CN101925407B - 制备水性胶体贵金属悬液的方法 - Google Patents

制备水性胶体贵金属悬液的方法 Download PDF

Info

Publication number
CN101925407B
CN101925407B CN2009801026646A CN200980102664A CN101925407B CN 101925407 B CN101925407 B CN 101925407B CN 2009801026646 A CN2009801026646 A CN 2009801026646A CN 200980102664 A CN200980102664 A CN 200980102664A CN 101925407 B CN101925407 B CN 101925407B
Authority
CN
China
Prior art keywords
noble metal
suspension
catalyst
quaternary ammonium
salt
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN2009801026646A
Other languages
English (en)
Chinese (zh)
Other versions
CN101925407A (zh
Inventor
彼得·特奥多鲁斯·威特尔
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF Catalysts LLC
Original Assignee
BASF Catalysts LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF Catalysts LLC filed Critical BASF Catalysts LLC
Publication of CN101925407A publication Critical patent/CN101925407A/zh
Application granted granted Critical
Publication of CN101925407B publication Critical patent/CN101925407B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/16—Making metallic powder or suspensions thereof using chemical processes
    • B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
    • B22F9/24—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from liquid metal compounds, e.g. solutions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B01J23/44—Palladium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/20—Catalysts, in general, characterised by their form or physical properties characterised by their non-solid state
    • B01J35/23—Catalysts, in general, characterised by their form or physical properties characterised by their non-solid state in a colloidal state
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/40—Catalysts, in general, characterised by their form or physical properties characterised by dimensions, e.g. grain size
    • B01J35/45—Nanoparticles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0203—Impregnation the impregnation liquid containing organic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0211—Impregnation using a colloidal suspension
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/05—Metallic powder characterised by the size or surface area of the particles
    • B22F1/054—Nanosized particles
    • B22F1/0545—Dispersions or suspensions of nanosized particles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/17—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrogenation of carbon-to-carbon double or triple bonds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/18—Carbon
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/09—Geometrical isomers

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Nanotechnology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Composite Materials (AREA)
  • Physics & Mathematics (AREA)
  • Inorganic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)
  • Colloid Chemistry (AREA)
  • Manufacture And Refinement Of Metals (AREA)
CN2009801026646A 2008-01-28 2009-01-27 制备水性胶体贵金属悬液的方法 Active CN101925407B (zh)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
EP081507261 2008-01-28
EP20080150726 EP2082805A1 (en) 2008-01-28 2008-01-28 Process for the preparation of an aqueous colloidal precious metal suspension
EP08150726.1 2008-01-28
PCT/NL2009/050039 WO2009096783A1 (en) 2008-01-28 2009-01-27 Process for the preparation of an aqueous colloidal precious metal suspension

Publications (2)

Publication Number Publication Date
CN101925407A CN101925407A (zh) 2010-12-22
CN101925407B true CN101925407B (zh) 2013-10-23

Family

ID=39473834

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2009801026646A Active CN101925407B (zh) 2008-01-28 2009-01-27 制备水性胶体贵金属悬液的方法

Country Status (10)

