description 3
- 238000004806 packaging method and process Methods 0.000 description 3
- 229920001470 polyketone Polymers 0.000 description 3
- 239000005058 Isophorone diisocyanate Substances 0.000 description 2
- 238000003556 assay Methods 0.000 description 2
- 239000012752 auxiliary agent Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 125000005594 diketone group Chemical group 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 238000003801 milling Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
- 239000002390 adhesive tape Substances 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 230000003749 cleanliness Effects 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 239000000306 component Substances 0.000 description 1
- 238000007334 copolymerization reaction Methods 0.000 description 1
- 239000008358 core component Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 229920006122 polyamide resin Polymers 0.000 description 1
- 230000000379 polymerizing effect Effects 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 235000010215 titanium dioxide Nutrition 0.000 description 1
Abstract
Description
检测项目 | 国家标准 | 检测值 | 结果 |
细度(μm)(刮板仪) | ≤25 | ≤10 | 合格 |
着色力(%) | 95~110 | 98~105 | 合格 |
粘度(s)(4#杯/25℃) | 25~70 | 28~50 | 合格 |
初干(mm)(30s/25℃) | 25~50 | 28~38 | 合格 |
附着牢度(%)(胶带法) | ≥85 | 93~98 | 合格 |
苯含量(ppm) | / | 无 | 合格 |
Claims (2)
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CN 201010507483 CN102040726B (zh) | 2010-10-15 | 2010-10-15 | 一种高性能油墨树脂的制备方法 |
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CN 201010507483 CN102040726B (zh) | 2010-10-15 | 2010-10-15 | 一种高性能油墨树脂的制备方法 |
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CN102040726A CN102040726A (zh) | 2011-05-04 |
CN102040726B true CN102040726B (zh) | 2012-01-25 |
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Families Citing this family (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102898659B (zh) * | 2011-07-28 | 2015-01-21 | 中国科学院化学研究所 | 聚丙烯酸酯-聚氨酯复合油墨连接料 |
CN103739785B (zh) * | 2012-10-17 | 2018-05-08 | 成都托展新材料股份有限公司 | Pvc热收缩膜用醇水性油墨树脂的制备方法 |
CN103772639A (zh) * | 2012-10-21 | 2014-05-07 | 成都市新津托展油墨有限公司 | 一种聚氨酯丙烯酸酯油墨树脂及其制备方法 |
CN104151561A (zh) * | 2014-08-04 | 2014-11-19 | 山西省应用化学研究所 | 印刷油墨用聚丙烯酸酯-聚氨酯树脂的制备方法 |
CN107698735A (zh) * | 2017-10-31 | 2018-02-16 | 广东丽格科技股份有限公司 | 一种低粘度聚酯树脂及其制备方法和应用 |
CN108840969A (zh) * | 2018-06-08 | 2018-11-20 | 常熟国和新材料有限公司 | 一种水性油墨树脂 |
CN110857342A (zh) * | 2018-08-08 | 2020-03-03 | 山西惠谷嘉旭生物科技有限公司 | 一种生物质基低碳可降解防滑餐垫及其制备方法 |
CN109651875B (zh) * | 2018-12-28 | 2020-06-12 | 中国科学院化学研究所 | 通用型水性油墨及其制备方法 |
CN109627844B (zh) * | 2019-01-30 | 2021-09-14 | 厦门红蚁化工有限公司 | 一种耐蒸煮耐凹版墨连接料及其制备方法 |
CN111019432A (zh) * | 2019-12-05 | 2020-04-17 | 曾令涛 | 一种3d复合板手机壳用油墨及其制备方法 |
CN112831020A (zh) * | 2020-12-31 | 2021-05-25 | 东胜化学(上海)有限公司 | 一种柔性线路板油墨树脂及其制备方法 |
CN115233454A (zh) * | 2022-06-30 | 2022-10-25 | 海宁市饰雅纺织有限公司 | 一种仿羊皮手感烫金沙发面料生产工艺 |
CN115304954B (zh) * | 2022-07-20 | 2023-08-11 | 成都托展新材料股份有限公司 | 一种凹版印刷油墨树脂及其制备方法 |
CN116265536B (zh) * | 2023-03-13 | 2024-03-12 | 上海欧畅新材料科技有限公司 | 一种pvc基材用水性油墨及其制备与应用 |
CN116120786B (zh) * | 2023-04-17 | 2023-07-14 | 深圳市龙腾电路科技有限公司 | 一种耐高温pcb板用的碳系水性导电油墨及其制备方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1865313A (zh) * | 2006-04-27 | 2006-11-22 | 华南理工大学 | 一种氨基硅烷改性的聚氨酯丙烯酸酯树脂的制备方法 |
CN1970655A (zh) * | 2006-12-15 | 2007-05-30 | 成都市新津托展油墨有限公司 | 凹版醇水性复合塑料油墨及其制备工艺 |
CN101121770A (zh) * | 2006-08-11 | 2008-02-13 | 上海市涂料研究所 | 水性丙烯酸树脂及其制备方法 |
-
2010
- 2010-10-15 CN CN 201010507483 patent/CN102040726B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1865313A (zh) * | 2006-04-27 | 2006-11-22 | 华南理工大学 | 一种氨基硅烷改性的聚氨酯丙烯酸酯树脂的制备方法 |
CN101121770A (zh) * | 2006-08-11 | 2008-02-13 | 上海市涂料研究所 | 水性丙烯酸树脂及其制备方法 |
CN1970655A (zh) * | 2006-12-15 | 2007-05-30 | 成都市新津托展油墨有限公司 | 凹版醇水性复合塑料油墨及其制备工艺 |
Non-Patent Citations (1)
Title |
---|
吴腊梅."丙烯酸聚氨酯树脂的制备和应用".《湖北化工》.1992,(第4期), |
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