CN101390583B - 从棉子粕中提取棉子糖的方法 - Google Patents
从棉子粕中提取棉子糖的方法 Download PDFInfo
- Publication number
- CN101390583B CN101390583B CN2007101218668A CN200710121866A CN101390583B CN 101390583 B CN101390583 B CN 101390583B CN 2007101218668 A CN2007101218668 A CN 2007101218668A CN 200710121866 A CN200710121866 A CN 200710121866A CN 101390583 B CN101390583 B CN 101390583B
- Authority
- CN
- China
- Prior art keywords
- raffinose
- cotton seed
- rice
- seed dregs
- extracting
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- MUPFEKGTMRGPLJ-ZQSKZDJDSA-N raffinose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO[C@@H]2[C@@H]([C@@H](O)[C@@H](O)[C@@H](CO)O2)O)O1 MUPFEKGTMRGPLJ-ZQSKZDJDSA-N 0.000 title claims abstract description 77
- 229920000742 Cotton Polymers 0.000 title claims abstract description 56
- 238000000034 method Methods 0.000 title claims abstract description 51
- 235000012054 meals Nutrition 0.000 title abstract 4
- MUPFEKGTMRGPLJ-RMMQSMQOSA-N Raffinose Natural products O(C[C@H]1[C@@H](O)[C@H](O)[C@@H](O)[C@@H](O[C@@]2(CO)[C@H](O)[C@@H](O)[C@@H](CO)O2)O1)[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 MUPFEKGTMRGPLJ-RMMQSMQOSA-N 0.000 claims abstract description 76
- MUPFEKGTMRGPLJ-UHFFFAOYSA-N UNPD196149 Natural products OC1C(O)C(CO)OC1(CO)OC1C(O)C(O)C(O)C(COC2C(C(O)C(O)C(CO)O2)O)O1 MUPFEKGTMRGPLJ-UHFFFAOYSA-N 0.000 claims abstract description 76
- 238000002425 crystallisation Methods 0.000 claims abstract description 25
- 230000008025 crystallization Effects 0.000 claims abstract description 25
- 239000013078 crystal Substances 0.000 claims abstract description 24
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000012141 concentrate Substances 0.000 claims abstract description 5
- 241000209094 Oryza Species 0.000 claims description 52
- 235000007164 Oryza sativa Nutrition 0.000 claims description 52
- 235000009566 rice Nutrition 0.000 claims description 52
- 238000002955 isolation Methods 0.000 claims description 12
- 238000001953 recrystallisation Methods 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract description 10
- 239000000284 extract Substances 0.000 abstract description 10
- 238000011084 recovery Methods 0.000 abstract description 3
- 239000007788 liquid Substances 0.000 abstract 3
- 238000001816 cooling Methods 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 238000002791 soaking Methods 0.000 abstract 1
- 239000000047 product Substances 0.000 description 9
- 238000002360 preparation method Methods 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 3
- 235000016068 Berberis vulgaris Nutrition 0.000 description 2
- 241000335053 Beta vulgaris Species 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 241000193830 Bacillus <bacterium> Species 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 238000013375 chromatographic separation Methods 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 210000000936 intestine Anatomy 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
Landscapes
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
Description
Claims (9)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2007101218668A CN101390583B (zh) | 2007-09-17 | 2007-09-17 | 从棉子粕中提取棉子糖的方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2007101218668A CN101390583B (zh) | 2007-09-17 | 2007-09-17 | 从棉子粕中提取棉子糖的方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101390583A CN101390583A (zh) | 2009-03-25 |
| CN101390583B true CN101390583B (zh) | 2011-08-10 |
Family
ID=40491247
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2007101218668A Active CN101390583B (zh) | 2007-09-17 | 2007-09-17 | 从棉子粕中提取棉子糖的方法 |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101390583B (zh) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105693783B (zh) * | 2016-01-23 | 2018-10-23 | 内蒙古昶辉生物科技股份有限公司 | 一种从棉子粕中提取棉子糖的制备方法 |
| CN106967129A (zh) * | 2017-03-24 | 2017-07-21 | 合肥云都棉花有限公司 | 一种棉籽糖的提取方法 |
| CN106967130A (zh) * | 2017-03-24 | 2017-07-21 | 合肥云都棉花有限公司 | 一种从棉籽粕中提取棉籽糖的方法 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU993946A1 (ru) * | 1981-04-17 | 1983-02-07 | Ордена Трудового Красного Знамени Институт Химии Растительных Веществ Ан Узсср | Способ получени раффинозы |
| US6224684B1 (en) * | 1997-09-12 | 2001-05-01 | Nippon Tensaiseito Kabushiki Kaisha | Method for preparing raffinose crystals and equipment for the same |
