CN102697169B - Moisturizing and flavor-enhancing additive for cigarettes as well as preparation method and application thereof - Google Patents
Moisturizing and flavor-enhancing additive for cigarettes as well as preparation method and application thereof Download PDFInfo
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Abstract
The invention discloses a moisturizing and flavor-enhancing additive for cigarettes as well as a preparation method and application thereof, wherein the additive comprises traditional Chinese medicine extract compositions or compound traditional Chinese medicine extracts; and the traditional Chinese medicines comprise herba epimedii, eclipta, sweet almond, leonurus, dandelion and pummelo peel. The moisturizing and flavor-enhancing additive is prepared according to the following steps of: respectively extracting and refining the herba epimedii, the eclipta, the sweet almond, the leonurus, the dandelion and the pummelo peel with solvent, and concocting the moisturizing and flavor-enhancing additive according to the proportion of 1-8: 0.8-6: 0..5-4: 0.3-4: 0.3-5: 1, or extracting and refining to prepare the moisturizing and flavor-enhancing additive after mixing the herba epimedii, the eclipta, the sweet almond, the leonurus, the dandelion and the pummelo peel according to the proportion of 0.5-8: 0.5-6: 0.2-4: 0.3-4: 0.3-5: 1. The additive is added to tobacco shreds, tobacco stems and slices of cigarettes and the addition proportion is 0.002-1%wt. After the additive is added to the tobacco shreds, tobacco stems and slices of cigarettes, the moisture can be maintained under normal-temperature dry environment, so that favorable physical moisturizing function is provided.
Description
Technical field
The present invention relates to cigarette additive and preparation and application field thereof, especially relate to a kind of Chinese medical extract combination or Chinese medicinal compound extract of comprising, there is the cigarette additive and preparation method thereof and application of moist-keeping flavouring effect.
Background technology
Humectant can strengthen tobacco in referring to and put on tobacco in tobacco product process, tobacco product performance of keeping humidity, increases flexibility, reduces broken material.Humectant can improve the physical property of blade and pipe tobacco, increases cigarette product toughness, and elasticity and water retention property reduce process loss in process.In China's cigarette industry, mainly adopting the polyhydroxy substances such as glycerine, propane diols, sorbierite, xylitol is at present humectant, the soaking with maintenance pipe tobacco by the airborne moisture of these material absorbings, but the object of using this type of humectant is only to maintain the moisture content of pipe tobacco in process, improve the resistance to processability of pipe tobacco, effect is not ideal for finished cigarettes, to suck the improvement of comfort level.In addition this class humectant is affected greatly by ambient temperature and humidity, and glycerine and propane diols cost are higher, although sorbierite and xylitol cost are controlled, humectation effect is not as glycerine and propane diols.
China just starts to carry out the research and development of Chinese medicine class natural plants additive cigarette since the middle of last century.Between many decades, researcher in industry reduces cigarette at Chinese herb feed additive and is done a lot of work in harm field, the low harm tobacco that contains plant extracts as mono-kind of < < and preparation method thereof > > (application number: 201110181597.0, publication number: CN102349697A), < < cigarette harm reduction additive and preparation method > > (application number: 201110241463.3 thereof, publication number: CN102318896A) etc.In recent years, along with industry industrialized development is accelerated, moist area of southern China produces cigarette and sells and increase in northern Arid Area, and humectant research and development cause higher attention, and the research that adopts Chinese medicine class natural products to improve cigarette humid keeping performance should become study hotspot.
Summary of the invention
One of the object of the invention is to provide a kind of cigarette moist-keeping flavouring additive agent and preparation method thereof.
Another object of the present invention, is to provide the application of this cigarette moist-keeping flavouring additive agent.
According to one of object of the present invention, technical scheme of the present invention is as follows:
A kind of cigarette moist-keeping flavouring additive agent, comprise traditional Chinese medicine extraction compositions or compound Chinese medicine extract, it is characterized in that: described traditional Chinese medicine extraction compositions or compound Chinese medicine extract comprise barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis.
