CN102499460A - Extracting method for radix ophiopogonis extract and dark plum extract as well as cigarette containing radix ophiopogonis extract and dark plum extract - Google Patents
Extracting method for radix ophiopogonis extract and dark plum extract as well as cigarette containing radix ophiopogonis extract and dark plum extract Download PDFInfo
- Publication number
- CN102499460A CN102499460A CN2011103412546A CN201110341254A CN102499460A CN 102499460 A CN102499460 A CN 102499460A CN 2011103412546 A CN2011103412546 A CN 2011103412546A CN 201110341254 A CN201110341254 A CN 201110341254A CN 102499460 A CN102499460 A CN 102499460A
- Authority
- CN
- China
- Prior art keywords
- dark plum
- tuber
- dwarf lilyturf
- extract
- medicinal extract
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses an extracting method for a radix ophiopogonis extract and a dark plum extract as well as a cigarette containing the radix ophiopogonis extract and the dark plum extract in order to solve the technical problem on the reduction of dry sensation and harm of smoke of the cigarette. The extracting method for the radix ophiopogonis extract and the dark plum extract comprises the following steps of: drying and crushing radix ophiopogonis and dark plums; adding hot water into radix ophiopogonis and dark plum powder; extracting and filtering; reducing pressure of filtrate; concentrating; adding ethanol; and stewing and filtering to obtain the ophiopogonis extract and the dark plum extract. According to the cigarette containing the radix ophiopogonis extract and the dark plum extract, disclosed by the invention, the mass of the radix ophiopogonis extract and the dark plum extract is 0.001-10% of that of cut tobacco. Compared with the prior art, the radix ophiopogonis extract and the dark plum extract are contained in the cut tobacco; during the smoking, components of the radix ophiopogonis extract and the dark plum extract can enter a human body along with mainstream smoke, and can be absorbed by the human body, so that the cigarette has the functions of killing bacteria, resisting pathogenic microorganisms, benefiting gallbladder, improving hypoxia tolerant capability and resisting aging; the smoke is plump and mellow, and has no foreign smells, so that secretion generation of the smoke is enhanced, and the throat is comfortable; the quality of the cigarette can be improved; and threats of the smoke to the human body can be reduced.
Description
Technical field
The present invention relates to a kind of extraction process of Chinese medicine and contain the cigarette of this extract, particularly a kind of tuber of dwarf lilyturf dark plum extraction process and contain the cigarette of this extract.
Background technology
China pays much attention to the harmful work of falling of cigarette, and since 2005, State Tobacco Monopoly Bureau has organized cigarette harmfulness index system and two great special research work of cigarette flavouring humectation, has obtained certain achievement.At 2010 beginning of the years, State Tobacco Monopoly Bureau clearly proposes " level on the cigarette " conduct basic principle and the strategic task of an industry job in period at present and in the future, and the humectation of cigarette flavouring, cigarette harm reduction technology are two big main directions.Homemade cigarette dry sensation is obvious, concentrate on moisture in cut tobacco scatter and disappear fast, main flume moisture is on the low side etc., these typical proterties are compiled, and make the comfortableness of sucking of cigarette receive obvious inhibition.Therefore, " moist-keeping flavouring " becomes the common issue with that industry faces.Meanwhile, along with the raising of living standards of the people, health perception further strengthens, and " lowering harm and decreasing coking " becomes each research staff's of cigarette industry enterprise main direction of studying.When continuing to reduce cigarette harm targetedly, keep and promote perfume quantity and the fragrance matter of tobacco, overcome the tangible proterties of Chinese style cigarette dry sensation simultaneously, be the developing goal of new period high-quality cigarette.Number of patent application 200610128283 disclosed Sargassum fusiforme aqueous extracts and in Application in Tobacco; Sargassum fusiforme aqueous extract is joined on the cigarette shreds with feed liquid as cigarette; Cigarette can produce special chemical component when burning and sucking; Obviously improve or improve the quality quality of cigarette, have the effect of promoting the production of body fluid significantly and certain relieving cough function, and can reduce some harmful components in the cigarette mainstream flue gas.The natural tobacco additive of number of patent application 200710052295 disclosed a kind of flavouring humectations, its raw material are Momordica grosvenori, and its manufacturing approach is with inserting in the ethanolic solution through the Momordica grosvenori raw material of pulverizing, soak or refluxing extraction, filter, obtaining the Momordica grosvenori extract; Decompression concentrates the Momordica grosvenori extract under water bath condition again, reclaims the extract solvent, obtains natural tobacco additive Momordica grosvenori medicinal extract; Utilized the Momordica grosvenori that China is peculiar and common, have cough-relieving apophlegmatic moistening lung effect, the very sweet nonhazardous again of flavor; Be made into natural additive and be added on the pipe tobacco, can increase cigarette perfume quantity, to set off the nature cigarette fragrant, reduce the flue gas drying sense, strengthen the flue gas sense of promoting the production of body fluid; Improve the cigarette comfort level, alleviate harmfulness of smoking.But can not satisfy consumer's multiple needs.
