CN102697170B - Aroma-increasing and humidity-preserving additive for cigarettes and preparation method and application thereof - Google Patents

Aroma-increasing and humidity-preserving additive for cigarettes and preparation method and application thereof Download PDF

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Publication number
CN102697170B
CN102697170B CN201210227599.3A CN201210227599A CN102697170B CN 102697170 B CN102697170 B CN 102697170B CN 201210227599 A CN201210227599 A CN 201210227599A CN 102697170 B CN102697170 B CN 102697170B
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moist
additive agent
keeping flavouring
eclipta
dandelion
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CN201210227599.3A
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Chinese (zh)
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CN102697170A (en
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吴彦
黄泰松
邹克兴
刘启斌
白家峰
陈志燕
李志华
潘连华
吴晶晶
胡志忠
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广西中烟工业有限责任公司
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Abstract

The invention discloses an aroma-increasing and humidity-preserving additive for cigarettes and a preparation method and application thereof. The additive contains a traditional Chinese medicine extract composition or a compound traditional Chinese medicine extract. The traditional Chinese medicine comprises epimedium, eclipta herb, coltsfoot flower, leonurus, dandelion and trichosanthes peels. The preparation method of the aroma-increasing and humidity-preserving additive comprises respectively using a solvent to extract and refine the epimedium, the eclipta herb, the coltsfoot flower, the leonurus, the dandelion and the trichosanthes peels and mixing the ingredients according to the proportion of 1-8:0.8-6:0.5-4:0.3-4:0.3-5:1 to prepare the aroma-increasing and humidity-preserving additive, or mixing the epimedium, the eclipta herb, the coltsfoot flower, the leonurus, the dandelion and the trichosanthes peels according to the proportion of 0.5-8:0.5-6:0.2-4:0.3-4:0.3-5:1 and then using the solvent to perform extraction and refining to prepare the aroma-increasing and humidity-preserving additive. The additive is added into tobacco shreds, cut stems and slices for cigarettes, and the adding proportion is 0.002-1%wt. After the additive is added into the tobacco shreds, the cut stems and the slices for the cigarettes, the moisture of the tobacco shreds can be maintained in the normal-temperature dry environment, the additive has good physical humidity-preserving effect and integrally improves the intrinsic quality of the cigarettes.

Description

A kind of moist-keeping flavouring additive agent for cigarette and its preparation method and application

Technical field

The present invention relates to cigarette additive and preparation and application field thereof, especially relate to and a kind ofly comprise Chinese medical extract combination or Chinese medicinal compound extract, there are natural cigarette additive and the preparation and application thereof of moist-keeping flavouring effect.

Background technology

Humectant refers to and puts in tobacco and can strengthen tobacco in tobacco product process, tobacco product performance of keeping humidity, increases flexibility, reduces broken material.Humectant can improve the physical property of blade and pipe tobacco, increases cigarette product toughness, elasticity and water retention property, reduces process loss in process.The polyhydroxy substances such as glycerine, propane diols, sorbierite, xylitol are mainly adopted to be humectant in current China cigarette industry, by the moisture in these material absorbing air to keep the wetting of pipe tobacco, but use the object of this type of humectant to be only to maintain the moisture content of pipe tobacco in process, improve the resist processing of pipe tobacco, then effect is not ideal to suck the improvement of comfort level for finished cigarettes.In addition this kind of humectant affects greatly by ambient temperature and humidity, glycerine and propane diols cost higher, although sorbierite and xylitol cost controlled, humectation effect is not as glycerine and propane diols.

China just starts the research and development carrying out Chinese medicine class natural plants additive cigarette from the middle of last century.Between many decades, researcher in industry reduces cigarette at Chinese herb feed additive and does a lot of work to harm field, as " a kind of less harmful tobacco containing plant extracts and preparation method thereof " (application number: 201110181597.0, publication number: CN102349697A), " a kind of cigarette harm reduction additive and preparation method thereof " (application number: 201110241463.3, publication number: CN102318896A) etc.In recent years, along with industry industrialized development is accelerated, moist area of southern China produces cigarette and sells increase in northern Arid Area, and humectant research and development cause higher attention, and the research adopting Chinese medicine class natural products to improve cigarette humid keeping performance should become study hotspot.

Summary of the invention

One of the object of the invention is to provide a kind of natural cigarette moist-keeping flavouring additive agent and application thereof.

