CN101878954A - Konjac humectant and application thereof in cigarettes - Google Patents
Konjac humectant and application thereof in cigarettes Download PDFInfo
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- CN101878954A CN101878954A CN2009100619909A CN200910061990A CN101878954A CN 101878954 A CN101878954 A CN 101878954A CN 2009100619909 A CN2009100619909 A CN 2009100619909A CN 200910061990 A CN200910061990 A CN 200910061990A CN 101878954 A CN101878954 A CN 101878954A
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- humectant
- konjac
- konjac humectant
- filter residue
- filter
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- 229920002752 Konjac Polymers 0.000 title claims abstract description 100
- 239000003906 humectant Substances 0.000 title claims abstract description 96
- 235000001206 Amorphophallus rivieri Nutrition 0.000 title claims abstract description 79
- 239000000252 konjac Substances 0.000 title claims abstract description 77
- 235000010485 konjac Nutrition 0.000 title claims abstract description 77
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 30
- 241001312219 Amorphophallus konjac Species 0.000 title claims description 70
- 241000208125 Nicotiana Species 0.000 claims abstract description 45
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 45
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 40
- 235000019441 ethanol Nutrition 0.000 claims abstract description 13
- 239000002245 particle Substances 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000012153 distilled water Substances 0.000 claims abstract description 10
- 238000000034 method Methods 0.000 claims abstract description 8
- 239000004677 Nylon Substances 0.000 claims description 21
- 229920001778 nylon Polymers 0.000 claims description 21
- 235000013312 flour Nutrition 0.000 claims description 17
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 12
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 12
- 238000000605 extraction Methods 0.000 claims description 8
- 230000008961 swelling Effects 0.000 claims description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 6
- 238000010828 elution Methods 0.000 claims description 5
- 241000196324 Embryophyta Species 0.000 claims description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 4
- 238000007654 immersion Methods 0.000 claims description 4
- 239000002253 acid Substances 0.000 claims description 3
- 238000013019 agitation Methods 0.000 claims description 2
- 238000012840 feeding operation Methods 0.000 claims description 2
- 238000002386 leaching Methods 0.000 claims description 2
- 239000000463 material Substances 0.000 claims description 2
- 238000003756 stirring Methods 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 19
- 238000004519 manufacturing process Methods 0.000 abstract description 6
- 238000001035 drying Methods 0.000 abstract description 2
- 230000001953 sensory effect Effects 0.000 abstract description 2
- 244000247812 Amorphophallus rivieri Species 0.000 abstract 9
- 238000002791 soaking Methods 0.000 abstract 2
- 238000000227 grinding Methods 0.000 abstract 1
- 239000000843 powder Substances 0.000 abstract 1
- 210000000697 sensory organ Anatomy 0.000 description 14
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 10
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 6
- 239000003546 flue gas Substances 0.000 description 6
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 description 6
- 238000012360 testing method Methods 0.000 description 6
- 235000011187 glycerol Nutrition 0.000 description 5
- 238000001291 vacuum drying Methods 0.000 description 5
- 229920001661 Chitosan Polymers 0.000 description 4
- FYGDTMLNYKFZSV-DZOUCCHMSA-N alpha-D-Glcp-(1->4)-alpha-D-Glcp-(1->4)-D-Glcp Chemical class O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)O[C@H](O[C@@H]2[C@H](OC(O)[C@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O FYGDTMLNYKFZSV-DZOUCCHMSA-N 0.000 description 4
- 238000012545 processing Methods 0.000 description 3
- 239000000779 smoke Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- STNJBCKSHOAVAJ-UHFFFAOYSA-N Methacrolein Chemical compound CC(=C)C=O STNJBCKSHOAVAJ-UHFFFAOYSA-N 0.000 description 2
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000009472 formulation Methods 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000000811 xylitol Substances 0.000 description 2
- 235000010447 xylitol Nutrition 0.000 description 2
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 description 2
- 229960002675 xylitol Drugs 0.000 description 2
