CN101774603B - 一种介孔硼酸镁微球的制备方法 - Google Patents
一种介孔硼酸镁微球的制备方法 Download PDFInfo
- Publication number
- CN101774603B CN101774603B CN 201010108792 CN201010108792A CN101774603B CN 101774603 B CN101774603 B CN 101774603B CN 201010108792 CN201010108792 CN 201010108792 CN 201010108792 A CN201010108792 A CN 201010108792A CN 101774603 B CN101774603 B CN 101774603B
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- Prior art keywords
- magnesium
- preparation
- mesoporous
- borax
- hours
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- NFMWFGXCDDYTEG-UHFFFAOYSA-N trimagnesium;diborate Chemical compound [Mg+2].[Mg+2].[Mg+2].[O-]B([O-])[O-].[O-]B([O-])[O-] NFMWFGXCDDYTEG-UHFFFAOYSA-N 0.000 title claims abstract description 36
- 239000004005 microsphere Substances 0.000 title claims abstract description 29
- 238000002360 preparation method Methods 0.000 title claims abstract description 25
- 159000000003 magnesium salts Chemical class 0.000 claims abstract description 28
- 229910021538 borax Inorganic materials 0.000 claims abstract description 22
- 235000010339 sodium tetraborate Nutrition 0.000 claims abstract description 22
- 239000004328 sodium tetraborate Substances 0.000 claims abstract description 22
- 230000032683 aging Effects 0.000 claims abstract description 11
- 235000011114 ammonium hydroxide Nutrition 0.000 claims abstract description 10
- 238000000034 method Methods 0.000 claims abstract description 8
- 238000006243 chemical reaction Methods 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 3
- 238000002156 mixing Methods 0.000 claims abstract 4
- 239000000243 solution Substances 0.000 claims description 24
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical group [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims description 18
- 239000004141 Sodium laurylsulphate Substances 0.000 claims description 18
- 235000019333 sodium laurylsulphate Nutrition 0.000 claims description 18
- 238000005406 washing Methods 0.000 claims description 14
- YIXJRHPUWRPCBB-UHFFFAOYSA-N magnesium nitrate Chemical group [Mg+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O YIXJRHPUWRPCBB-UHFFFAOYSA-N 0.000 claims description 12
- 239000000706 filtrate Substances 0.000 claims description 11
- 230000007935 neutral effect Effects 0.000 claims description 11
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 claims description 10
- 238000003483 aging Methods 0.000 claims description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 9
- 239000012065 filter cake Substances 0.000 claims description 9
- 238000001354 calcination Methods 0.000 claims description 6
- 238000001035 drying Methods 0.000 claims description 6
- 239000012266 salt solution Substances 0.000 claims description 6
- 239000007864 aqueous solution Substances 0.000 claims description 5
- 229910001629 magnesium chloride Inorganic materials 0.000 claims description 5
- 238000000151 deposition Methods 0.000 claims description 4
- 230000008021 deposition Effects 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- 206010013786 Dry skin Diseases 0.000 claims description 3
- RCEAADKTGXTDOA-UHFFFAOYSA-N OS(O)(=O)=O.CCCCCCCCCCCC[Na] Chemical compound OS(O)(=O)=O.CCCCCCCCCCCC[Na] RCEAADKTGXTDOA-UHFFFAOYSA-N 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims description 2
- 239000007788 liquid Substances 0.000 claims description 2
- 239000011777 magnesium Substances 0.000 claims description 2
- 239000012716 precipitator Substances 0.000 claims description 2
- 238000000967 suction filtration Methods 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 11
- 239000013078 crystal Substances 0.000 abstract description 3
- 238000005516 engineering process Methods 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 12
- 239000000463 material Substances 0.000 description 12
- 238000013019 agitation Methods 0.000 description 10