Another object of the present invention, is the preparation method providing this natural cigarette moist-keeping flavouring additive agent.

According to an object of the present invention, technical scheme of the present invention is as follows:

A kind of cigarette moist-keeping flavouring additive agent, comprise traditional Chinese medicine extract composition or compound Chinese medicine extract, it is characterized in that: described traditional Chinese medicine extract composition or compound Chinese medicine extract comprise barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS.

The extract weight ratio of barrenwort in described traditional Chinese medicine extract composition, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS is 1-8: 0.8-6: 0.5-4: 0.3-4: 0.3-5: 1.

The part by weight of described compound Chinese medicine extract Raw medicine barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS is 0.5-8: 0.5-6: 0.2-4: 0.3-4: 0.3-5: 1.

As preferred embodiment, a kind of preparation method of cigarette moist-keeping flavouring additive agent, is characterized in that: carry out according to following steps:

Get barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS, extract separately after pulverizing, add 6-15 times amount pure water respectively, after soaking 2-48h, 65-100 DEG C of circumfluence distillation 1-3h, extracts 3 times altogether, merges No. 3 extracts, being concentrated into density under 60-80 DEG C, pressure 0.02-0.08Mpa condition is 1.12 ± 0.01 liquid extracts;

Subsequently, add 2 times of volume ethanol, leave standstill 24-96h, filtering-depositing, 60-80 DEG C, being concentrated into density under pressure 0.02-0.08Mpa condition is 1.12 ± 0.01 liquid extracts, is mixed by the liquid extract of barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS, filter and obtain moist-keeping flavouring additive agent by 1-8: 0.8-6: 0.5-4: 0.3-4: 0.3-5: 1.

As another kind of preferred embodiment, a kind of preparation method of cigarette moist-keeping flavouring additive agent, is characterized in that: carry out according to following steps:

Get barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS respectively, 0.5-8: 0.5-6: 0.2-4: 0.3-4: 0.3-5: 1 ratio uniform mixing is pressed after pulverizing, add 6-15 times amount pure water, after soaking 2-48h, 65-100 DEG C of circumfluence distillation 1-3h, extracts 3 times altogether, merges No. 3 extracts, being concentrated into density under 60-80 DEG C, pressure 0.02-0.08Mpa condition is 1.12 ± 0.01 liquid extracts;

Add 2 times of volume ethanol, leave standstill 24-96h, filtering-depositing, being concentrated into density under 60-80 DEG C, pressure 0.02-0.08Mpa condition is 1.12 ± 0.01 liquid extracts, filters, obtains moist-keeping flavouring additive agent.

For applying of large industry, the present invention also provides a kind of application of cigarette moist-keeping flavouring additive agent, it is characterized in that, gets appropriate moist-keeping flavouring additive agent, is dissolved in certain volume distilled water, is evenly sprayed on cigarette shreds, stem, thin slice.The consumption of moist-keeping flavouring additive agent is pipe tobacco, stem, the 0.002-1%wt of flake weight.

Compared with prior art, the present invention has following beneficial effect, this additive makes an addition to cigarette shreds, stem, after thin slice, under air drying environment, there is good moisture holding capacity, the moisture content of tobacco sample can be improved, scattering and disappearing of moisture can be slowed down, reduce the percentage of water loss of pipe tobacco, play the effect maintaining moisture in cut tobacco, there is good physics humectation effect; Obviously can also promote perfume quantity, improve harmony, improve pleasant impression, reduce assorted gas and excitant, increase and promote the production of body fluid sense and return sweet sense, Integral lifting cigarette comfort level.And equipment is simple, and extraction process is simple, and cost is controlled, and raw material is easy to get.

Accompanying drawing explanation

Above-mentioned and/or additional aspect of the present invention and advantage will become obvious and easy understand from the following description of the accompanying drawings of embodiments, wherein:

Fig. 1 is under air drying condition, containing pipe tobacco and the blank pipe tobacco (blank) of moist-keeping flavouring agent, containing propane diols pipe tobacco (contrast) moisture content changing trend diagram in time;

Fig. 2 is under air drying condition, containing pipe tobacco and the blank pipe tobacco (blank) of moist-keeping flavouring agent, containing propane diols pipe tobacco (contrast) percentage of water loss changing trend diagram in time.