- LUEWUZLMQUOBSB-FSKGGBMCSA-N (2s,3s,4s,5s,6r)-2-[(2r,3s,4r,5r,6s)-6-[(2r,3s,4r,5s,6s)-4,5-dihydroxy-2-(hydroxymethyl)-6-[(2r,4r,5s,6r)-4,5,6-trihydroxy-2-(hydroxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-4,5-dihydroxy-2-(hydroxymethyl)oxan-3-yl]oxy-6-(hydroxymethyl)oxane-3,4,5-triol Chemical compound O[C@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@@H](O[C@@H]2[C@H](O[C@@H](OC3[C@H](O[C@@H](O)[C@@H](O)[C@H]3O)CO)[C@@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O LUEWUZLMQUOBSB-FSKGGBMCSA-N 0.000 description 1
- 229920002581 Glucomannan Polymers 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 230000002860 competitive effect Effects 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 229940046240 glucomannan Drugs 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000009738 saturating Methods 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 235000019615 sensations Nutrition 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
Landscapes
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses a konjac humectant and an application thereof in cigarettes, belonging to the technical field of cigarettes. The konjac humectant is prepared by the following steps: adding 20-50% ethanol in konjac powder, soaking and extracting; (2) soaking and extracting filter residue for 2-6 times; (3) eluting by utilizing 95% ethanol or absolute ethyl alcohol; (4) drying at the temperature of 60-80 DEG C; and (5) grinding until the particles can pass through a 60-80 meshed sieve. The konjac humectant is dissolved into konjac humectant solution by utilizing distilled water the weight of which is 1000-10000 times of the konjac humectant, and then the konjac humectant solution is sprayed on tobacco leaves evenly based on the mass ratio of the konjac humectant solution to the tobacco leaves of (0.5-1.5):100 in the tobacco leaf charging process. The konjac humectant in the invention can greatly lower the tobacco production cost, improve physical and sensory moisture-keeping effects, and has simple and feasible method, thereby having wide application prospect in tobacco industry.
Description
Technical field
The invention belongs to technical field of cigarettes, a kind ofly specifically can reduce the production of cigarettes cost, improve the humectation of tobacco physics and the natural humectant for smoke of sense organ humectation effect and the application in cigarette thereof simultaneously.
Background technology
The humectant that uses in the cigarette industry can only be kept the suitable moisture content of cigarette at present, and these humectant roles are to preserve moisture, and are not humectation.Along with the further investigation of cigarette industry to the humectation technology, industry also has more and more deep understanding to the effect that humectant should play: the humectation of cigarette not only will comprise the physics humectation, also should comprise the sense organ humectation.The physics humectation is promptly preserved moisture, and is meant the moisture of keeping tobacco leaf, the moisture that purpose is to improve the anti-processing characteristics of tobacco and keeps flue gas; The sense organ humectation then is directly at sensory issues, and dry sensation, excitant, pleasant impression etc. are improved.Therefore the exploitation of novel humectant should be started with from physics humectation and sense organ humectation two aspects.
Mainly adopt humectants such as glycerine, propane diols, xylitol, sorbierite at present in China's cigarette industry.The humectation better performances of glycerine and propane diols wherein, but the methacrylaldehyde that the glycerine combustion decomposition produces can make that flue gas is jealous to degenerate, and glycerine and propane diols cost an arm and a leg.Though the price of xylitol, sorbierite is low, its humectation performance is good not as glycerine and propane diols, and long storage time has precipitation, easily solidifies when temperature is low, is not easy to use aborning.Along with cigarette industry in recent years to the continuous research of novel humectant, obtained certain achievement, wherein use extensive relatively with two kinds of humectants of the pure and mild chitosan derivatives of malto-oligosaccharide, but malto-oligosaccharide alcohol humectation effect is poor slightly, and chitosan derivatives has certain influence because of containing more nitrogen element to cigarette flavor and pleasant impression.
Summary of the invention
Above-mentioned deficiency at prior art, the technical problem to be solved in the present invention provides a kind of natural cigarette konjac humectant, and be applied in the cigarette, can improve the anti-processing characteristics of pipe tobacco, and can improve mouthfeel, flue gas drying sense, excitant and pleasant impression etc., and has outstanding advantage with low cost.
Konjac humectant of the present invention is made through following steps after the natural plants konjaku is worn into konjaku flour:
(1) 20%～50% ethanol that adds 1～3 times of himself weight in konjaku flour soaks extraction, in above-mentioned soak, add acid solution and regulate pH to 4.0-5.0, it was placed 8-16 hour, treat the abundant swelling of konjaku flour after, filter with 100 orders-140 order nylon net filter device, keep filter residue; Mainly be removal of impurities in this step, in regulating pH and being on the one hand and alkaline components, also play modifying function konjaku.
(2) 20%～50% ethanol that adds 1～3 times of himself weight in step (1) the gained filter residue is soaked extraction, soaked extraction time 2-6 hour; After more than immersion extraction operation repeats 2-6 time, filter the reservation filter residue with 100 orders-140 order nylon net filter device;
(3) with adding 0.5-2 95% ethanol or absolute ethyl alcohol doubly in the filter residue of step (2) filter residue was carried out wash-out 1-3 hour, filter the reservation filter residue with 100 orders-140 order nylon net filter device;
(4) with the filter residue of step (3) under 60-80 ℃ of temperature dry 8-12 hour, obtain the konjac humectant head product;
(5) the konjac humectant head product is crushed to passes through the 60-80 mesh sieve, obtain amorphophallus rivieri particles humectant product, pack with waterproof material.
Carry out gentle agitation in the immersion leaching process of above-mentioned steps (1); Constantly stir in the elution process of step (3).What regulate pH is citric acid or acetic acid or hydrochloric acid or sulfuric acid.
The application of konjac humectant in cigarette: is konjac humectant solution with konjac humectant with its weight 1000-10000 dissolved in distilled water doubly, in the tobacco feeding operation konjac humectant solution evenly is sprayed in the tobacco leaf, the mass ratio of konjac humectant solution and tobacco leaf is (0.5～1.5): 100.
Konjac humectant of the present invention belongs to the natural plants humectant, and konjaku has abundant raw material sources in China, and super quality and competitive price, and the main component Glucomannan of konjaku flour has superpower water absorbing capacity and performance of keeping humidity.The konjac humectant of extracted form natural plant is applied in the tobacco, and physics humectation and sense organ humectation effect are all good, can coordinate the few side effects of generation preferably mutually with tobacco aroma, flue gas; And because the amount that adds is minimum, therefore with low cost.
The specific embodiment
Below in conjunction with embodiment the relevant technical problem of the present invention is described in further detail.
The different adding proportion of tobacco humectant has different influences to the physics of cigarette with sense organ humectation effect, the applicant has carried out experimental study to konjac humectant different adding proportions in cigarette, by smokeing panel test, determine suitable amounts scope and the optimum amount of konjac humectant in cigarette.At first, with the dissolved in distilled water of konjac humectant with 5000 times, in reinforced mode konjac humectant solution evenly is sprayed in the pipe tobacco, the mass ratio of konjac humectant solution and pipe tobacco is 0.1～2: 100.Evaluation result sees Table 1:
Table 1 konjac humectant applies ratio and sense organ humectation effect
Annotate: participate in totally 14 judging panels that smoke panel test: wherein two is national judging panel, seven provincial judging panels, five level of factory judging panels.
According to smoking result, konjac humectant to soft flue gas, increase smooth and easy sense, improve the mouthfeel aspect apparent in view effect is arranged, behind the consumption to 2%, fragrance is oppressive to some extent.Therefore can think and be fit to consumption 0.5-1.5%, optimum amount 0.8-1.2%.
In the above-mentioned test, the applicant is earlier with the dissolved in distilled water of konjac humectant with 5000 times, and be (0.1～2) with mass ratio again: 100 ratio makes an addition in the pipe tobacco.So, only added the konjac humectant of minute quantity in the pipe tobacco, just reached the effect of sense organ humectation preferably, the cost that uses konjac humectant of the present invention can reduce production of cigarettes greatly is described.
