JP5791901B2 - 水性コロイド状貴金属懸濁物の製造方法 - Google Patents

水性コロイド状貴金属懸濁物の製造方法 Download PDF

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Publication number
JP5791901B2
JP5791901B2 JP2010544252A JP2010544252A JP5791901B2 JP 5791901 B2 JP5791901 B2 JP 5791901B2 JP 2010544252 A JP2010544252 A JP 2010544252A JP 2010544252 A JP2010544252 A JP 2010544252A JP 5791901 B2 JP5791901 B2 JP 5791901B2
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Japan
Prior art keywords
noble metal
catalyst
quaternary ammonium
producing
suspension
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Japanese (ja)
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JP2011510803A (ja
JP2011510803A5 (https=
Inventor
テオドルス ウィッテ，ペテル
テオドルス ウィッテ，ペテル
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BASF Corp
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BASF Corp
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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/16—Making metallic powder or suspensions thereof using chemical processes
    • B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
    • B22F9/24—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from liquid metal compounds, e.g. solutions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B01J23/44—Palladium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/20—Catalysts, in general, characterised by their form or physical properties characterised by their non-solid state
    • B01J35/23—Catalysts, in general, characterised by their form or physical properties characterised by their non-solid state in a colloidal state
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/40—Catalysts, in general, characterised by their form or physical properties characterised by dimensions, e.g. grain size
    • B01J35/45—Nanoparticles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0203—Impregnation the impregnation liquid containing organic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0211—Impregnation using a colloidal suspension
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/05—Metallic powder characterised by the size or surface area of the particles
    • B22F1/054—Nanosized particles
    • B22F1/0545—Dispersions or suspensions of nanosized particles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/17—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrogenation of carbon-to-carbon double or triple bonds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/18—Carbon
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/09—Geometrical isomers

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Nanotechnology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Composite Materials (AREA)
  • Physics & Mathematics (AREA)
  • Inorganic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)
  • Colloid Chemistry (AREA)
  • Manufacture And Refinement Of Metals (AREA)
JP2010544252A 2008-01-28 2009-01-27 水性コロイド状貴金属懸濁物の製造方法 Active JP5791901B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP20080150726 EP2082805A1 (en) 2008-01-28 2008-01-28 Process for the preparation of an aqueous colloidal precious metal suspension
EP08150726.1 2008-01-28
PCT/NL2009/050039 WO2009096783A1 (en) 2008-01-28 2009-01-27 Process for the preparation of an aqueous colloidal precious metal suspension

Related Child Applications (1)

Application Number Title Priority Date Filing Date
JP2015096377A Division JP2015227504A (ja) 2008-01-28 2015-05-11 水性コロイド状貴金属懸濁物の製造方法

Publications (3)

Publication Number Publication Date
JP2011510803A JP2011510803A (ja) 2011-04-07
JP2011510803A5 JP2011510803A5 (https=) 2012-03-15
JP5791901B2 true JP5791901B2 (ja) 2015-10-07

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JP2010544252A Active JP5791901B2 (ja) 2008-01-28 2009-01-27 水性コロイド状貴金属懸濁物の製造方法
JP2015096377A Pending JP2015227504A (ja) 2008-01-28 2015-05-11 水性コロイド状貴金属懸濁物の製造方法

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JP2015096377A Pending JP2015227504A (ja) 2008-01-28 2015-05-11 水性コロイド状貴金属懸濁物の製造方法

Country Status (10)

Country Link
US (1) US8822725B2 (https=)
EP (2) EP2082805A1 (https=)
JP (2) JP5791901B2 (https=)
KR (1) KR20100123702A (https=)
CN (1) CN101925407B (https=)
BR (1) BRPI0907090A2 (https=)
CA (1) CA2712482A1 (https=)
MX (1) MX2010007883A (https=)
RU (1) RU2491988C2 (https=)
WO (1) WO2009096783A1 (https=)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2015227504A (ja) * 2008-01-28 2015-12-17 ビーエーエスエフ コーポレーション 水性コロイド状貴金属懸濁物の製造方法