Summary of the invention
The purpose of this invention is to provide a kind of tuber of dwarf lilyturf of dark plum medicinal extract method for distilling and contain the cigarette of the dark plum medicinal extract tuber of dwarf lilyturf, the technical problem that solve is to reduce dry sensation of cigarette smoke to endanger with flue gas.
The present invention adopts following technical scheme: a kind of tuber of dwarf lilyturf dark plum medicinal extract method for distilling, may further comprise the steps: one, dark plum 1-99% by mass percentage, the tuber of dwarf lilyturf, 1-99% got the dry tuber of dwarf lilyturf, dark plum, was not more than 60 ℃ of oven dry, and was crushed to the 10-100 order; Two, the hot water that adds 90 ℃ by the mass ratio of feed liquid at 1: 10, lixiviate under this temperature conditions, one time 5 hours, lixiviate 2 times merged 2 times water extract, filtered, and obtained filtrating; Three, filtrate at 0.05Mpa, reduced pressure under the condition in 60 ℃, 2 hours, concentrate; Four, the filtrating after will concentrating adds 75% ethanol of 5 times of volumes, is no more than 4 ℃ and leaves standstill and be no less than 12 hours, and 4000 rev/mins of centrifugal treating rotating speeds filter, and obtain the dark plum medicinal extract tuber of dwarf lilyturf.
The present invention is dark plum 40-75% by mass percentage, the tuber of dwarf lilyturf 25-60%.
The present invention is dark plum 50% by mass percentage, the tuber of dwarf lilyturf 50%.
A kind of tuber of dwarf lilyturf dark plum medicinal extract method for distilling, may further comprise the steps: one, 1-99% by mass percentage, the tuber of dwarf lilyturf, cream 1-99% got the dry tuber of dwarf lilyturf, dark plum, was not more than 60 ℃ of oven dry, steeped 2 hours the mass ratio of feed liquid 1: 15 with 20 ℃ of water loggings; Two, ultrasonic power is 80W/cm
2, the processing time is 30 minutes, filters, and obtains filtrating; Three, filtrate at 0.05Mpa, reduced pressure under the condition in 60 ℃, 2 hours, concentrate; Four, the filtrating after will concentrating adds 75% ethanol of 10 times of volumes, and be no more than 10 ℃ and leave standstill and be no less than 12 hours, centrifugal treating, 4000 rev/mins of rotating speeds filter, and obtain the dark plum medicinal extract tuber of dwarf lilyturf.
The present invention is dark plum 40-75% by mass percentage, the tuber of dwarf lilyturf 25-60%.
The present invention is dark plum 50% by mass percentage, the tuber of dwarf lilyturf 50%.
A kind of cigarette that contains the dark plum medicinal extract tuber of dwarf lilyturf comprises pipe tobacco, adds in the said pipe tobacco to account for tobacco quality dark plum medicinal extract 0.001～10% tuber of dwarf lilyturf.
Add in the pipe tobacco of the present invention and account for tobacco quality dark plum medicinal extract 0.01～1% tuber of dwarf lilyturf.
Add in the pipe tobacco of the present invention and account for tobacco quality dark plum medicinal extract 0.1% tuber of dwarf lilyturf.
The cigarette that contains the dark plum medicinal extract tuber of dwarf lilyturf of the present invention prepares in order to the below method: with the tuber of dwarf lilyturf dark plum medicinal extract be dissolved in 10-80% ethanol, liquor capacity concentration is 1-10%, evenly is sprayed onto in the pipe tobacco, dries, processes cigarette by art methods.
The present invention compared with prior art contains the dark plum medicinal extract tuber of dwarf lilyturf in the pipe tobacco, the tuber of dwarf lilyturf, dark plum medicinal extract composition can get into human body with main flume in smoking process; Be absorbed by the body through blood circulation, thereby bring into play its sterilization, resisting pathogenic microbes, cholagogic, raising hypoxia-bearing capability, antidotal effect, can improve flue gas strength; Make cigarette smoke full, mellow, do not have assorted gas, strengthen the flue gas sense of promoting the production of body fluid, throat is comfortable; Can improve the cigarette quality, reduce the harmfulness of flue gas human body.
The specific embodiment
Below in conjunction with embodiment the present invention is elaborated.Tuber of dwarf lilyturf of the present invention, dark plum medicinal extract method for distilling adopted the hot water extraction, may further comprise the steps:
One, dark plum 1-99% by mass percentage, the tuber of dwarf lilyturf, 1-99% got the dry tuber of dwarf lilyturf, dark plum, removed impurity, was not more than 60 ℃ of oven dry, and was crushed to the 10-100 order.
Two, the hot water that adds 90 ℃ by the mass ratio of feed liquid at 1: 10, lixiviate under this temperature conditions, one time 5 hours, lixiviate 2 times merged 2 times water extract, filtered, and obtained filtrating.
Three, filtrate at 0.05Mpa, reduced pressure under the condition in 60 ℃, 2 hours, concentrate.
Four, the filtrating after will concentrating adds 75% ethanol of 5 times of volumes, and be no more than 4 ℃ and leave standstill and be no less than 12 hours, centrifugal treating, 4000 rev/mins of rotating speeds filter, and obtain the dark plum medicinal extract tuber of dwarf lilyturf.
Tuber of dwarf lilyturf of the present invention, dark plum medicinal extract method for distilling adopted ultrasonic extraction, may further comprise the steps:
One, 1-99% by mass percentage, the tuber of dwarf lilyturf, cream 1-99% got the dry tuber of dwarf lilyturf, dark plum, removed impurity, was not more than 60 ℃ of oven dry, steeped 2 hours the mass ratio of feed liquid 1: 15 with 20 ℃ of water loggings.
Two, feed liquid is used Extraction by Ultrasound, and ultrasonic power is 80W/cm
2, the processing time is 30 minutes, filters, and obtains filtrating.
Three, filtrate at 0.05Mpa, reduced pressure under the condition in 60 ℃, 2 hours, concentrate.
Four, the filtrating after will concentrating adds 75% ethanol of 10 times of volumes, and be no more than 10 ℃ and leave standstill and be no less than 12 hours, centrifugal treating, 4000 rev/mins of rotating speeds filter, and obtain the dark plum medicinal extract tuber of dwarf lilyturf.
The cigarette that contains the dark plum medicinal extract tuber of dwarf lilyturf of the present invention, adding accounts for tobacco quality dark plum medicinal extract 0.001～10% tuber of dwarf lilyturf in the pipe tobacco of cigarette.The tuber of dwarf lilyturf, dark plum medicinal extract can adopt the dark plum medicinal extract tuber of dwarf lilyturf of the inventive method preparation, the dark plum medicinal extract tuber of dwarf lilyturf that also can adopt prepared by other to obtain.
The tuber of dwarf lilyturf, dark plum medicinal extract was soluble in 10-80% ethanol, and dissolubility is good.The cigarette that contains the dark plum medicinal extract tuber of dwarf lilyturf of the present invention; Prepare in order to the below method: with the tuber of dwarf lilyturf dark plum medicinal extract be dissolved in 10-80% ethanol; Liquor capacity concentration behind the 10-80% dissolve with ethanol is 1-10%, evenly is sprayed onto in the pipe tobacco, dries, processes cigarette by art methods.
Dark plum is the almost ripe fruit of the plum Prunus mume of rosaceae plant deciduous tree (Sieh.) Sieb.et Zucc., smokes through pyrotechnics to form.Function cures mainly: astringe the lung, puckery intestines promote the production of body fluid, claming ascaris.Be used for chronic cough of deficiency lung, abnormal heat polydipsia, chronic malaria, rush down for a long time, dysentery, have blood in stool, hematuria, metrorrhagia, ascariasis of biliary tract stomachache, vomiting, hookworm disease etc.Fruit contains citric acid edge citric? Acid
malic acid malicacid
total acid content of 4% -5.5%.
Be the dried root of Liliaceae Ophiopogon perennial evergreen herbaceous plant Ophiopogon tuber of dwarf lilyturf japonicus (T.f) Ker-Gawl. the tuber of dwarf lilyturf.Sweet cold clear and rich, function with cure mainly: nourishing Yin and promoting production of body fluid, moistening lung clears away heart-fire.Be used for dryness of the lung dry cough, deficiency of Yin consumptive disease is coughed, larynx numbness pharyngalgia, and Tianjin wound is thirsty, and interior heat is quenched one's thirst, vexed insomnia, the dry constipation of intestines.Contain the saponin A tuber of dwarf lilyturf, B, C, D ophiopogoninA the tuber of dwarf lilyturf; B; C,
Dark plum pharmacological action: 1, resisting pathogenic microbes effect; Experiment in vitro shows; 1: 1 water decocted solution of fructus mume of mass ratio all has inhibitory action to bacillus anthracis, diphtheria and diphtheroid, hay bacillus, staphylococcus (golden yellow, lemon yellow, white), pneumococcus; Also effective to pathogenic bacteria in the intestines such as Escherichia coli, bacterium sonnei, proteus, typhoid fever and paratyphosum Bacterium, Pseudomonas aeruginosa, comma bacillus, the bacteriostasis of dark plum and its preparation are acidity has certain relation.2, to the effect of roundworm, the effect that dark plum has excitement, stimulates roundworm to retreat roundworm.Volume is that the roundworm activity obviously is restricted in 5% the dark plum solution.3, choleretic effect, dark plum can increase the secretion of bile, and can make bile be tending towards acid, gall-bladder is had promote to shrink and choleretic effect, be beneficial to the drainage biliary tract bile, reduce and prevent infection of biliary tract.