Country Link
US (1) US8822725B2 (https=)
EP (2) EP2082805A1 (https=)
JP (2) JP5791901B2 (https=)
KR (1) KR20100123702A (https=)
CN (1) CN101925407B (https=)
BR (1) BRPI0907090A2 (https=)
CA (1) CA2712482A1 (https=)
MX (1) MX2010007883A (https=)
RU (1) RU2491988C2 (https=)
WO (1) WO2009096783A1 (https=)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2082805A1 (en) * 2008-01-28 2009-07-29 Basf Se Process for the preparation of an aqueous colloidal precious metal suspension
PL3063275T3 (pl) 2013-10-31 2020-03-31 Resolve Therapeutics, Llc Terapeutyczne fuzje nukleaza-albumina i sposoby
UA111104C2 (uk) 2014-07-08 2016-03-25 ТОВАРИСТВО З ОБМЕЖЕНОЮ ВІДПОВІДАЛЬНІСТЮ "НаноМедТраст" Біосумісний колоїдний розчин наночасток золота в неводному полярному розчиннику та спосіб його одержання
CA2975108A1 (en) * 2015-01-29 2016-08-04 Basf Corporation Platinum group metal (pgm) catalysts for automotive emissions treatment
EP3271072B1 (en) * 2015-03-20 2022-05-11 BASF Corporation Enhanced dispersion of edge-coated precious metal catalysts
US10258967B2 (en) 2015-03-20 2019-04-16 Basf Corporation PT and/or PD egg-shell catalyst and use thereof
CN105932306A (zh) * 2016-05-26 2016-09-07 昆明理工大学 利用光化学法还原MnPd制备碳纳米管负载金属纳米粒子催化剂的方法
CN109499566B (zh) * 2018-06-11 2020-06-09 太原氦舶新材料有限责任公司 一种贵金属载体催化剂及其制备方法和应用
KR20210116500A (ko) * 2019-01-17 2021-09-27 쉘 인터내셔날 리써취 마트샤피지 비.브이. 이종금속 나노입자계 촉매, 선택적 수소화에서의 이의 사용 및 촉매의 제조 방법
MY208300A (en) * 2019-05-27 2025-04-30 Dsm Ip Assets Bv Selective hydrogenation of alkynes to alkenes in the presence of a phosphorus compound and an organic sulphur compound
EP3906998A1 (en) * 2020-05-05 2021-11-10 BASF Corporation Supported transition metal nanoparticle catalyst and use thereof as a hydrogenation catalyst
CN115609001B (zh) * 2022-07-15 2023-10-10 西北工业大学 一种以炔类化合物制备功能化金纳米颗粒的方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1996017685A1 (en) * 1994-12-08 1996-06-13 Studiengesellschaft Kohle Mbh Process for producing tenside-stabilized colloids of mono- and bimetals of the group viii and ib of the periodic system in the form of precursors for catalysts which are isolable and water soluble at high concentration
US20070151631A1 (en) * 2004-03-25 2007-07-05 Fernandez Camacho M Asuncion Magnetic nanoparticles of noble metals

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
HU177860B (en) * 1979-05-22 1982-01-28 Mta Koezponti Hivatala Method for producing carrier metal catalyzers
DE4203489A1 (de) * 1992-02-07 1993-08-12 Henkel Kgaa Verfahren zur herstellung niedrigviskoser waessriger esterquat-konzentrate
DE69510477T2 (de) * 1994-03-14 2000-03-16 Studiengesellschaft Kohle Mbh Verfahren zur Herstellung von hoch verstreuten Metall-Kolloiden und von auf einem Substrat gebundenen Metall-Clusters durch elektrochemische Reduktion von Metallsalzen
DE19502580A1 (de) * 1995-01-27 1996-08-01 Basf Ag Verfahren zur Herstellung eines Hydrierungskatalysators
RU2115474C1 (ru) * 1997-02-20 1998-07-20 Институт химии твердого тела и переработки минерального сырья СО РАН Способ получения высокодисперсных катализаторов металл-носитель
DE19803891A1 (de) * 1998-01-31 1999-08-05 Bayer Ag Wäßrige Edelmetallkolloide und ihre Verwendung
FR2803224B1 (fr) * 1999-12-30 2002-09-27 Rhodia Chimie Sa Dispersion colloidale aqueuse a base d'au moins un compose d'un metal et d'un complexant, procede de preparation et utilisation
DE10037071A1 (de) * 2000-07-29 2002-02-21 Omg Ag & Co Kg Edelmetall-Nanopartikel, Verfahren zu ihrer Herstellung und Verwendung
RU2238140C2 (ru) * 2001-07-17 2004-10-20 Крыжановский Андрей Викторович Способ получения коллоидных растворов металлов
JP4678244B2 (ja) * 2005-06-10 2011-04-27 信越化学工業株式会社 燃料電池用触媒及びダイレクトメタノール型燃料電池
EP2082805A1 (en) * 2008-01-28 2009-07-29 Basf Se Process for the preparation of an aqueous colloidal precious metal suspension