Detailed description of the invention

Embodiments of the invention are described below in detail.Being exemplary below by the embodiment be described with reference to the drawings, only for explaining the present invention, and can not limitation of the present invention being interpreted as.

Experimental example:

One, humectation effect assessment

1. test purpose

Contrast under equal conditions, containing pipe tobacco and the blank pipe tobacco (blank) of moist-keeping flavouring agent, the physics humectation effect containing propane diols pipe tobacco (contrast).

2. test sample

Moist-keeping flavouring agent: 1% moist-keeping flavouring agent+middle-grade blank pipe tobacco

Contrast: 1% propane diols+middle-grade blank pipe tobacco

Blank: middle-grade blank pipe tobacco

3. method of testing

3.1 equilibrium process: three of test experiments groups of samples are placed in temperature: (22 ± 1) DEG C, humidity: balance 48 hours in the climatic chamber of (60 ± 3) %, measure the initial water content of three groups of test samples by Oven Method, be the moisture content of 0h.

3.2 test process: be temperature by climatic chamber Environmental adjustments: (22 ± 1) DEG C, humidity: (40 ± 3) %, be placed in one by three groups of test samples, separated in time weighs an example weight, and calculates its instant moisture content according to example weight now.

4. test result

Moisture content and percentage of water loss in time limit breathe out tendency chart analysis: see attached Fig. 1 and 2.

Fig. 1 contains the pipe tobacco of moist-keeping flavouring agent with blank pipe tobacco (blank), containing propane diols pipe tobacco (contrast) moisture content changing trend diagram in time

Be the moisture-time test curve of air drying condition under Figure 1 shows that test condition, curve shows, and when 0-20h, moist-keeping flavouring agent, blank, the violent dehydration of contrast, moisture is downward trend linearly.After 24h, both moisture content curves tend towards stability, and this means, after 24h, both reach the absorption equilibrium of moisture in the present context, compare from moisture content at this moment, and moist-keeping flavouring agent > is blank.Visible, in the environment of air drying, moist-keeping flavouring agent has certain moisture holding capacity, can improve the moisture content of tobacco sample.

Fig. 2 contains the pipe tobacco of moist-keeping flavouring agent with blank pipe tobacco (blank), containing propane diols pipe tobacco (contrast) percentage of water loss changing trend diagram in time.

As shown in Figure 2, percentage of water loss refers within certain period, the fluid loss of sample and the ratio of initial moisture, the fluid loss/initial moisture of n hour percentage of water loss=n hour.In 24 hours, the percentage of water loss change of 3 groups of samples is violent.Because sample is positioned in dry environment, what first lose is the free state moisture on pipe tobacco surface, and therefore the speed of moisture loss is very fast.In the prolongation along with equilibration time after 48 hours, percentage of water loss is tending towards constant.The situation of percentage of water loss change after 48 hours, blank > moist-keeping flavouring agent=contrast.The contrast percentage of water loss DATA POPULATION later from 48h be it seems, under air drying environment, moist-keeping flavouring agent can delay sample moisture loss, delays moisture loss speed.

In sum, moist-keeping flavouring agent can be played and slow down scattering and disappearing of moisture in air drying environment, reduces the percentage of water loss of pipe tobacco, plays the effect maintaining moisture in cut tobacco.

Two. effect assessment of smokeing panel test

Get the agent of finished product moist-keeping flavouring, respectively according to 0.005%, 0.01%, 0.02% makes an addition on high, medium and low Virginian-type cigarette leaf group pipe tobacco, after room temperature places 2h in sealing bag, is rolled into cigarette with on CMB120 cigarette machine, in the wet tank inner equilibrium 48h of 22 DEG C ± 1 DEG C and RH60% ± 2%, organize the committee expert that originally smokes panel test to smoke panel test, expert totally 7, is provincial judging panel.

Result shows, after moist-keeping flavouring agent makes an addition to cigarette leaf group, effectively can increase the perfume quantity of cigarette, improve aroma quality and harmony, reduce assorted gas and excitant, increase sweet sense, make pleasant impression cleaner, comfortable, the Integral lifting interior quality of cigarette, especially in low and middle-grade cigarette, effect is more obvious.Smoking result is in table 2.

The agent of table 2. moist-keeping flavouring makes an addition to the smoking result after cigarette

Embodiment one

Get barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS respectively, by 0.5: 0.5: 0.2: 0.3: 0.3: 1 ratio uniform mixing after pulverizing, add 8 times amount pure water, after soaking 2h, 75 DEG C of circumfluence distillation 1h, extract 3 times altogether, merge No. 3 extracts, 80 DEG C, being concentrated into density under pressure 0.02Mpa condition is 1.12 liquid extracts.Add 2 times of volume ethanol, leave standstill 24h, filtering-depositing, 80 DEG C, being concentrated into density under pressure 0.02Mpa condition is 1.12 liquid extracts, filters, obtains moist-keeping flavouring additive agent.Get additive 10g, be dissolved in 20kg distilled water, after being sprayed on 500kg pipe tobacco, roll into cigarette.

Embodiment two

Get barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS respectively, by 1: 0.8: 0.5: 0.5: 0.5: 1 ratio uniform mixing after pulverizing, add 6 times amount pure water, after soaking 6h, 70 DEG C of circumfluence distillation 1.5h, extract 3 times altogether, merge No. 3 extracts, 75 DEG C, being concentrated into density under pressure 0.06Mpa condition is 1.11 liquid extracts.Add 2 times of volume ethanol, leave standstill 36h, filtering-depositing, 75 DEG C, being concentrated into density under pressure 0.06Mpa condition is 1.11 liquid extracts, filters, obtains moist-keeping flavouring additive agent.Get additive 50g, be dissolved in 20kg distilled water, after being sprayed on 500kg pipe tobacco, roll into cigarette.

Embodiment three

Get barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS respectively, by 1.5: 1: 1: 1.5: 1.5: 1 ratio uniform mixing after pulverizing, add 10 times amount pure water, after soaking 12h, 65 DEG C of circumfluence distillation 1.5h, extract 3 times altogether, merge No. 3 extracts, 70 DEG C, being concentrated into density under pressure 0.03Mpa condition is 1.13 liquid extracts.Add 2 times of volume ethanol, leave standstill 48h, filtering-depositing, 70 DEG C, being concentrated into density under pressure 0.03Mpa condition is 1.13 liquid extracts, filters, obtains moist-keeping flavouring additive agent.Get additive 100g, be dissolved in 20kg distilled water, after being sprayed on 500kg pipe tobacco, roll into cigarette.

Embodiment four

Get barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS respectively, by 2: 1.5: 1: 1: 1: 1 ratio uniform mixing after pulverizing, add 12 times amount pure water, after soaking 24h, 90 DEG C of circumfluence distillation 2h, extract 3 times altogether, merge No. 3 extracts, 65 DEG C, being concentrated into density under pressure 0.05Mpa condition is 1.12 liquid extracts.Add 2 times of volume ethanol, leave standstill 72h, filtering-depositing, 65 DEG C, being concentrated into density under pressure 0.05Mpa condition is 1.12 liquid extracts, filters, obtains moist-keeping flavouring additive agent.Get additive 500g, be dissolved in 20kg distilled water, after being sprayed on 500kg pipe tobacco, roll into cigarette.

Embodiment five

Get barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS respectively, by 4: 3: 2: 2: 2: 1 ratio uniform mixing after pulverizing, add 13 times amount pure water, after soaking 36h, 80 DEG C of circumfluence distillation 2.5h, extract 3 times altogether, merge No. 3 extracts, 75 DEG C, being concentrated into density under pressure 0.04Mpa condition is 1.12 liquid extracts.Add 2 times of volume ethanol, leave standstill 72h, filtering-depositing, 75 DEG C, being concentrated into density under pressure 0.04Mpa condition is 1.12 liquid extracts, filters, obtains moist-keeping flavouring additive agent.Get additive 1kg, be dissolved in 20kg distilled water, after being sprayed on 500kg pipe tobacco, roll into cigarette.

Embodiment six

Get barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS respectively, by 8: 6: 4: 4: 5: 1 ratio uniform mixing after pulverizing, add 15 times amount pure water, after soaking 48h, 100 DEG C of circumfluence distillation 3h, extract 3 times altogether, merge No. 3 extracts, 60 DEG C, being concentrated into density under pressure 0.06Mpa condition is 1.13 liquid extracts.Add 2 times of volume ethanol, leave standstill 96h, filtering-depositing, 60 DEG C, being concentrated into density under pressure 0.06Mpa condition is 1.13 liquid extracts, filters, obtains moist-keeping flavouring additive agent.Get additive 5kg, be dissolved in 20kg distilled water, after being sprayed on 500kg pipe tobacco, roll into cigarette.