In described traditional Chinese medicine extraction compositions, the extract weight ratio of barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis is 1-8:0.8-6:0.5-4:0.3-4:0.3-5:1.
The part by weight of described compound Chinese medicine extract Raw medicine barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis is 0.5～8:0.5-6:0.2-4:0.3-4:0.3-5:1.
Described preparation method's preferred version one, carries out according to following steps:
Get barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis, after pulverizing, extract separately, add respectively 6-15 doubly to measure pure water, soak 2-48h, 1-3h is extracted in 65-100 ℃ of hot reflux, extracts altogether 3 times, merges No. 3 times extract, 60-80 ℃, under pressure 0.02-0.08Mpa condition, being concentrated into density is 1.12 ± 0.01 liquid extracts;
Subsequently, add 2 times of volume ethanol, standing 24-96h, filtering-depositing, 60-80 ℃, under pressure 0.02-0.08Mpa condition, being concentrated into density is 1.12 ± 0.01 liquid extracts;
The liquid extract of barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis is mixed by 1-8:0.8-6:0.5-4:0.3-4:0.3-5:1, filter and obtain moist-keeping flavouring additive agent.
As two of preferred version, described preparation method carries out according to following steps:
Get respectively barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis, after pulverizing, in 0.5-8:0.5-6:0.2-4:0.3-4:0.3-5:1 ratio, evenly mix, add 6-15 doubly to measure pure water, soak after 2-48h, 1-3h is extracted in 65-100 ℃ of hot reflux, extracts altogether 3 times, merges No. 3 times extract, 60-80 ℃, under pressure 0.02-0.08Mpa condition, being concentrated into density is 1.12 ± 0.01 liquid extracts;
Add 2 times of volume ethanol, standing 24-96h, filtering-depositing, 60-80 ℃, under pressure 0.02-0.08Mpa condition, being concentrated into density is 1.12 ± 0.01 liquid extracts, filters, and obtains moist-keeping flavouring additive agent.
For applying of large industry, the present invention also provides a kind of application of cigarette moist-keeping flavouring additive agent: get appropriate moist-keeping flavouring additive agent, be dissolved in certain volume distilled water, be evenly sprayed on cigarette shreds, stem, thin slice.The consumption of moist-keeping flavouring additive agent is pipe tobacco, stem, the 0.002-1%wt of flake weight.
One of beneficial effect of the present invention is: this additive makes an addition to cigarette shreds, stem, after thin slice, under air drying environment, there is good moisture holding capacity, can improve the moisture content of tobacco sample, can slow down scattering and disappearing of moisture, reduce the percentage of water loss of pipe tobacco, play the effect that maintains moisture in cut tobacco, there is good physics humectation effect.
This technology compared with prior art also has the following advantages: this additive not only has good physics humectation effect, can also effectively increase the perfume quantity of cigarette, improve fragrance matter and harmony, reduce assorted gas and excitant, increase sweet sense, make pleasant impression cleaner, comfortable, Integral lifting the interior quality of cigarette.And equipment is simple, extraction process is simple, and cost is controlled, and raw material is easy to get.
Accompanying drawing explanation
To making the present invention become in the description of embodiment, obviously and easily understand by reference to the accompanying drawings, wherein:
Fig. 1 is under air drying condition, containing pipe tobacco and the blank pipe tobacco (blank) of moist-keeping flavouring agent, containing propane diols pipe tobacco (contrast) moisture content temporal evolution tendency chart;
Fig. 2 is under air drying condition, containing pipe tobacco and the blank pipe tobacco (blank) of moist-keeping flavouring agent, containing propane diols pipe tobacco (contrast) percentage of water loss temporal evolution tendency chart.
The specific embodiment
Describe embodiments of the invention below in detail.Below by the embodiment being described with reference to the drawings, be exemplary, only for explaining the present invention, and can not be interpreted as limitation of the present invention.