The humectant that the applicant comparatively uses always several tobacco business such as konjac humectant and propane diols, malto-oligosaccharide alcohol and chitosan derivatives has carried out the contrast test of physics humectation effect, and test method is as follows:
The conventional amount used (promptly being optimum amount separately) that above-mentioned four kinds of humectant solution are pressed separately makes an addition in the pipe tobacco of identical tobacco leaf formulation, humectant of the present invention makes an addition in the pipe tobacco of identical tobacco leaf formulation by optimum amount, balance 48h under 22 ℃ of humidity 40% conditions of temperature, measure moisture standards method " YC/T28.8-1996 " to its mensuration of carrying out moisture content according to tobacco business then, measurement result sees Table 2:
The comparison of table 2 konjac humectant and other humectant physical package profit effect
By table 2 as can be known: behind balance 48h under 22 ℃ of humidity 40% conditions of temperature, the average moisture content that adds the pipe tobacco of konjac humectant will can show that konjac humectant is applied to have better physical humectation effect in the tobacco humectation apparently higher than the average moisture content of the pipe tobacco that adds other three kinds of humectants.Can improve the anti-processing characteristics and the ability of keeping the moisture of flue gas of tobacco.
Konjac humectant provided by the present invention can be by a relatively large margin the cost of reduction production of cigarettes, can improve simultaneously the physics humectation and the sense organ humectation effect of cigarette again, and its method that is applied to cigarette industry production is simple, therefore has a wide range of applications at tobacco business.
Below embodiments of the invention are described, but the scope of the invention is not limited to these embodiment.
Embodiment 1:
Get konjaku flour 100 grams, add 200 milliliter of 25% ethanolic solution and carry out lixiviate, add acetic acid again and regulate pH value to 4.5, make the abundant swelling of konjaku flour 10 hours, filter with 100 order nylon net filter devices then, the gained filter residue adds 200 milliliter of 25% ethanolic solution and carries out lixiviate 3 times, filters with 100 order nylon net filter devices after the lixiviate again.In the gained filter residue, added 150 milliliter of 95% ethanol elution 1 hour, filter with 120 order nylon net filter devices then, filter residue was placed 60 ℃ of vacuum drying chambers dry 10 hours, promptly obtain the konjac humectant head product, the konjac humectant head product is pulverized and mistake 60 eye mesh screens, promptly obtain the konjac humectant finished particle.With the dissolved in distilled water of konjac humectant particle with 2000 times, the konjac humectant solution with gained evenly is sprayed in the tobacco leaf with 1% of quality of tobacco again.
Embodiment 2:
Get konjaku flour 100 grams, add 300 milliliter of 30% ethanolic solution and carry out lixiviate, add citric acid again and regulate pH value to 4.8, make the abundant swelling of konjaku flour 10 hours, filter with 120 order nylon net filter devices then, the gained filter residue adds 300 milliliter of 30% ethanolic solution and carries out lixiviate 2 times, filters with 120 order nylon net filter devices after the lixiviate again.In the gained filter residue, added 200 milliliter of 95% ethanol elution 1.5 hours, filter with 120 order nylon net filter devices then, filter residue was placed 70 ℃ of vacuum drying chambers dry 8 hours, promptly obtain the konjac humectant head product, the konjac humectant head product is pulverized and mistake 80 eye mesh screens, promptly obtain the konjac humectant finished particle.With the dissolved in distilled water of konjac humectant particle with 5000 times, the konjac humectant solution with gained evenly is sprayed in the tobacco leaf with 0.8% of quality of tobacco again.
Embodiment 3:
Get konjaku flour 200 grams, add 500 milliliter of 30% ethanolic solution and carry out lixiviate, add acetic acid again and regulate pH value to 4.8, make the abundant swelling of konjaku flour 12 hours, filter with 100 order nylon net filter devices then, the gained filter residue adds 500 milliliter of 30% ethanolic solution and carries out lixiviate 4 times, filters with 100 order nylon net filter devices after the lixiviate again.In the gained filter residue, added 400 milliliters of absolute ethyl alcohol wash-outs 2 hours, filter with 120 order nylon net filter devices then, filter residue was placed 80 ℃ of vacuum drying chambers dry 10 hours, promptly obtain the konjac humectant head product, the konjac humectant head product is pulverized and mistake 80 eye mesh screens, promptly obtain the konjac humectant finished particle.With the dissolved in distilled water of konjac humectant particle with 5000 times, the konjac humectant solution with gained evenly is sprayed in the tobacco leaf with 1.2% of quality of tobacco again.