Embodiment seven

Get barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS, extract separately after pulverizing, add 8 times amount pure water respectively, after soaking 6h, 70 DEG C of circumfluence distillation 1h, extract 3 times altogether, merge No. 3 extracts, 70 DEG C, being concentrated into density under pressure 0.05Mpa condition is 1.13 liquid extracts.Add 2 times of volume ethanol, leave standstill 24h, filtering-depositing, 70 DEG C, being concentrated into density under pressure 0.05Mpa condition is 1.13 liquid extracts, the liquid extract of barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS is mixed by 1: 0.8: 0.5: 0.3: 0.3: 1, filters and obtain moist-keeping flavouring additive agent.Get additive 10g, be dissolved in 20kg distilled water, after being sprayed on 500kg pipe tobacco, roll into cigarette.

Embodiment eight

Get barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS, extract separately after pulverizing, add 10 times amount pure water respectively, after soaking 12h, 80 DEG C of circumfluence distillation 1.5h, extract 3 times altogether, merge No. 3 extracts, 75 DEG C, being concentrated into density under pressure 0.08Mpa condition is 1.12 liquid extracts.Add 2 times of volume ethanol, leave standstill 36h, filtering-depositing, 75 DEG C, being concentrated into density under pressure 0.08Mpa condition is 1.12 liquid extracts, the liquid extract of barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS is mixed by 2: 1.5: 1.5: 1: 1: 1, filters and obtain moist-keeping flavouring additive agent.Get additive 50g, be dissolved in 20kg distilled water, after being sprayed on 500kg pipe tobacco, roll into cigarette.

Embodiment nine

Get barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS, extract separately after pulverizing, add 12 times amount pure water respectively, after soaking 18h, 85 DEG C of circumfluence distillation 2h, extract 3 times altogether, merge No. 3 extracts, 80 DEG C, being concentrated into density under pressure 0.02Mpa condition is 1.12 liquid extracts.Add 2 times of volume ethanol, leave standstill 48h, filtering-depositing, 80 DEG C, being concentrated into density under pressure 0.02Mpa condition is 1.12 liquid extracts, the liquid extract of barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS is mixed by 3: 2: 2: 2: 1.5: 1, filters and obtain moist-keeping flavouring additive agent.Get additive 100g, be dissolved in 20kg distilled water, after being sprayed on 500kg pipe tobacco, roll into cigarette.

Embodiment ten

Get barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS, extract separately after pulverizing, add 6 times amount pure water respectively, after soaking 24h, 90 DEG C of circumfluence distillation 2.5h, extract 3 times altogether, merge No. 3 extracts, 65 DEG C, being concentrated into density under pressure 0.04Mpa condition is 1.12 liquid extracts.Add 2 times of volume ethanol, leave standstill 60h, filtering-depositing, 65 DEG C, being concentrated into density under pressure 0.04Mpa condition is 1.12 liquid extracts, the liquid extract of barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS is mixed by 4: 3: 2: 2: 1.5: 1, filters and obtain moist-keeping flavouring additive agent.Get additive 500g, be dissolved in 20kg distilled water, after being sprayed on 500kg pipe tobacco, roll into cigarette.

Embodiment 11

Get barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS, extract separately after pulverizing, add 10 times amount pure water respectively, after soaking 36h, 65 DEG C of circumfluence distillation 3h, extract 3 times altogether, merge No. 3 extracts, 60 DEG C, being concentrated into density under pressure 0.06Mpa condition is 1.12 liquid extracts.Add 2 times of volume ethanol, leave standstill 72h, filtering-depositing, 60 DEG C, being concentrated into density under pressure 0.06Mpa condition is 1.12 liquid extracts, the liquid extract of barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS is mixed by 6: 5: 4: 3: 2: 1, filters and obtain moist-keeping flavouring additive agent.Get additive 1kg, be dissolved in 20kg distilled water, after being sprayed on 500kg pipe tobacco, roll into cigarette.