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1996017685A1 (en) * 1994-12-08 1996-06-13 Studiengesellschaft Kohle Mbh Process for producing tenside-stabilized colloids of mono- and bimetals of the group viii and ib of the periodic system in the form of precursors for catalysts which are isolable and water soluble at high concentration
US20070151631A1 (en) * 2004-03-25 2007-07-05 Fernandez Camacho M Asuncion Magnetic nanoparticles of noble metals

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Novel one-step synthesis of amine-stabilized aqueous colloidal gold nanoparticles;M.Aslam等;《Journal of materials chemistry》;20040519;第14卷;1795-1797 *

Also Published As

Publication number Publication date
EP2249965A1 (en) 2010-11-17
JP2011510803A (ja) 2011-04-07
US8822725B2 (en) 2014-09-02
KR20100123702A (ko) 2010-11-24
CA2712482A1 (en) 2009-08-06
CN101925407A (zh) 2010-12-22
MX2010007883A (es) 2010-08-10
BRPI0907090A2 (pt) 2015-07-14
EP2082805A1 (en) 2009-07-29
JP2015227504A (ja) 2015-12-17
EP2249965B1 (en) 2017-08-02
JP5791901B2 (ja) 2015-10-07
RU2010136285A (ru) 2012-03-10
US20110015451A1 (en) 2011-01-20
RU2491988C2 (ru) 2013-09-10
WO2009096783A1 (en) 2009-08-06

Similar Documents

Publication Publication Date Title
CN101925407B (zh) 制备水性胶体贵金属悬液的方法
US9433932B2 (en) Hydrogenation catalyst and method of manufacturing the same
WO2008043060A2 (en) Highly dispersed nickel hydrogenation catalysts and methods for making the same
CN103657643B (zh) 一种制备纳米钯金属催化剂的方法
US7396795B2 (en) Low temperature preparation of supported nanoparticle catalysts having increased dispersion
JP2018531148A (ja) ルテニウム／鉄／炭素担体触媒を生成する方法
JP2018531148A6 (ja) ルテニウム／鉄／炭素担体触媒を生成する方法
JP7371102B2 (ja) 炭素ベースの貴金属－遷移金属複合触媒及びこれの製造方法
CN114849694A (zh) 一种基于金属负载氧化钨氢化硝基芳烃的催化剂及其制备方法和应用
CN103819295B (zh) 一种催化剂在芳香硝基化合物选择性加氢反应中的应用
CN113522296A (zh) CO加氢制乙醇CuZn催化剂及其制备方法和应用
JP4605334B2 (ja) 触媒製造法
CN105457631A (zh) 一种用于草酸酯气相加氢制备乙醇酸酯的催化剂和制备方法
CN114618491A (zh) 铜基催化剂的制备方法及铜基催化剂催化加氢制备烷醇的方法
CN114632511A (zh) 一种用于苯甲酸类化合物加氢反应的催化剂及其制备方法
WO2009122149A1 (en) Method for the preparation of supported catalyst using noble metal nanoparticles and catalyst so obtained
CN105148922A (zh) NiB非晶态合金催化剂及其制备方法
CN106512993B (zh) 钯-钌双金属纳米催化剂制备及加氢应用
JP2008503332A (ja) 金属酸化物ゾル
CN109400633B (zh) 金纳米团簇及其高产率制备方法
JP2011038158A (ja) 金属微粒子およびその製造方法
CN101856627B (zh) 间杯芳烃包合纳米镍催化剂及其制备
JP5197308B2 (ja) 多価アルコールの水素化分解物の製造方法
CN105601962A (zh) 一种内部交联胶束稳定的金属纳米粒子及其制备方法和在催化中的应用
CN115532290B (zh) 一种特定晶面选择性氢化催化剂及其制备方法和应用

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant