CN101346340B - 碳酸二烷基酯的工业分离方法 - Google Patents
碳酸二烷基酯的工业分离方法 Download PDFInfo
- Publication number
- CN101346340B CN101346340B CN2006800492531A CN200680049253A CN101346340B CN 101346340 B CN101346340 B CN 101346340B CN 2006800492531 A CN2006800492531 A CN 2006800492531A CN 200680049253 A CN200680049253 A CN 200680049253A CN 101346340 B CN101346340 B CN 101346340B
- Authority
- CN
- China
- Prior art keywords
- distillation column
- formula
- carbonate
- dialkyl carbonate
- aliphatic monohydric
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C68/00—Preparation of esters of carbonic or haloformic acids
- C07C68/06—Preparation of esters of carbonic or haloformic acids from organic carbonates
- C07C68/065—Preparation of esters of carbonic or haloformic acids from organic carbonates from alkylene carbonates
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C68/00—Preparation of esters of carbonic or haloformic acids
- C07C68/06—Preparation of esters of carbonic or haloformic acids from organic carbonates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/32—Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B63/00—Purification; Separation; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C68/00—Preparation of esters of carbonic or haloformic acids
- C07C68/08—Purification; Separation; Stabilisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
- C07C69/96—Esters of carbonic or haloformic acids
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP371643/2005 | 2005-12-26 | ||
| JP2005371643 | 2005-12-26 | ||
| PCT/JP2006/325089 WO2007074664A1 (ja) | 2005-12-26 | 2006-12-15 | ジアルキルカーボネートの工業的分離方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101346340A CN101346340A (zh) | 2009-01-14 |
| CN101346340B true CN101346340B (zh) | 2012-03-28 |
Family
ID=38217884
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2006800492531A Active CN101346340B (zh) | 2005-12-26 | 2006-12-15 | 碳酸二烷基酯的工业分离方法 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US8049028B2 (enExample) |
| EP (1) | EP1967508B1 (enExample) |
| JP (1) | JP4260212B2 (enExample) |
| KR (1) | KR101002863B1 (enExample) |
| CN (1) | CN101346340B (enExample) |
| BR (1) | BRPI0620605B1 (enExample) |
| EA (1) | EA012062B1 (enExample) |
| IN (1) | IN2008KN00869A (enExample) |
| TW (1) | TWI314549B (enExample) |
| WO (1) | WO2007074664A1 (enExample) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EA012516B1 (ru) * | 2005-11-25 | 2009-10-30 | Асахи Касеи Кемикалз Корпорейшн | Способ промышленного получения диалкилкарбоната и диола |
| TWI334410B (en) | 2006-01-10 | 2010-12-11 | Asahi Kasei Chemicals Corp | Industrial process for production of high-purity diol |
| DE102009053370A1 (de) * | 2009-11-14 | 2011-05-19 | Bayer Materialscience Ag | Verfahren zur Reinigung von Dialkylcarbonaten |
| DE102010042934A1 (de) * | 2010-10-26 | 2012-04-26 | Bayer Materialscience Aktiengesellschaft | Verfahren zur kontinuierlichen Herstellung von Dialkylcarbonat |
| DE102010042936A1 (de) | 2010-10-26 | 2012-04-26 | Bayer Materialscience Aktiengesellschaft | Verfahren zur kontinuierlichen Herstellung von Dialkylcarbonat |
| JP5958549B2 (ja) * | 2012-10-15 | 2016-08-02 | 宇部興産株式会社 | ジエチルカーボネートの製造方法 |
| CN107428669B (zh) | 2015-03-23 | 2021-07-16 | 沙特基础工业全球技术有限公司 | 用于生产碳酸芳基酯的整合的方法和装置 |
| WO2016151488A1 (en) | 2015-03-23 | 2016-09-29 | Sabic Global Technologies B.V. | Integrated method and apparatus for the production of aryl carbonates |
| CN105194899A (zh) * | 2015-10-16 | 2015-12-30 | 青岛科技大学 | 一种分离甲苯-异丁苯混合物的变径精馏装置及方法 |
| ES3042288T3 (en) * | 2021-01-08 | 2025-11-19 | Asahi Chemical Ind | Distillation column and method for industrial production of dialkyl carbonates and diols |
| US20240199527A1 (en) * | 2021-04-28 | 2024-06-20 | Asahi Kasei Kabushiki Kaisha | Production method of dialkyl carbonate and production apparatus for dialkyl carbonate |
