CN101970614A - 从烃料流中脱除汞的方法 - Google Patents

从烃料流中脱除汞的方法 Download PDF

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Publication number
CN101970614A
CN101970614A CN2009801084389A CN200980108438A CN101970614A CN 101970614 A CN101970614 A CN 101970614A CN 2009801084389 A CN2009801084389 A CN 2009801084389A CN 200980108438 A CN200980108438 A CN 200980108438A CN 101970614 A CN101970614 A CN 101970614A
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CN
China
Prior art keywords
mercury
absorbent
weight
oxide
copper
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CN2009801084389A
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English (en)
Chinese (zh)
Inventor
P·鲁道夫
M·本德尔
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BASF SE
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BASF SE
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Publication of CN101970614A publication Critical patent/CN101970614A/zh
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G25/00—Refining of hydrocarbon oils in the absence of hydrogen, with solid sorbents
    • C10G25/003—Specific sorbent material, not covered by C10G25/02 or C10G25/03
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/11—Purification; Separation; Use of additives by absorption, i.e. purification or separation of gaseous hydrocarbons with the aid of liquids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/0203—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04
    • B01J20/0233—Compounds of Cu, Ag, Au
    • B01J20/0237—Compounds of Cu
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
    • B01J20/041—Oxides or hydroxides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/06—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/06—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04
    • B01J20/08—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04 comprising aluminium oxide or hydroxide; comprising bauxite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/103—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate comprising silica
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3202—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the carrier, support or substrate used for impregnation or coating
    • B01J20/3204—Inorganic carriers, supports or substrates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3231—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
    • B01J20/3234—Inorganic material layers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3231—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
    • B01J20/3234—Inorganic material layers
    • B01J20/3236—Inorganic material layers containing metal, other than zeolites, e.g. oxides, hydroxides, sulphides or salts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/34—Regenerating or reactivating
    • B01J20/345—Regenerating or reactivating using a particular desorbing compound or mixture
    • B01J20/3458—Regenerating or reactivating using a particular desorbing compound or mixture in the gas phase
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/34—Regenerating or reactivating
    • B01J20/3483—Regenerating or reactivating by thermal treatment not covered by groups B01J20/3441 - B01J20/3475, e.g. by heating or cooling
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/86—Chromium
    • B01J23/868—Chromium copper and chromium
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C10G45/02—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2251/00—Reactants
    • B01D2251/20—Reductants
    • B01D2251/202—Hydrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/112—Metals or metal compounds not provided for in B01D2253/104 or B01D2253/106
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/60—Heavy metals or heavy metal compounds
    • B01D2257/602—Mercury or mercury compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/50—Aspects relating to the use of sorbent or filter aid materials
    • B01J2220/56—Use in the form of a bed
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/72—Copper

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Materials Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Catalysts (AREA)
CN2009801084389A 2008-03-10 2009-03-09 从烃料流中脱除汞的方法 Pending CN101970614A (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP08152517.2 2008-03-10
EP08152517 2008-03-10
PCT/EP2009/052693 WO2009112440A1 (de) 2008-03-10 2009-03-09 Verfahren zur abtrennung von quecksilber aus kohlenwasserstoffströmen

Publications (1)

Publication Number Publication Date
CN101970614A true CN101970614A (zh) 2011-02-09

Family

ID=40558912

Family Applications (1)

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CN2009801084389A Pending CN101970614A (zh) 2008-03-10 2009-03-09 从烃料流中脱除汞的方法

Country Status (6)

Country Link
US (1) US20110005975A1 (https=)
EP (1) EP2265695A1 (https=)
JP (1) JP5455939B2 (https=)
KR (1) KR20100133394A (https=)
CN (1) CN101970614A (https=)
WO (1) WO2009112440A1 (https=)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102764655A (zh) * 2011-12-23 2012-11-07 盐城工学院 一种新型脱汞催化剂
CN104582834A (zh) * 2012-02-06 2015-04-29 环球油品公司 用于汞脱除的保护吸附剂及其制备和使用方法
CN105148913A (zh) * 2015-10-08 2015-12-16 宁波海越新材料有限公司 一种用于仲丁醇制备甲乙酮的催化剂及其制备方法
CN108249955A (zh) * 2018-04-02 2018-07-06 中科京投环境科技江苏有限公司 一种脱除废、污水中汞的复合陶瓷材料及制备方法
CN115698231A (zh) * 2020-05-29 2023-02-03 埃克森美孚化学专利公司 含汞进料的烃热解

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20090031900A (ko) * 2006-06-21 2009-03-30 바스프 에스이 수은 제거를 위한 흡착 조성물 및 방법
JP6076854B2 (ja) * 2013-08-07 2017-02-08 Ｊｘエネルギー株式会社 炭化水素油中の水銀の除去方法