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PL3063275T3 (pl) 2013-10-31 2020-03-31 Resolve Therapeutics, Llc Terapeutyczne fuzje nukleaza-albumina i sposoby
UA111104C2 (uk) 2014-07-08 2016-03-25 ТОВАРИСТВО З ОБМЕЖЕНОЮ ВІДПОВІДАЛЬНІСТЮ "НаноМедТраст" Біосумісний колоїдний розчин наночасток золота в неводному полярному розчиннику та спосіб його одержання
CA2975108A1 (en) * 2015-01-29 2016-08-04 Basf Corporation Platinum group metal (pgm) catalysts for automotive emissions treatment
EP3271072B1 (en) * 2015-03-20 2022-05-11 BASF Corporation Enhanced dispersion of edge-coated precious metal catalysts
US10258967B2 (en) 2015-03-20 2019-04-16 Basf Corporation PT and/or PD egg-shell catalyst and use thereof
CN105932306A (zh) * 2016-05-26 2016-09-07 昆明理工大学 利用光化学法还原MnPd制备碳纳米管负载金属纳米粒子催化剂的方法
CN109499566B (zh) * 2018-06-11 2020-06-09 太原氦舶新材料有限责任公司 一种贵金属载体催化剂及其制备方法和应用
KR20210116500A (ko) * 2019-01-17 2021-09-27 쉘 인터내셔날 리써취 마트샤피지 비.브이. 이종금속 나노입자계 촉매, 선택적 수소화에서의 이의 사용 및 촉매의 제조 방법
MY208300A (en) * 2019-05-27 2025-04-30 Dsm Ip Assets Bv Selective hydrogenation of alkynes to alkenes in the presence of a phosphorus compound and an organic sulphur compound
EP3906998A1 (en) * 2020-05-05 2021-11-10 BASF Corporation Supported transition metal nanoparticle catalyst and use thereof as a hydrogenation catalyst
CN115609001B (zh) * 2022-07-15 2023-10-10 西北工业大学 一种以炔类化合物制备功能化金纳米颗粒的方法

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
HU177860B (en) * 1979-05-22 1982-01-28 Mta Koezponti Hivatala Method for producing carrier metal catalyzers
DE4203489A1 (de) * 1992-02-07 1993-08-12 Henkel Kgaa Verfahren zur herstellung niedrigviskoser waessriger esterquat-konzentrate
DE69510477T2 (de) * 1994-03-14 2000-03-16 Studiengesellschaft Kohle Mbh Verfahren zur Herstellung von hoch verstreuten Metall-Kolloiden und von auf einem Substrat gebundenen Metall-Clusters durch elektrochemische Reduktion von Metallsalzen
DE4443705A1 (de) * 1994-12-08 1996-06-13 Studiengesellschaft Kohle Mbh Verfahren zur Herstellung von tensidstabilisierten Mono- und Bimetallkolloiden der Gruppe VIII und Ib des Periodensystems als isolierbare und in hoher Konzentration wasserlösliche Precursor für Katalysatoren
DE19502580A1 (de) * 1995-01-27 1996-08-01 Basf Ag Verfahren zur Herstellung eines Hydrierungskatalysators
RU2115474C1 (ru) * 1997-02-20 1998-07-20 Институт химии твердого тела и переработки минерального сырья СО РАН Способ получения высокодисперсных катализаторов металл-носитель
DE19803891A1 (de) * 1998-01-31 1999-08-05 Bayer Ag Wäßrige Edelmetallkolloide und ihre Verwendung
FR2803224B1 (fr) * 1999-12-30 2002-09-27 Rhodia Chimie Sa Dispersion colloidale aqueuse a base d'au moins un compose d'un metal et d'un complexant, procede de preparation et utilisation
DE10037071A1 (de) * 2000-07-29 2002-02-21 Omg Ag & Co Kg Edelmetall-Nanopartikel, Verfahren zu ihrer Herstellung und Verwendung
RU2238140C2 (ru) * 2001-07-17 2004-10-20 Крыжановский Андрей Викторович Способ получения коллоидных растворов металлов
ES2242528B1 (es) * 2004-03-25 2006-12-01 Consejo Sup. Investig. Cientificas Nanoparticulas magneticas de metales nobles.
JP4678244B2 (ja) * 2005-06-10 2011-04-27 信越化学工業株式会社 燃料電池用触媒及びダイレクトメタノール型燃料電池
EP2082805A1 (en) * 2008-01-28 2009-07-29 Basf Se Process for the preparation of an aqueous colloidal precious metal suspension

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2015227504A (ja) * 2008-01-28 2015-12-17 ビーエーエスエフ コーポレーション 水性コロイド状貴金属懸濁物の製造方法

Also Published As

Publication number Publication date
EP2249965A1 (en) 2010-11-17
JP2011510803A (ja) 2011-04-07
US8822725B2 (en) 2014-09-02
KR20100123702A (ko) 2010-11-24
CA2712482A1 (en) 2009-08-06
CN101925407A (zh) 2010-12-22
MX2010007883A (es) 2010-08-10
BRPI0907090A2 (pt) 2015-07-14
EP2082805A1 (en) 2009-07-29
JP2015227504A (ja) 2015-12-17
EP2249965B1 (en) 2017-08-02
RU2010136285A (ru) 2012-03-10
CN101925407B (zh) 2013-10-23
US20110015451A1 (en) 2011-01-20
RU2491988C2 (ru) 2013-09-10
WO2009096783A1 (en) 2009-08-06

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