Embodiment 4:
Get konjaku flour 100 grams, add 300 milliliter of 35% ethanolic solution and carry out lixiviate, add hydrochloric acid again and regulate pH value to 4.2, make the abundant swelling of konjaku flour 14 hours, filter with 120 order nylon net filter devices then, the gained filter residue adds 300 milliliter of 35% ethanolic solution and carries out lixiviate 5 times, filters with 120 order nylon net filter devices after the lixiviate again.In the gained filter residue, added 200 milliliters of absolute ethyl alcohol wash-outs 3 hours, filter with 140 order nylon net filter devices then, filter residue was placed 75 ℃ of vacuum drying chambers dry 12 hours, promptly obtain the konjac humectant head product, the konjac humectant head product is pulverized and mistake 80 eye mesh screens, promptly obtain the konjac humectant finished particle.With the dissolved in distilled water of konjac humectant particle with 8000 times, the konjac humectant solution with gained evenly is sprayed in the tobacco leaf with 1% of quality of tobacco again.
Embodiment 5:
Get konjaku flour 500 grams, add 1200 milliliter of 35% ethanolic solution and carry out lixiviate, add citric acid again and regulate pH value to 5.0, make the abundant swelling of konjaku flour 8 hours, filter with 100 order nylon net filter devices then, the gained filter residue adds 1200 milliliter of 35% ethanolic solution and carries out lixiviate 5 times, filters with 100 order nylon net filter devices after the lixiviate again.In the gained filter residue, added 800 milliliter of 95% ethanol elution 3 hours, filter with 120 order nylon net filter devices then, filter residue was placed 80 ℃ of vacuum drying chambers dry 8 hours, promptly obtain the konjac humectant head product, the konjac humectant head product is pulverized and mistake 60 eye mesh screens, promptly obtain the konjac humectant finished particle.With the dissolved in distilled water of konjac humectant particle with 3000 times, the konjac humectant solution with gained evenly is sprayed in the tobacco leaf with 0.8% of quality of tobacco again.
Konjac humectant provided by the present invention is applied to cigarette industry production has the effect of sense organ humectation preferably to cigarette, propane diols that the applicant mainly uses at tobacco business five kinds of embodiment provided by the present invention and prior art and the novel in recent years pure and mild chitosan derivatives humectant of malto-oligosaccharide carry out the contrast of sense organ humectation effect smokes panel test, and comparing result sees Table 3:
Table 3: the sense organ humectation effect contrast of konjac humectant cigarette and other humectant cigarette
Annotate: participate in totally 14 judging panels that smoke panel test: wherein two is national judging panel, seven provincial judging panels, five level of factory judging panels.
By table 3 as can be known: five embodiment of konjac humectant provided by the present invention have effect preferably to the sense organ humectation of cigarette, can effectively improve the saturating property sent out and the smooth and easy sense of fragrance, abirritate and raising pleasant impression comfort level, its sense organ humectation effect several main humectant existing than tobacco business improves.
Claims (5)
1. konjac humectant, it is characterized in that: described konjac humectant is made through following steps after wearing into konjaku flour by the natural plants konjaku:
(1) 20%～50% ethanol that adds 1～3 times of himself weight in konjaku flour soaks extraction, in above-mentioned soak, add acid solution and regulate pH to 4.0-5.0, it was placed 8-16 hour, treat the abundant swelling of konjaku flour after, filter with 100 orders-140 order nylon net filter device, keep filter residue;
(2) 20%～50% ethanol that adds 1～3 times of himself weight in step (1) the gained filter residue is soaked extraction, soaked extraction time 2-6 hour; After more than immersion extraction operation repeats 2-6 time, filter the reservation filter residue with 100 orders-140 order nylon net filter device;
(3) with adding 0.5-2 95% ethanol or absolute ethyl alcohol doubly in the filter residue of step (2) filter residue was carried out wash-out 1-3 hour, filter the reservation filter residue with 100 orders-140 order nylon net filter device;
(4) with the filter residue of step (3) under 60-80 ℃ of temperature dry 8-12 hour, obtain the konjac humectant head product;
(5) the konjac humectant head product is crushed to passes through the 60-80 mesh sieve, obtain amorphophallus rivieri particles humectant product, pack with waterproof material.