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US3227645A (en) * 1962-01-22 1966-01-04 Chevron Res Combined process for metal removal and hydrocracking of high boiling oils
US3755989A (en) * 1972-06-16 1973-09-04 Union Carbide Corp Removal of mercury from gas streams
IT1043119B (it) * 1975-10-03 1980-02-20 Tecneco Spa Metodo per la rimozione di mer curio metallico
DE2656803C2 (de) * 1975-12-18 1986-12-18 Institut Français du Pétrole, Rueil-Malmaison, Hauts-de-Seine Verfahren zur Entfernung von in einem Gas oder in einer Flüssigkeit vorhandenem Quecksilber
US4230486A (en) * 1978-04-28 1980-10-28 Olin Corporation Process for removal and recovery of mercury from liquids
AU559284B2 (en) * 1982-07-08 1987-03-05 Takeda Chemical Industries Ltd. Adsorption of mercury vapour
FR2628338B1 (fr) * 1988-03-10 1991-01-04 Inst Francais Du Petrole Procede pour l'elimination du mercure dans les hydrocarbures
US4909926A (en) * 1989-02-01 1990-03-20 Mobil Oil Corporation Method for removing mercury from hydrocarbon oil by high temperature reactive adsorption
JP2578514B2 (ja) * 1989-03-03 1997-02-05 三井石油化学工業株式会社 液体炭化水素化合物中の水銀の除去方法
US5401392A (en) * 1989-03-16 1995-03-28 Institut Francais Du Petrole Process for eliminating mercury and possibly arsenic in hydrocarbons
FR2644472B1 (fr) * 1989-03-16 1991-06-21 Inst Francais Du Petrole Procede pour l'elimination du mercure et eventuellement d'arsenic dans les hydrocarbures
WO1991015559A2 (en) * 1990-04-04 1991-10-17 Exxon Chemical Patents Inc. Mercury removal by dispersed-metal adsorbents
US5080799A (en) * 1990-05-23 1992-01-14 Mobil Oil Corporation Hg removal from wastewater by regenerative adsorption
FR2673191B1 (fr) * 1991-02-27 1994-02-04 Institut Francais Petrole Procede d'enlevement de mercure et/ou d'arsenic des charges des unites de desaromatisation de solvants. .
DE4221207A1 (de) * 1992-06-27 1994-01-05 Huels Chemische Werke Ag Verfahren zur Entfernung von Quecksilber aus Flüssigkeiten
FR2701270B1 (fr) * 1993-02-08 1995-04-14 Inst Francais Du Petrole Procédé d'élimination du mercure dans les hydrocarbures par passage sur un catalyseur présulfuré.
US5948726A (en) * 1994-12-07 1999-09-07 Project Earth Industries, Inc. Adsorbent and/or catalyst and binder system and method of making therefor
FR2764214B1 (fr) * 1997-06-10 1999-07-16 Inst Francais Du Petrole Procede et masses de captation pour l'elimination du mercure et de l'arsenic dans les coupes hydrocarbonees
JP2004167306A (ja) * 2002-11-18 2004-06-17 Ict:Kk 排ガス浄化用触媒および排ガス浄化方法
DE10255240A1 (de) * 2002-11-26 2004-06-09 Basf Ag Verfahren zur Entfernung von Quecksilber aus mit Quecksilber verunreinigten Lösungen
KR20090031900A (ko) * 2006-06-21 2009-03-30 바스프 에스이 수은 제거를 위한 흡착 조성물 및 방법

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102764655A (zh) * 2011-12-23 2012-11-07 盐城工学院 一种新型脱汞催化剂
CN102764655B (zh) * 2011-12-23 2015-03-04 盐城工学院 一种脱汞催化剂
CN104582834A (zh) * 2012-02-06 2015-04-29 环球油品公司 用于汞脱除的保护吸附剂及其制备和使用方法
CN105148913A (zh) * 2015-10-08 2015-12-16 宁波海越新材料有限公司 一种用于仲丁醇制备甲乙酮的催化剂及其制备方法
CN108249955A (zh) * 2018-04-02 2018-07-06 中科京投环境科技江苏有限公司 一种脱除废、污水中汞的复合陶瓷材料及制备方法
CN108249955B (zh) * 2018-04-02 2020-12-29 中科京投环境科技江苏有限公司 一种脱除废、污水中汞的复合陶瓷材料的制备方法
CN115698231A (zh) * 2020-05-29 2023-02-03 埃克森美孚化学专利公司 含汞进料的烃热解

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Publication number Publication date
JP5455939B2 (ja) 2014-03-26
KR20100133394A (ko) 2010-12-21
EP2265695A1 (de) 2010-12-29
US20110005975A1 (en) 2011-01-13
WO2009112440A1 (de) 2009-09-17
JP2011513565A (ja) 2011-04-28

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Application publication date: 20110209