- 239000000047 product Substances 0.000 description 7
- 238000003795 desorption Methods 0.000 description 6
- 238000002386 leaching Methods 0.000 description 6
- 229910052757 nitrogen Inorganic materials 0.000 description 6
- 239000011148 porous material Substances 0.000 description 6
- 238000001556 precipitation Methods 0.000 description 6
- 235000012970 cakes Nutrition 0.000 description 5
- 229960000935 dehydrated alcohol Drugs 0.000 description 5
- 239000012153 distilled water Substances 0.000 description 5
- 235000021463 dry cake Nutrition 0.000 description 5
- 239000000843 powder Substances 0.000 description 5
- 239000002244 precipitate Substances 0.000 description 5
- 238000010792 warming Methods 0.000 description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 239000013543 active substance Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000005229 chemical vapour deposition Methods 0.000 description 1
- 238000013375 chromatographic separation Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000001027 hydrothermal synthesis Methods 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000011147 inorganic material Substances 0.000 description 1
- 239000010687 lubricating oil Substances 0.000 description 1
- 238000003836 solid-state method Methods 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 239000012745 toughening agent Substances 0.000 description 1
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Abstract
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Priority Applications (1)
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CN 201010108792 CN101774603B (zh) | 2010-02-07 | 2010-02-07 | 一种介孔硼酸镁微球的制备方法 |
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CN 201010108792 CN101774603B (zh) | 2010-02-07 | 2010-02-07 | 一种介孔硼酸镁微球的制备方法 |
Publications (2)
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CN101774603A CN101774603A (zh) | 2010-07-14 |
CN101774603B true CN101774603B (zh) | 2013-04-17 |
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CN 201010108792 Expired - Fee Related CN101774603B (zh) | 2010-02-07 | 2010-02-07 | 一种介孔硼酸镁微球的制备方法 |
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CN (1) | CN101774603B (zh) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102633274A (zh) * | 2011-02-15 | 2012-08-15 | 长春理工大学 | Mg2B2O5一维纳米棒的两步制备法 |
CN104140112B (zh) * | 2014-08-14 | 2016-06-01 | 曲阜师范大学 | 一种微球状多孔碱式硼酸镁及硼酸镁纳米超结构的离子热合成方法 |
CN105399108B (zh) * | 2015-12-21 | 2017-09-26 | 浙江工业大学 | 可见光响应具有介孔结构Cu3B2O6的制备方法 |
CN107855096B (zh) * | 2017-11-20 | 2020-07-28 | 陕西师范大学 | 一种复盐相转化制备多级孔花球状纳米结构7MgO·2B2O3·7H2O的方法 |
-
2010
- 2010-02-07 CN CN 201010108792 patent/CN101774603B/zh not_active Expired - Fee Related
Non-Patent Citations (1)
Title |
---|
张光宇.纳米硼酸镁微粒的合成及其减摩性能的研究.《中国优秀博硕士学位论文全文数据库(硕士) 工程科技I辑》.2006,(第10期),全文. * |
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CN101774603A (zh) | 2010-07-14 |
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Effective date of registration: 20191225 Address after: 314400 No.2, Fengshou Avenue, Haining warp knitting industrial park, Jiaxing City, Zhejiang Province Patentee after: Zhejiang Haining Warp Knitting Industrial Park Development Co.,Ltd. Address before: 510000 unit 2414-2416, building, No. five, No. 371, Tianhe District, Guangdong, China Patentee before: GUANGDONG GAOHANG INTELLECTUAL PROPERTY OPERATION Co.,Ltd. Effective date of registration: 20191225 Address after: 510000 unit 2414-2416, building, No. five, No. 371, Tianhe District, Guangdong, China Patentee after: GUANGDONG GAOHANG INTELLECTUAL PROPERTY OPERATION Co.,Ltd. Address before: Hangzhou City, Zhejiang province 310014 City Zhaohui District Six Patentee before: Zhejiang University of Technology |
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Granted publication date: 20130417 Termination date: 20200207 |
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