The pharmacological action tuber of dwarf lilyturf: 1, antiarrhythmic effect, ophiopogon root total saponin can effectively prevent or resist the arrhythmia cordis that low potassium brings out.2, immunization, ophiopogon root total saponin have obvious antifatigue effect and delay senility, and improve immunity of organisms.
The main active ingredient of the dark plum medicinal extract tuber of dwarf lilyturf is organic acid, has multiple physiologically active.The tuber of dwarf lilyturf, dark plum medicinal extract had sterilization, resisting pathogenic microbes, immunological regulation, raising hypoxia-bearing capability and anti-fatigue effect.
The tuber of dwarf lilyturf, the pharmacological action of dark plum medicinal extract was:
1, the effect of sterilization, resisting pathogenic microbes: the tuber of dwarf lilyturf, dark plum medicinal extract contained compositions such as rich organic acid such as malic acid, citric acid, butanedioic acid, citric acid; The in-vitro antibacterial experiment shows that it has significant antibacterial action, all has inhibitory action to shigella dysenteriae, Pseudomonas aeruginosa, typhoid bacillus, Escherichia coli, tubercle bacillus, proteus, staphylococcus aureus, comma bacillus and various dermatophytes etc.
2, immunoregulation effect: the tuber of dwarf lilyturf, dark plum medicinal extract can increase the spleen weight of mouse significantly, significantly strengthened the carbon clearance effect of mouse, and antagonism is reduced by the murine interleukin that endoxan and 60 Co-radiation gammas cause.
3, anti-anoxic and antifatigue effect: the tuber of dwarf lilyturf, dark plum medicinal extract prolonged the time-to-live of mouse significantly; In the experiment of rat carotid artery caused by ligature cerebral ischemia; The dark plum cream tuber of dwarf lilyturf that gives 200mg/kg and 400mg/kg before the ligation all can make the interior lactic acid content of administration group ligation hindbrain significantly reduce (P＜0.05～P＜0.01) than model group; Thereby alleviate acid poisoning, protection ischemic tissue prevents primary cellular defect.The prompting ophiopogonpolysaccharide has anti-hypoxia protection effect to cerebral ischemia.Mouse swimming test shows that the tuber of dwarf lilyturf, amino acid and ophiopogonpolysaccharide had certain antifatigue effect.
The present invention with the tuber of dwarf lilyturf dark plum medicinal extract join in the cigarette shreds, during smoking, the cigarette smoke free from extraneous odour has Hui Tian, falls evil effect.Prior art is compared in invention has following advantage: the flue gas that 1, improves cigarette.2, the harmful components in the reduction cigarette mainstream flue gas.3, do not change the original manufacturing process of cigarette.4, increase cigarette flavor, can obviously keep moisture in cut tobacco, reduce the flue gas drying sense, and can enrich cigarette perfume (or spice), improve the cigarette comfort level.5, the sweet sense that keeps cigarette has Hui Tian, reduces the effect that flue gas stimulates.6, security is very high.Have no side effect
With the cigarette that contains the dark plum medicinal extract tuber of dwarf lilyturf of the present invention; Measure by " the mensuration chromatography of ions of ammonia in the YC/T 377-2010 cigarette mainstream flue gas " and " the mensuration high performance liquid chromatography of main carbonyls in the YC/T 254-2008 cigarette mainstream flue gas "; Adding the cigarette that the tuber of dwarf lilyturf of the present invention, dark plum medicinal extract was made compares with the blank cigarette that does not add the dark plum medicinal extract tuber of dwarf lilyturf; Reduce the peculiar ammonia of the tobacco in the flue gas, crotonaldehyde, reduced scope 15-20%.Show the respiratory tract injury that can reduce the smoker by making the animal toxicity test by " GB15193.1-21-2003 toxicological evaluation of food safety procedure and method ".Guangdong provincial cigarette teacher of the smokeing panel test is according to " specification requirement of GB5606.4-2005 cigarette sense organ " flue gas delicate fragrance, mellow when smokeing panel test, and throat is comfortable, Hui Tian, free from extraneous odour, assorted gas.
Embodiment 1, heat-obtaining flooding dark plum tuber of dwarf lilyturf medicinal extract, and wherein the mass percent dark plum 50%; The tuber of dwarf lilyturf 50%; Behind 50% dissolve with ethanol, join in the cigarette shreds, the tuber of dwarf lilyturf, the volumetric concentration of dark plum medicinal extract solution was 10%, and the tuber of dwarf lilyturf, dark plum medicinal extract consumption was that 1% of tobacco quality is processed cigarette.When Guangdong provincial cigarette teacher of the smokeing panel test; Cigarette smoke is mellow, full, free from extraneous odour; Throat is comfortable, and Hui Tian is by " the mensuration chromatography of ions of ammonia in the YC/T 377-2010 cigarette mainstream flue gas " and " the mensuration high performance liquid chromatography of main carbonyls in the YC/T 254-2008 cigarette mainstream flue gas "; Detecting flue gas has and falls the evil effect, and testing result is seen table 1.
Embodiment 2, and dark plum 75% by mass percentage, the tuber of dwarf lilyturf 25%, get the dry tuber of dwarf lilyturf, dark plum; Remove impurity, 60 ℃ of oven dry, and be crushed to the 10-100 order, press mass ratio and add 90 ℃ of hot water at 1: 10; 90 ℃ of following lixiviates, one time 5 hours, lixiviate was 2 times altogether, merges 2 times water extract; Filter, filtrating decompression under 0.05Mpa, 60 ℃, 2 hours conditions, concentrate, the filtrating after concentrating is added 75% ethanol of 5 times of volumes, be no more than 4 ℃ and left standstill 12 hours; 4000 rev/mins of centrifugal rotational speeds filter, and obtain the dark plum medicinal extract tuber of dwarf lilyturf.With the tuber of dwarf lilyturf dark plum medicinal extract behind 10% dissolve with ethanol, be added in the cigarette shreds, the tuber of dwarf lilyturf, the liquor capacity concentration of dark plum medicinal extract was 10%, the tuber of dwarf lilyturf, dark plum medicinal extract consumption was 0.1% of a tobacco quality.When Guangdong provincial cigarette teacher of the smokeing panel test; Mellow, the free from extraneous odour of cigarette smoke; Throat is comfortable; By " the mensuration chromatography of ions of ammonia in the YC/T 377-2010 cigarette mainstream flue gas " and the mensuration high performance liquid chromatography of carbonyls " in the YC/T 254-2008 cigarette mainstream flue gas main ", detecting flue gas has and falls evil and act on, and testing result is seen table 1.
Embodiment 3, and dark plum 40% by mass percentage, will get the dry tuber of dwarf lilyturf, dark plum the tuber of dwarf lilyturf 60%, remove impurity, 60 ℃ of oven dry, and with 20 ℃ of floodings 2 hours, the feed liquid mass ratio was 1: 15, ultrasonic power is 80W/cm
2, the processing time is 30 minutes, filters; Filtrating decompression under 0.05Mpa, 60 ℃, 2 hours conditions, concentrate, the filtrating after concentrating is added 75% ethanol of 10 times of volumes, be no more than 10 ℃ and left standstill 12 hours; 4000 rev/mins of centrifugal rotational speeds filter, and obtain the dark plum medicinal extract tuber of dwarf lilyturf.With the tuber of dwarf lilyturf dark plum medicinal extract behind 75% dissolve with ethanol, be added in the cigarette shreds, the tuber of dwarf lilyturf, the liquor capacity concentration of dark plum medicinal extract was 8%, the tuber of dwarf lilyturf, dark plum medicinal extract consumption was 0.01% of a pipe tobacco weight.When Guangdong provincial cigarette teacher of the smokeing panel test; Mellow comfortable, the free from extraneous odour of cigarette cigarette smoke, assorted gas; By " the mensuration chromatography of ions of ammonia in the YC/T 377-2010 cigarette mainstream flue gas " and " the mensuration high performance liquid chromatography of main carbonyls in the YC/T254-2008 cigarette mainstream flue gas "; Detecting flue gas has and falls the evil effect, and testing result is seen table 1.
About the consumption of the dark plum medicinal extract tuber of dwarf lilyturf, as long as in the 0.001-10% of pipe tobacco weight, all can reach certain effect.
Table 1 dark plum tuber of dwarf lilyturf medicinal extract reduces harmful components BaP, phenol testing result in the flue gas
Claims (10)
- One kind the tuber of dwarf lilyturf dark plum medicinal extract method for distilling, may further comprise the steps: one, dark plum 1-99% by mass percentage, the tuber of dwarf lilyturf, 1-99% got the dry tuber of dwarf lilyturf, dark plum, was not more than 60 ℃ of oven dry, and was crushed to the 10-100 order; Two, the hot water that adds 90 ℃ by the mass ratio of feed liquid at 1: 10, lixiviate under this temperature conditions, one time 5 hours, lixiviate 2 times merged 2 times water extract, filtered, and obtained filtrating; Three, filtrate at 0.05Mpa, reduced pressure under the condition in 60 ℃, 2 hours, concentrate; Four, the filtrating after will concentrating adds 75% ethanol of 5 times of volumes, is no more than 4 ℃ and leaves standstill and be no less than 12 hours, and 4000 rev/mins of centrifugal treating rotating speeds filter, and obtain the dark plum medicinal extract tuber of dwarf lilyturf.
- 2. tuber of dwarf lilyturf according to claim 1 dark plum medicinal extract method for distilling, it is characterized in that: the said 40-75% of dark plum by mass percentage, the tuber of dwarf lilyturf 25-60%.
- 3. tuber of dwarf lilyturf according to claim 2, dark plum medicinal extract method for distilling is characterized in that: said dark plum by mass percentage 50%, the tuber of dwarf lilyturf 50%.
- One kind the tuber of dwarf lilyturf dark plum medicinal extract method for distilling, may further comprise the steps: one, 1-99% by mass percentage, the tuber of dwarf lilyturf, cream 1-99% got the dry tuber of dwarf lilyturf, dark plum, was not more than 60 ℃ of oven dry, steeped 2 hours the mass ratio of feed liquid 1: 15 with 20 ℃ of water loggings; Two, ultrasonic power is 80W/cm 2, the processing time is 30 minutes, filters, and obtains filtrating; Three, filtrate at 0.05Mpa, reduced pressure under the condition in 60 ℃, 2 hours, concentrate; Four, the filtrating after will concentrating adds 75% ethanol of 10 times of volumes, and be no more than 10 ℃ and leave standstill and be no less than 12 hours, centrifugal treating, 4000 rev/mins of rotating speeds filter, and obtain the dark plum medicinal extract tuber of dwarf lilyturf.
- 5. tuber of dwarf lilyturf according to claim 4 dark plum medicinal extract method for distilling, it is characterized in that: the said 40-75% of dark plum by mass percentage, the tuber of dwarf lilyturf 25-60%.
- 6. tuber of dwarf lilyturf according to claim 5, dark plum medicinal extract method for distilling is characterized in that: said dark plum by mass percentage 50%, the tuber of dwarf lilyturf 50%.
- 7. a cigarette that contains the dark plum medicinal extract tuber of dwarf lilyturf comprises pipe tobacco, it is characterized in that: adding accounts for tobacco quality dark plum medicinal extract 0.001～10% tuber of dwarf lilyturf in the said pipe tobacco.
- 8. the cigarette that contains the dark plum medicinal extract tuber of dwarf lilyturf according to claim 5 is characterized in that: adding accounts for tobacco quality dark plum medicinal extract 0.01～1% tuber of dwarf lilyturf in the said pipe tobacco.
- 9. the cigarette that contains the dark plum medicinal extract tuber of dwarf lilyturf according to claim 6 is characterized in that: adding accounts for tobacco quality dark plum medicinal extract 0.1% tuber of dwarf lilyturf in the said pipe tobacco.
- 10. the cigarette that contains the dark plum medicinal extract tuber of dwarf lilyturf according to claim 9; It is characterized in that: the said cigarette that contains the dark plum medicinal extract tuber of dwarf lilyturf; Prepare in order to the below method: with the tuber of dwarf lilyturf dark plum medicinal extract be dissolved in 10-80% ethanol; Liquor capacity concentration is 1-10%, evenly is sprayed onto in the pipe tobacco, dries, processes cigarette by art methods.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110341254 CN102499460B (en) | 2011-11-02 | 2011-11-02 | Extracting method for radix ophiopogonis extract and dark plum extract as well as cigarette containing radix ophiopogonis extract and dark plum extract |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110341254 CN102499460B (en) | 2011-11-02 | 2011-11-02 | Extracting method for radix ophiopogonis extract and dark plum extract as well as cigarette containing radix ophiopogonis extract and dark plum extract |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102499460A true CN102499460A (en) | 2012-06-20 |
| CN102499460B CN102499460B (en) | 2013-09-04 |
Family
ID=46211642
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201110341254 Active CN102499460B (en) | 2011-11-02 | 2011-11-02 | Extracting method for radix ophiopogonis extract and dark plum extract as well as cigarette containing radix ophiopogonis extract and dark plum extract |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102499460B (en) |
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102697169A (en) * | 2012-07-02 | 2012-10-03 | 广西中烟工业有限责任公司 | Moisturizing and flavor-enhancing additive for cigarettes as well as preparation method and application thereof |
| CN102697170A (en) * | 2012-07-02 | 2012-10-03 | 广西中烟工业有限责任公司 | Aroma-increasing and humidity-preserving additive for cigarettes and preparation method and application thereof |
| CN103349355A (en) * | 2013-06-28 | 2013-10-16 | 湖北中烟工业有限责任公司 | Black pepper and dark plum compound extract, preparation method thereof and application of compound extract taken as tobacco product additive |
| CN103494320A (en) * | 2013-09-09 | 2014-01-08 | 湖南中烟工业有限责任公司 | Buccal type smokeless tobacco product with plum flavor |
| CN103555425A (en) * | 2013-11-14 | 2014-02-05 | 浙江安赛生物科技有限公司 | Method for preparing jasmine concrete by using high-frequency ultrasonic cavitation technology |
| CN104188087A (en) * | 2014-08-20 | 2014-12-10 | 云南中烟工业有限责任公司 | Application of preserved plum spice in cigarettes |
| CN104188088A (en) * | 2014-08-20 | 2014-12-10 | 云南中烟工业有限责任公司 | Method for improving smoking flavor quality of cigarettes with preserved plums |
| CN107319626A (en) * | 2017-07-07 | 2017-11-07 | 河南中烟工业有限责任公司 | A kind of tobacco aromaticss and preparation method thereof and the application in cigarette |
| CN110123893A (en) * | 2019-06-25 | 2019-08-16 | 云南中烟工业有限责任公司 | Smoked plum extractive is preparing the application in drug or health care product for preventing and treating the death of mouth epithelial cells caused by buccal cigarette |
| CN110484369A (en) * | 2019-08-06 | 2019-11-22 | 云南中烟新材料科技有限公司 | A method of tobacco aromaticss are prepared based on dark plum recovery rate is promoted |
| CN110747061A (en) * | 2019-11-12 | 2020-02-04 | 云南中烟新材料科技有限公司 | Smoked plum tobacco flavoring particle material and preparation method and application thereof |
| CN112098568A (en) * | 2019-06-17 | 2020-12-18 | 国药集团同济堂（贵州）制药有限公司 | Preparation method and quality detection method of dark plum extract |
| CN113974213A (en) * | 2021-12-06 | 2022-01-28 | 云南中烟工业有限责任公司 | Composite additive for reducing phenol release amount in smoke and preparation method and application thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101214088A (en) * | 2008-01-22 | 2008-07-09 | 红云烟草(集团)有限责任公司 | Chinese herbal medicine extract for reforging tobacco leaf by papermaking method and preparation and using method thereof |
| CN101444333A (en) * | 2008-11-28 | 2009-06-03 | 华芳烟用香料有限公司 | Method of preparing Grosvenor momordica extract and application thereof |
| CN101461565A (en) * | 2009-01-08 | 2009-06-24 | 华健 | Medicinal health type tobacco juice for electronic smoke |
| CN102090711A (en) * | 2009-12-15 | 2011-06-15 | 大连水产学院 | Preparation method for health cigarette and product |
-
2011
- 2011-11-02 CN CN 201110341254 patent/CN102499460B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101214088A (en) * | 2008-01-22 | 2008-07-09 | 红云烟草(集团)有限责任公司 | Chinese herbal medicine extract for reforging tobacco leaf by papermaking method and preparation and using method thereof |
| CN101444333A (en) * | 2008-11-28 | 2009-06-03 | 华芳烟用香料有限公司 | Method of preparing Grosvenor momordica extract and application thereof |
| CN101461565A (en) * | 2009-01-08 | 2009-06-24 | 华健 | Medicinal health type tobacco juice for electronic smoke |
| CN102090711A (en) * | 2009-12-15 | 2011-06-15 | 大连水产学院 | Preparation method for health cigarette and product |
Cited By (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102697169B (en) * | 2012-07-02 | 2014-08-20 | 广西中烟工业有限责任公司 | Moisturizing and flavor-enhancing additive for cigarettes as well as preparation method and application thereof |
| CN102697170A (en) * | 2012-07-02 | 2012-10-03 | 广西中烟工业有限责任公司 | Aroma-increasing and humidity-preserving additive for cigarettes and preparation method and application thereof |
| CN102697169A (en) * | 2012-07-02 | 2012-10-03 | 广西中烟工业有限责任公司 | Moisturizing and flavor-enhancing additive for cigarettes as well as preparation method and application thereof |
| CN103349355B (en) * | 2013-06-28 | 2016-03-09 | 湖北中烟工业有限责任公司 | Black pepper dark plum composite extract and preparation method thereof and the purposes as additive of tobacco product |
| CN103349355A (en) * | 2013-06-28 | 2013-10-16 | 湖北中烟工业有限责任公司 | Black pepper and dark plum compound extract, preparation method thereof and application of compound extract taken as tobacco product additive |
| CN103494320A (en) * | 2013-09-09 | 2014-01-08 | 湖南中烟工业有限责任公司 | Buccal type smokeless tobacco product with plum flavor |
| CN103494320B (en) * | 2013-09-09 | 2015-12-02 | 湖南中烟工业有限责任公司 | A kind of type of sucking smokeless tobacco articles containing plum flavor |
| CN103555425B (en) * | 2013-11-14 | 2015-12-30 | 浙江安赛生物科技有限公司 | A kind of method utilizing high-frequency ultrasonic cavitation technology to prepare jasmine concrete |
| CN103555425A (en) * | 2013-11-14 | 2014-02-05 | 浙江安赛生物科技有限公司 | Method for preparing jasmine concrete by using high-frequency ultrasonic cavitation technology |
| CN104188087A (en) * | 2014-08-20 | 2014-12-10 | 云南中烟工业有限责任公司 | Application of preserved plum spice in cigarettes |
| CN104188088A (en) * | 2014-08-20 | 2014-12-10 | 云南中烟工业有限责任公司 | Method for improving smoking flavor quality of cigarettes with preserved plums |
| CN107319626A (en) * | 2017-07-07 | 2017-11-07 | 河南中烟工业有限责任公司 | A kind of tobacco aromaticss and preparation method thereof and the application in cigarette |
| CN112098568A (en) * | 2019-06-17 | 2020-12-18 | 国药集团同济堂（贵州）制药有限公司 | Preparation method and quality detection method of dark plum extract |