2. konjac humectant according to claim 1 is characterized in that: carry out gentle agitation in the immersion leaching process of step (1);
3. konjac humectant according to claim 1 is characterized in that: constantly stir in the elution process of step (3).
4. konjac humectant according to claim 1 is characterized in that: the acid solution in order to adjusting pH is citric acid or acetic acid or hydrochloric acid or sulfuric acid.
5. the application of konjac humectant in cigarette, it is characterized in that: is konjac humectant solution with konjac humectant with its weight 1000-10000 dissolved in distilled water doubly, in the tobacco feeding operation konjac humectant solution evenly is sprayed in the tobacco leaf, the mass ratio of konjac humectant solution and tobacco leaf is (0.5～1.5): 100.
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| CN 200910061990 CN101878954B (en) | 2009-05-05 | 2009-05-05 | Konjac humectant and application thereof in cigarettes |
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| CN 200910061990 CN101878954B (en) | 2009-05-05 | 2009-05-05 | Konjac humectant and application thereof in cigarettes |
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| CN101878954B CN101878954B (en) | 2012-12-26 |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102613696A (en) * | 2012-03-31 | 2012-08-01 | 广西中烟工业有限责任公司 | Application of konjac extract as tobacco humectant |
| CN102754916A (en) * | 2012-07-27 | 2012-10-31 | 红云红河烟草(集团)有限责任公司 | Xylo-oligosaccharide cigarette humectant and using method thereof |
| CN102823942A (en) * | 2012-09-20 | 2012-12-19 | 上海烟草集团有限责任公司 | Application of aqueous solution of salt serving as hydrous stem humectant |
| CN102839051A (en) * | 2012-08-27 | 2012-12-26 | 江苏中烟工业有限责任公司 | Cigarette sensory flavoring humectant and preparation method and application thereof |
| CN103126063A (en) * | 2011-11-23 | 2013-06-05 | 福建中烟工业有限责任公司 | Novel tobacco sense organ humectant and using method thereof in tobacco |
| CN108851199A (en) * | 2018-05-22 | 2018-11-23 | 湖北中烟工业有限责任公司 | A kind of preparation method of enzymolysis glucomannan and the compound humectant of medicinal fungus fermentation material |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003289842A (en) * | 2002-03-27 | 2003-10-14 | Hygen Enbio Tec Co Ltd | Tobacco leaf-processing method for reducing harmful component |
| CN101323816A (en) * | 2008-07-29 | 2008-12-17 | 红云烟草(集团)有限责任公司 | White tea essential oil, preparation and use thereof |
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2009
- 2009-05-05 CN CN 200910061990 patent/CN101878954B/en not_active Expired - Fee Related
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103126063A (en) * | 2011-11-23 | 2013-06-05 | 福建中烟工业有限责任公司 | Novel tobacco sense organ humectant and using method thereof in tobacco |
| CN102613696A (en) * | 2012-03-31 | 2012-08-01 | 广西中烟工业有限责任公司 | Application of konjac extract as tobacco humectant |
| CN102754916A (en) * | 2012-07-27 | 2012-10-31 | 红云红河烟草(集团)有限责任公司 | Xylo-oligosaccharide cigarette humectant and using method thereof |
| CN102839051A (en) * | 2012-08-27 | 2012-12-26 | 江苏中烟工业有限责任公司 | Cigarette sensory flavoring humectant and preparation method and application thereof |
| CN102823942A (en) * | 2012-09-20 | 2012-12-19 | 上海烟草集团有限责任公司 | Application of aqueous solution of salt serving as hydrous stem humectant |
| CN102823942B (en) * | 2012-09-20 | 2014-10-15 | 上海烟草集团有限责任公司 | Application of aqueous solution of salt serving as hydrous stem humectants, and method for keeping moisture of stem |
| CN108851199A (en) * | 2018-05-22 | 2018-11-23 | 湖北中烟工业有限责任公司 | A kind of preparation method of enzymolysis glucomannan and the compound humectant of medicinal fungus fermentation material |
| CN108851199B (en) * | 2018-05-22 | 2019-11-08 | 湖北中烟工业有限责任公司 | A kind of preparation method of enzymolysis glucomannan and the compound humectant of medicinal fungus fermentation material |
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