Experimental example:
One. humectation effect assessment
1. test purpose
Contrast under equal conditions, containing the pipe tobacco of moist-keeping flavouring agent and blank pipe tobacco (blank), contain the physics humectation effect of propane diols pipe tobacco (contrast).
2. test sample
Moist-keeping flavouring agent: 1% moist-keeping flavouring agent+middle-grade blank pipe tobacco
Contrast: 1% propane diols+middle-grade blank pipe tobacco
Blank: middle-grade blank pipe tobacco
3. method of testing
3.1 equilibrium process: three groups of samples of test experiments are placed in to temperature: (22 ± 1) ℃, humidity: in the climatic chamber of (60 ± 3) %, balance is 48 hours, measures three groups of initial water contents of testing samples by Oven Method, is the moisture content of 0h.
3.2 test process: be temperature by climatic chamber Environmental adjustments: (22 ± 1) ℃, humidity: (40 ± 3) %, three groups of test samples are placed in one, and interval certain hour weighs an example weight, and calculates its instant moisture content according to example weight now.
4. test result
Moisture content and percentage of water loss in time limit are breathed out tendency chart analysis: referring to attached Fig. 1 and 2.
Fig. 1 contains the pipe tobacco of moist-keeping flavouring agent with blank pipe tobacco (blank), containing propane diols pipe tobacco (contrast) moisture content temporal evolution trend pattern.
Figure 1 shows that under test condition to be moisture-time test curve of air drying condition, curve demonstration, when 0-20h, moist-keeping flavouring agent, blank, the violent dehydration of contrast, moisture is downward trend linearly.After 24h, both moisture content curves tend towards stability, and this means, after 24h, both are issued to the absorption equilibrium of moisture at this environment, and from moisture content comparison at this moment, moist-keeping flavouring agent > is blank.Visible, in the environment of air drying, moist-keeping flavouring agent has certain moisture holding capacity, can improve the moisture content of tobacco sample.
Fig. 2 contains the pipe tobacco of moist-keeping flavouring agent with blank pipe tobacco (blank), containing propane diols pipe tobacco (contrast) percentage of water loss temporal evolution tendency chart.
As shown in Figure 2, percentage of water loss referred within certain period, the ratio of the fluid loss of sample and initial moisture.The fluid loss of n hour percentage of water loss=n hour/initial moisture.In 24 hours, the percentage of water loss of 3 groups of samples changes violent.Because sample is positioned in dry environment, what first lose is the free state moisture on pipe tobacco surface, so the speed of moisture loss is very fast.After 48 hours, in the prolongation along with equilibration time, it is constant that percentage of water loss is tending towards.The situation that percentage of water loss changes from 48 hours can be found out, the agent of blank > contrast > moist-keeping flavouring.From the contrast percentage of water loss data that 48h is later, totally it seems, under air drying environment, moist-keeping flavouring agent can delay sample moisture loss, delays moisture loss speed, and effect is better than propane diols.
In sum, moist-keeping flavouring agent can be played and slow down scattering and disappearing of moisture in air drying environment, reduces the percentage of water loss of pipe tobacco, plays the effect that maintains moisture in cut tobacco.
Two. the effect assessment of smokeing panel test
Get the agent of finished product moist-keeping flavouring, respectively according to 0.005%, 0.01%, 0.02% makes an addition on high, medium and low Virginian-type cigarette leaf group pipe tobacco, and in sealing bag, room temperature is placed after 2h, with being rolled into cigarette on CMBl20 cigarette machine, in the wet tank inner equilibrium 48h of 22 ℃ ± l ℃ and RH60% ± 2%, organize the expert of the committee that originally smokes panel test to smoke panel test, totally 7 of experts, are provincial judging panel.
Result shows, moist-keeping flavouring agent makes an addition to after cigarette leaf group, can effectively increase the perfume quantity of cigarette, improve fragrance matter and harmony, reduce assorted gas and excitant, increase sweet sense, make pleasant impression cleaner, comfortable, Integral lifting the interior quality of cigarette, especially in low and middle-grade cigarette, effect is more obvious.Smoking result is in Table 2.
The agent of table 2. moist-keeping flavouring makes an addition to the smoking result after cigarette
Embodiment mono-
Get respectively barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis, after pulverizing, in 0.5:0.5:0.2:0.3:0.3:1 ratio, evenly mix, add 8 times of amount pure water, soak after 2h, 1h is extracted in 75 ℃ of hot refluxs, extracts altogether 3 times, merges No. 3 times extract, 80 ℃, under pressure 0.02Mpa condition, being concentrated into density is 1.12 liquid extracts.Add 2 times of volume ethanol, standing 24h, filtering-depositing, 80 ℃, under pressure 0.02Mpa condition, being concentrated into density is 1.12 liquid extracts, filters, and obtains moist-keeping flavouring additive agent.Get additive 10g, be dissolved in 20kg distilled water, be sprayed on after 500kg pipe tobacco, roll into cigarette.
Embodiment bis-
Get respectively barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis, after pulverizing, in 1:0.75:0.5:0.5:0.5:1 ratio, evenly mix, add 6 times of amount pure water, soak after 6h, 1.5h is extracted in 70 ℃ of hot refluxs, extracts altogether 3 times, merges No. 3 times extract, 75 ℃, under pressure 0.06Mpa condition, being concentrated into density is 1.11 liquid extracts.Add 2 times of volume ethanol, standing 36h, filtering-depositing, 75 ℃, under pressure 0.06Mpa condition, being concentrated into density is 1.11 liquid extracts, filters, and obtains moist-keeping flavouring additive agent.Get additive 50g, be dissolved in 20kg distilled water, be sprayed on after 500kg pipe tobacco, roll into cigarette.
Embodiment tri-
Get respectively barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis, after pulverizing, in 1.5:1:1:1.5:1.5:1 ratio, evenly mix, add 10 times of amount pure water, soak after 12h, 1.5h is extracted in 65 ℃ of hot refluxs, extracts altogether 3 times, merges No. 3 times extract, 70 ℃, under pressure 0.03Mpa condition, being concentrated into density is 1.13 liquid extracts.Add 2 times of volume ethanol, standing 48h, filtering-depositing, 70 ℃, under pressure 0.03Mpa condition, being concentrated into density is 1.13 liquid extracts, filters, and obtains moist-keeping flavouring additive agent.Get additive 100g, be dissolved in 20kg distilled water, be sprayed on after 500kg pipe tobacco, roll into cigarette.
Embodiment tetra-
Get respectively barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis, after pulverizing, in 2:1.5:1:1:1:1 ratio, evenly mix, add 12 times of amount pure water, soak after 24h, 2h is extracted in 90 ℃ of hot refluxs, extracts altogether 3 times, merges No. 3 times extract, 65 ℃, under pressure 0.05Mpa condition, being concentrated into density is 1.12 liquid extracts.Add 2 times of volume ethanol, standing 72h, filtering-depositing, 65 ℃, under pressure 0.05Mpa condition, being concentrated into density is 1.12 liquid extracts, filters, and obtains moist-keeping flavouring additive agent.Get additive 500g, be dissolved in 20kg distilled water, be sprayed on after 500kg pipe tobacco, roll into cigarette.
Embodiment five
Get respectively barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis, after pulverizing, in 4:3:2:2:2:1 ratio, evenly mix, add 13 times of amount pure water, soak after 36h, 2.5h is extracted in 80 ℃ of hot refluxs, extracts altogether 3 times, merges No. 3 times extract, 75 ℃, under pressure 0.04Mpa condition, being concentrated into density is 1.12 liquid extracts.Add 2 times of volume ethanol, standing 72h, filtering-depositing, 75 ℃, under pressure 0.04Mpa condition, being concentrated into density is 1.12 liquid extracts, filters, and obtains moist-keeping flavouring additive agent.Get additive 1kg, be dissolved in 20kg distilled water, be sprayed on after 500kg pipe tobacco, roll into cigarette.