| CN110123893A (en) * | 2019-06-25 | 2019-08-16 | 云南中烟工业有限责任公司 | Smoked plum extractive is preparing the application in drug or health care product for preventing and treating the death of mouth epithelial cells caused by buccal cigarette |
| CN110123893B (en) * | 2019-06-25 | 2022-07-01 | 云南中烟工业有限责任公司 | Application of dark plum extract in preparation of medicine or health-care product for preventing and treating oral epithelial cell death caused by mouth tobacco |
| CN110484369A (en) * | 2019-08-06 | 2019-11-22 | 云南中烟新材料科技有限公司 | A method of tobacco aromaticss are prepared based on dark plum recovery rate is promoted |
| CN110747061A (en) * | 2019-11-12 | 2020-02-04 | 云南中烟新材料科技有限公司 | Smoked plum tobacco flavoring particle material and preparation method and application thereof |
| CN110747061B (en) * | 2019-11-12 | 2022-11-08 | 云南中烟新材料科技有限公司 | Smoked plum tobacco flavoring particle material and preparation method and application thereof |
| CN113974213A (en) * | 2021-12-06 | 2022-01-28 | 云南中烟工业有限责任公司 | Composite additive for reducing phenol release amount in smoke and preparation method and application thereof |
| CN113974213B (en) * | 2021-12-06 | 2024-06-25 | 云南中烟工业有限责任公司 | Composite additive for reducing release amount of phenol in flue gas, and preparation method and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102499460B (en) | 2013-09-04 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102499460B (en) | Extracting method for radix ophiopogonis extract and dark plum extract as well as cigarette containing radix ophiopogonis extract and dark plum extract | |
| CN101693745B (en) | Lucid ganoderma polysaccharide and extraction method thereof as well as cigarette containing lucid ganoderma polysaccharide and preparation method thereof | |
| CN103989244B (en) | A kind of Chinese style tobacco juice for electronic smoke and preparation method thereof | |
| CN102499435B (en) | Cigarette containing cordyceps militaris extract | |
| CN101361590B (en) | Use Chinese chive seed extract in cigarette | |
| CN101928352B (en) | Extraction for active ingredients of cordyceps sinensis and application thereof in cigarette filter | |
| CN105920977A (en) | Pure vegetal air disinfection purifying agent and preparing method thereof | |
| CN101692930B (en) | Cigarette containing wolfberry polysaccharide and preparation method thereof | |
| CN108029811A (en) | A kind of King solomonseal rhizome tea and its preparation process for improving smoking and people's constitution of drinking | |
| CN101692932B (en) | Cigarette containing tea polysaccharide and preparation method thereof | |
| KR101411944B1 (en) | Herbal tea and its manufacturing method | |
| CN103045370B (en) | Method for preparing cigarette essence containing aloe extractive and application of cigarette essence to cigarettes | |
| KR20130121324A (en) | Composition for preventing and treating hangover comprising extracts of leaves of perilla frutescens britton var | |
| CN101773297A (en) | Cypress essential oil and cigarette containing same | |
| CN105941714A (en) | Herbal tea beverage capable of clearing away heat and removing fire and preparation method of herbal tea beverage | |
| CN101928353A (en) | Extraction of cordyceps polysaccharide and application of cordyceps polysaccharide to cigarettes | |
| CN101653290A (en) | Cigarette containing rosmarinic acid and preparation method thereof | |
| CN106281714A (en) | A kind of characteristic Camellia nitidissima Chi tobacco aromatics using and preparation method and application | |
| CN107216947B (en) | Preparation method of catechu extract for cigarettes | |
| CN101862028B (en) | Wintergreen extraction method, preparation method of cigarette comprising wintergreen extract | |
| CN101692933A (en) | Cigarette containing lentinan and preparation method thereof | |
| CN112715709B (en) | Agilawood compound tea and preparation method thereof | |
| CN111642786B (en) | Chinese herbal medicine tea cigarette with epidemic prevention and health care effects and application thereof | |
| CN106418666B (en) | Additive for composite plant extract cigarette | |
| CN104997156A (en) | Tea cigarette and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| EE01 | Entry into force of recordation of patent licensing contract |
Application publication date: 20120620 Assignee: Dabaihui Industrial Group Co.,Ltd. Assignor: SHENZHEN DABAIHUI TECHNOLOGY Co.,Ltd. Contract record no.: X2021980011440 Denomination of invention: Extraction method of Ophiopogon japonicus mume extract and cigarette containing Ophiopogon japonicus mume extract Granted publication date: 20130904 License type: Common License Record date: 20211028 |
|
| EE01 | Entry into force of recordation of patent licensing contract |