Embodiment 12

Get barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS, extract separately after pulverizing, add 15 times amount pure water respectively, after soaking 48h, 100 DEG C of circumfluence distillation 3h, extract 3 times altogether, merge No. 3 extracts, 80 DEG C, being concentrated into density under pressure 0.03Mpa condition is 1.13 liquid extracts.Add 2 times of volume ethanol, leave standstill 96h, filtering-depositing, 80 DEG C, being concentrated into density under pressure 0.03Mpa condition is 1.13 liquid extracts, the liquid extract of barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS is mixed by 8: 6: 4: 4: 5: 1, filters and obtain moist-keeping flavouring additive agent.Get additive 5kg, be dissolved in 20kg distilled water, after being sprayed on 500kg pipe tobacco, roll into cigarette.

Claims (6)

1. the moist-keeping flavouring additive agent for cigarette, comprise traditional Chinese medicine extract composition or compound Chinese medicine extract, it is characterized in that: described traditional Chinese medicine extract composition or compound Chinese medicine extract comprise barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS;
The extract weight ratio of barrenwort in wherein said traditional Chinese medicine extract composition, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS is 1-8:0.8-6:0.5-4:0.3-4:0.3-5:1;
The part by weight of described compound Chinese medicine extract Raw medicine barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS is 0.5-8:0.5-6:0.2-4:0.3-4:0.3-5:1.
2. the preparation method of a kind of moist-keeping flavouring additive agent for cigarette according to claim 1, is characterized in that: carry out according to following steps:
Get barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS, extract separately after pulverizing, add 6-15 times amount pure water respectively, after soaking 2-48h, 65-100 DEG C of circumfluence distillation 1-3h, extracts 3 times altogether, merges No. 3 extracts, being concentrated into density under 60-80 DEG C, pressure 0.02-0.08Mpa condition is 1.12 ± 0.01 liquid extracts;
Subsequently, add 2 times of volume ethanol, leave standstill 24-96h, filtering-depositing, 60-80 DEG C, being concentrated into density under pressure 0.02-0.08Mpa condition is 1.12 ± 0.01 liquid extracts, is mixed in proportion by the liquid extract of barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS, filters and obtain moist-keeping flavouring additive agent.
3. the preparation method of a kind of moist-keeping flavouring additive agent for cigarette according to claim 1, is characterized in that: carry out according to following steps:
Get barrenwort, eclipta, tussilago, motherwort, dandelion and PERICARPIUM TRICHOSANTHIS respectively, Homogeneous phase mixing in proportion after pulverizing, add 6-15 times amount pure water, after soaking 2-48h, 65-100 DEG C of circumfluence distillation 1-3h, extracts 3 times altogether, merges No. 3 extracts, being concentrated into density under 60-80 DEG C, pressure 0.02-0.08Mpa condition is 1.12 ± 0.01 liquid extracts;
Add 2 times of volume ethanol, leave standstill 24-96h, filtering-depositing, being concentrated into density under 60-80 DEG C, pressure 0.02-0.08Mpa condition is 1.12 ± 0.01 liquid extracts, filters, obtains moist-keeping flavouring additive agent.
4. the application of a kind of moist-keeping flavouring additive agent for cigarette according to claim 1, is characterized in that, get appropriate moist-keeping flavouring additive agent, be dissolved in certain volume distilled water, be evenly sprayed on cigarette shreds, stem, thin slice; The consumption of moist-keeping flavouring additive agent is pipe tobacco, stem, the 0.002-1%wt of flake weight.
5. the application of moist-keeping flavouring additive agent for preparing of preparation method according to claim 2, is characterized in that, get appropriate moist-keeping flavouring additive agent, be dissolved in certain volume distilled water, be evenly sprayed on cigarette shreds, stem, thin slice; The consumption of moist-keeping flavouring additive agent is pipe tobacco, stem, the 0.002-1%wt of flake weight.
6. the application of moist-keeping flavouring additive agent for preparing of preparation method according to claim 3, is characterized in that, get appropriate moist-keeping flavouring additive agent, be dissolved in certain volume distilled water, be evenly sprayed on cigarette shreds, stem, thin slice; The consumption of moist-keeping flavouring additive agent is pipe tobacco, stem, the 0.002-1%wt of flake weight.
CN201210227599.3A 2012-07-02 2012-07-02 Aroma-increasing and humidity-preserving additive for cigarettes and preparation method and application thereof CN102697170B (en)

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