CN101990521A - 在水溶性氟化添加剂存在下硫酸银微粒的制备 - Google Patents

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Publication number

CN101990521A

CN101990521A CN2009801126165A CN200980112616A CN101990521A CN 101990521 A CN101990521 A CN 101990521A CN 2009801126165 A CN2009801126165 A CN 2009801126165A CN 200980112616 A CN200980112616 A CN 200980112616A CN 101990521 A CN101990521 A CN 101990521A

Authority

CN

China

Prior art keywords

sulfuric acid

salt

silver

acid disilver

disilver salt

Prior art date

2008-04-11

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Pending

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• YPNVIBVEFVRZPJ-UHFFFAOYSA-L silver sulfate Chemical compound [Ag+].[Ag+].[O-]S([O-])(=O)=O YPNVIBVEFVRZPJ-UHFFFAOYSA-L 0.000 title claims abstract description 133
• 239000000654 additive Substances 0.000 title claims abstract description 106
• 229910000367 silver sulfate Inorganic materials 0.000 title abstract 5
• 238000004519 manufacturing process Methods 0.000 title description 11
• 238000000034 method Methods 0.000 claims abstract description 100
• 238000001556 precipitation Methods 0.000 claims abstract description 49
• 230000008569 process Effects 0.000 claims abstract description 49
• 230000000996 additive effect Effects 0.000 claims abstract description 39
• 238000006243 chemical reaction Methods 0.000 claims abstract description 33
• GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 claims abstract description 20
• QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims abstract description 10
• -1 polyoxyethylene Polymers 0.000 claims description 191
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• SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 claims description 59
• 239000005020 polyethylene terephthalate Substances 0.000 claims description 57
• BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims description 52
• 229910052921 ammonium sulfate Inorganic materials 0.000 claims description 52
• 235000011130 ammonium sulphate Nutrition 0.000 claims description 52
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• 229910001961 silver nitrate Inorganic materials 0.000 claims description 30
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• WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 15
• ICIWUVCWSCSTAQ-UHFFFAOYSA-M iodate Chemical compound [O-]I(=O)=O ICIWUVCWSCSTAQ-UHFFFAOYSA-M 0.000 claims description 14
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• LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 claims description 7
• SXDBWCPKPHAZSM-UHFFFAOYSA-M bromate Inorganic materials [O-]Br(=O)=O SXDBWCPKPHAZSM-UHFFFAOYSA-M 0.000 claims description 7
• AHHWIHXENZJRFG-UHFFFAOYSA-N oxetane Chemical compound C1COC1 AHHWIHXENZJRFG-UHFFFAOYSA-N 0.000 claims description 6
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• 239000001230 potassium iodate Substances 0.000 claims description 6
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• SXDBWCPKPHAZSM-UHFFFAOYSA-N bromic acid Chemical compound OBr(=O)=O SXDBWCPKPHAZSM-UHFFFAOYSA-N 0.000 claims description 5
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