Embodiment six
Get respectively barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis, after pulverizing, in 8:6:4:4:5:1 ratio, evenly mix, add 15 times of amount pure water, soak after 48h, 3h is extracted in 100 ℃ of hot refluxs, extracts altogether 3 times, merges No. 3 times extract, 60 ℃, under pressure 0.06Mpa condition, being concentrated into density is 1.13 liquid extracts.Add 2 times of volume ethanol, standing 96h, filtering-depositing, 60 ℃, under pressure 0.06Mpa condition, being concentrated into density is 1.13 liquid extracts, filters, and obtains moist-keeping flavouring additive agent.Get additive 5kg, be dissolved in 20kg distilled water, be sprayed on after 500kg pipe tobacco, roll into cigarette.
Embodiment seven
Get barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis, after pulverizing, extract separately, add respectively 8 times of amount pure water, soak after 6h, 1h is extracted in 70 ℃ of hot refluxs, extracts altogether 3 times, merges No. 3 times extract, 70 ℃, under pressure 0.05Mpa condition, being concentrated into density is 1.13 liquid extracts.Add 2 times of volume ethanol, standing 24h, filtering-depositing, 70 ℃, under pressure 0.05Mpa condition, being concentrated into density is 1.13 liquid extracts, the liquid extract of barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis is mixed by 1:0.8:0.5:0.3:0.3:1, filter and obtain moist-keeping flavouring additive agent.Get additive 10g, be dissolved in 20kg distilled water, be sprayed on after 500kg pipe tobacco, roll into cigarette.
Embodiment eight
Get barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis, after pulverizing, extract separately, add respectively 10 times of amount pure water, soak after 12h, 1.5h is extracted in 80 ℃ of hot refluxs, extracts altogether 3 times, merges No. 3 times extract, 75 ℃, under pressure 0.08Mpa condition, being concentrated into density is 1.12 liquid extracts.Add 2 times of volume ethanol, standing 36h, filtering-depositing, 75 ℃, under pressure 0.08Mpa condition, being concentrated into density is 1.12 liquid extracts, the liquid extract of barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis is mixed by 2:1.5:1.5:1:1:1, filter and obtain moist-keeping flavouring additive agent.Get additive 50g, be dissolved in 20kg distilled water, be sprayed on after 500kg pipe tobacco, roll into cigarette.
Embodiment nine
Get barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis, after pulverizing, extract separately, add respectively 12 times of amount pure water, soak after 18h, 2h is extracted in 85 ℃ of hot refluxs, extracts altogether 3 times, merges No. 3 times extract, 80 ℃, under pressure 0.02Mpa condition, being concentrated into density is 1.12 liquid extracts.Add 2 times of volume ethanol, standing 48h, filtering-depositing, 80 ℃, under pressure 0.02Mpa condition, being concentrated into density is 1.12 liquid extracts, the liquid extract of barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis is mixed by 3:2:2:2:1.5:1, filter and obtain moist-keeping flavouring additive agent.Get additive 100g, be dissolved in 20kg distilled water, be sprayed on after 500kg pipe tobacco, roll into cigarette.
Embodiment ten
Get barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis, after pulverizing, extract separately, add respectively 6 times of amount pure water, soak after 24h, 2.5h is extracted in 90 ℃ of hot refluxs, extracts altogether 3 times, merges No. 3 times extract, 65 ℃, under pressure 0.04Mpa condition, being concentrated into density is 1.12 liquid extracts.Add 2 times of volume ethanol, standing 60h, filtering-depositing, 65 ℃, under pressure 0.04Mpa condition, being concentrated into density is 1.12 liquid extracts, the liquid extract of barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis is mixed by 4:3:2:2:1.5:1, filter and obtain moist-keeping flavouring additive agent.Get additive 500g, be dissolved in 20kg distilled water, be sprayed on after 500kg pipe tobacco, roll into cigarette.