-
2007
- 2007-09-17 CN CN2007101218668A patent/CN101390583B/zh active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU993946A1 (ru) * | 1981-04-17 | 1983-02-07 | Ордена Трудового Красного Знамени Институт Химии Растительных Веществ Ан Узсср | Способ получени раффинозы |
| US6224684B1 (en) * | 1997-09-12 | 2001-05-01 | Nippon Tensaiseito Kabushiki Kaisha | Method for preparing raffinose crystals and equipment for the same |
Non-Patent Citations (4)
| Title |
|---|
| 杨寿清.天然功能性活性因子——棉籽糖.《冷饮与速冻食品工业》.2002,第8卷(第3期),42－44. * |
| 袁美兰等.功能性低聚糖-棉籽糖的开发应用现状.《中国食品添加剂》.2002,(第4期),54-57. * |
| 詹少春等.用乙醇-水从双液相棉粕中提取棉子糖的研究.《南京工业大学学报(自然科学版)》.2006,第28卷(第1期),46－49. * |
| 金青哲等.棉籽糖提取液的脱色与棉酚去除.《中国油脂》.2005,第30卷(第4期),47-49. * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101390583A (zh) | 2009-03-25 |
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Application publication date: 20090325 Assignee: Kailu Zhaohui Biotechnology Co.,Ltd. Assignor: Bai Xinliang Contract record no.: 2012990000603 Denomination of invention: Method for extracting gossypose from cotton seed meal Granted publication date: 20110810 License type: Exclusive License Record date: 20120820 |
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Owner name: INNER MONGOLIA XINJILI BIOTECHNOLOGY CO., LTD. Free format text: FORMER OWNER: BAI XINLIANG Effective date: 20140709 |
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Effective date of registration: 20140709 Address after: 602, room 3, unit 7, B District, Wanda Plaza, Xinhua East Street, Xincheng District, the Inner Mongolia Autonomous Region, Hohhot, 010010 Patentee after: INNER MONGOLIA SCI-GEELY BIOTECHNOLOGY CO.,LTD. Address before: 028400 Tongliao city the Inner Mongolia Autonomous Region Kailu County Gongnong Street No. 1 Patentee before: Bai Xinliang |
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Address after: 602, room 3, unit 7, B District, Wanda Plaza, Xinhua East Street, Xincheng District, the Inner Mongolia Autonomous Region, Hohhot, 010010 Patentee after: INNER MONGOLIA CHANGHUI BIOLOGICAL TECHNOLOGY Co.,Ltd. Address before: 602, room 3, unit 7, B District, Wanda Plaza, Xinhua East Street, Xincheng District, the Inner Mongolia Autonomous Region, Hohhot, 010010 Patentee before: INNER MONGOLIA SCI-GEELY BIOTECHNOLOGY CO.,LTD. |
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Address after: 602, room 3, unit 7, B District, Wanda Plaza, Xinhua East Street, Xincheng District, the Inner Mongolia Autonomous Region, Hohhot, 010010 Patentee after: INNER MONGOLIA CHANGHUI BIOTECHNOLOGY CO.,LTD. Address before: 602, room 3, unit 7, B District, Wanda Plaza, Xinhua East Street, Xincheng District, the Inner Mongolia Autonomous Region, Hohhot, 010010 Patentee before: INNER MONGOLIA CHANGHUI BIOLOGICAL TECHNOLOGY Co.,Ltd. |
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Address after: 028400 no.0427, Dongjiao Industrial Park, Kailu Town, Kailu County, Tongliao City, Inner Mongolia Autonomous Region Patentee after: INNER MONGOLIA CHANGHUI BIOTECHNOLOGY CO.,LTD. Address before: 602, room 3, unit 7, B District, Wanda Plaza, Xinhua East Street, Xincheng District, the Inner Mongolia Autonomous Region, Hohhot, 010010 Patentee before: INNER MONGOLIA CHANGHUI BIOTECHNOLOGY CO.,LTD. |
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Denomination of invention: Method of extracting raffinose from cottonseed meal Effective date of registration: 20230307 Granted publication date: 20110810 Pledgee: China Minsheng Banking Corp Hohhot branch Pledgor: INNER MONGOLIA CHANGHUI BIOTECHNOLOGY CO.,LTD. Registration number: Y2023150000031 |
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Date of cancellation: 20231031 Granted publication date: 20110810 Pledgee: China Minsheng Banking Corp Hohhot branch Pledgor: INNER MONGOLIA CHANGHUI BIOTECHNOLOGY CO.,LTD. Registration number: Y2023150000031 |
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Denomination of invention: Method for extracting raffinose from cottonseed meal Effective date of registration: 20231101 Granted publication date: 20110810 Pledgee: China Minsheng Banking Corp Hohhot branch Pledgor: INNER MONGOLIA CHANGHUI BIOTECHNOLOGY CO.,LTD. Registration number: Y2023150000154 |
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