Embodiment 11
Get barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis, after pulverizing, extract separately, add respectively 10 times of amount pure water, soak after 36h, 3h is extracted in 65 ℃ of hot refluxs, extracts altogether 3 times, merges No. 3 times extract, 60 ℃, under pressure 0.06Mpa condition, being concentrated into density is 1.12 liquid extracts.Add 2 times of volume ethanol, standing 72h, filtering-depositing, 60 ℃, under pressure 0.06Mpa condition, being concentrated into density is 1.12 liquid extracts, the liquid extract of barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis is mixed by 6:5:4:3:2:1, filter and obtain moist-keeping flavouring additive agent.Get additive 1kg, be dissolved in 20kg distilled water, be sprayed on after 500kg pipe tobacco, roll into cigarette.
Embodiment 12
Get barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis, after pulverizing, extract separately, add respectively 15 times of amount pure water, soak after 48h, 3h is extracted in 100 ℃ of hot refluxs, extracts altogether 3 times, merges No. 3 times extract, 80 ℃, under pressure 0.03Mpa condition, being concentrated into density is 1.13 liquid extracts.Add 2 times of volume ethanol, standing 96h, filtering-depositing, 80 ℃, under pressure 0.03Mpa condition, being concentrated into density is 1.13 liquid extracts, the liquid extract of barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis is mixed by 8:6:4:4:5:1, filter and obtain moist-keeping flavouring additive agent.Get additive 5kg, be dissolved in 20kg distilled water, be sprayed on after 500kg pipe tobacco, roll into cigarette.
Claims (3)
1. a cigarette moist-keeping flavouring additive agent, comprise traditional Chinese medicine extraction compositions or compound Chinese medicine extract, it is characterized in that: described traditional Chinese medicine extraction compositions or compound Chinese medicine extract comprise barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis; The part by weight of barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis is 0.5～8:0.5-6:0.2-4:0.3-4:0.3-5:1.
2. cigarette moist-keeping flavouring additive agent according to claim 1, is characterized in that: the extract weight ratio of barrenwort, eclipta, dessert almond, motherwort, dandelion and Exocarpium Citri Grandis is 1-8:0.8-6:0.5-4:0.3-4:0.3-5:1.
3. according to the application of arbitrary described a kind of cigarette moist-keeping flavouring additive agent in claim 1 or 2, it is characterized in that, get appropriate moist-keeping flavouring additive agent, be dissolved in certain volume distilled water, be evenly sprayed on cigarette shreds, stem, thin slice; The consumption of moist-keeping flavouring additive agent is pipe tobacco, stem, the 0.002-1%wt of flake weight.
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| CN103497834B (en) * | 2013-10-22 | 2015-07-08 | 中国烟草总公司郑州烟草研究院 | Method for preparing dandelion absolute oil and application of dandelion absolute oil in cigarettes |
| CN103710149B (en) * | 2013-12-30 | 2015-06-10 | 湖南先伟实业有限公司 | Wild chrysanthemum extract and taraxacum extract matched tobacco flavor, preparation method and application thereof |
| CN105011370B (en) * | 2015-07-29 | 2018-08-21 | 将军烟草集团有限公司 | A kind of cigarette moisturizing harm reduction device |
| CN109330016A (en) * | 2018-11-14 | 2019-02-15 | 河南中烟工业有限责任公司 | A kind of Exocarpium Citri Grandis medicinal extract, preparation method and the application in cigarette |
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| CN101693745A (en) * | 2009-09-01 | 2010-04-14 | 广东神农烟科技术有限公司 | Lucid ganoderma polysaccharide and extraction method thereof as well as cigarette containing lucid ganoderma polysaccharide and preparation method thereof |
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