| KR102759664B1 (ko) * | 2021-11-30 | 2025-02-03 | 롯데케미칼 주식회사 | 카보네이트의 제조 방법 |
| CN118059788B (zh) * | 2024-04-17 | 2024-07-16 | 临涣焦化股份有限公司 | 一种碳酸二甲酯提纯脱轻装置及脱轻方法 |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06196464A (ja) | 1992-12-25 | 1994-07-15 | San Seal:Kk | 半導体洗浄用炭酸ジエチルの製造方法 |
| JPH06228026A (ja) | 1993-02-01 | 1994-08-16 | Mitsubishi Gas Chem Co Inc | メタノールとジメチルカーボネートの分離法 |
| JPH0725830A (ja) | 1993-07-08 | 1995-01-27 | Daicel Chem Ind Ltd | 炭酸ジエステルの精製法及びその精製法によって得られた炭酸ジエステルを用いて製造したポリカーボネート |
| JP2000281630A (ja) * | 1999-03-26 | 2000-10-10 | Mitsubishi Chemicals Corp | 非対称ジアルキルカーボネートの製造方法 |
| JP2002371037A (ja) * | 2001-06-12 | 2002-12-26 | Mitsubishi Chemicals Corp | 高純度ジメチルカーボネートの製造方法 |
Family Cites Families (48)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3642858A (en) | 1969-02-12 | 1972-02-15 | Dow Chemical Co | Carbonate synthesis from alkylene carbonates |
| US3803201A (en) | 1971-02-22 | 1974-04-09 | Dow Chemical Co | Synthesis of dimethyl carbonate |
| IT1034961B (it) | 1975-04-09 | 1979-10-10 | Snam Progetti | Procedimento per la preparazione di dialchilcarbonati |
| DE2740251A1 (de) | 1977-09-07 | 1979-03-22 | Bayer Ag | Verfahren zur herstellung von dialkylcarbonaten |
| DE2740243A1 (de) | 1977-09-07 | 1979-03-15 | Bayer Ag | Verfahren zur herstellung von dialkylcarbonaten |
| JPS5463023A (en) | 1977-10-26 | 1979-05-21 | Mitsubishi Chem Ind Ltd | Ester exchange of carbonate |
| JPS6022697B2 (ja) | 1978-05-16 | 1985-06-03 | 日曹油化工業株式会社 | ジアルキル炭酸エステルの製造法 |
| DE3146142A1 (de) | 1981-11-21 | 1983-06-01 | Henkel KGaA, 4000 Düsseldorf | Reaktionskolonne und dessen verwendung |
| JPS6431737A (en) | 1986-01-03 | 1989-02-02 | Texaco Development Corp | Manufacture of ethylene glycol and dimethyl carbonate |
| US4691041A (en) | 1986-01-03 | 1987-09-01 | Texaco Inc. | Process for production of ethylene glycol and dimethyl carbonate |
| US4661609A (en) | 1986-07-31 | 1987-04-28 | Texaco Inc. | Process for cosynthesis of ethylene glycol and dimethyl carbonate |
| US4734518A (en) | 1987-01-12 | 1988-03-29 | Texaco Inc. | Process for cosynthesis of ethylene glycol and dimethyl carbonate |
| JPH0737422B2 (ja) | 1987-03-26 | 1995-04-26 | 旭化成工業株式会社 | ジアルキルカ−ボネ−トの製造方法 |
| JP2529025B2 (ja) | 1990-11-29 | 1996-08-28 | 旭化成工業株式会社 | ジアルキルカ―ボネ―トとジオ―ル類の連続的製造法 |
| JPH0768180B2 (ja) | 1990-12-27 | 1995-07-26 | 旭化成工業株式会社 | ジアルキルカーボネートとジオール類の連続的製法 |
| DE4129316A1 (de) | 1991-09-03 | 1993-03-04 | Bayer Ag | Verfahren zur kontinuierlichen herstellung von dialkylcarbonaten |
| DE4216121A1 (de) | 1992-05-15 | 1993-11-18 | Bayer Ag | Verfahren zur kontinuierlichen Herstellung von Dialkylcarbonaten |
| JP3652035B2 (ja) * | 1995-10-31 | 2005-05-25 | 旭化成ケミカルズ株式会社 | ジアルキルカーボネートおよびジオールの連続的製造法 |
| JP4093607B2 (ja) | 1995-11-14 | 2008-06-04 | 旭化成ケミカルズ株式会社 | ジアルキルカーボネートおよびジオールの連続的製造方法 |
| DE69620470T2 (de) | 1995-12-22 | 2002-11-21 | Asahi Kasei Kabushiki Kaisha, Osaka | Verfahren zur kontinuierlichen herstellung von dialkylcarbonaten und diolen |
| JPH09176061A (ja) | 1995-12-28 | 1997-07-08 | Asahi Chem Ind Co Ltd | ジアルキルカーボネートとジオールの連続的製造法 |
| US6346638B1 (en) * | 1998-06-10 | 2002-02-12 | Asahi Kasel Kabushiki Kaisha | Process for continuous production of dialkyl carbonate and diol |
| AU2827900A (en) | 1999-03-03 | 2000-09-21 | Asahi Kasei Kabushiki Kaisha | Process for continuously producing dialkyl carbonate and diol |
| JP4467204B2 (ja) | 2001-04-13 | 2010-05-26 | 旭化成ケミカルズ株式会社 | ジアルキルカーボネートおよびジオールの製造方法 |
| JP4380102B2 (ja) | 2001-10-10 | 2009-12-09 | 三菱化学株式会社 | ジメチルカーボネートの製造方法 |
| WO2003006418A1 (en) | 2001-07-10 | 2003-01-23 | Mitsubishi Chemical Corporation | Method for producing dialkylcarbonate |
| US6573396B2 (en) | 2001-10-12 | 2003-06-03 | Exxonmobil Chemical Patents Inc. | Co-production of dialkyl carbonates and diols with treatment of hydroxy alkyl carbonate |
| JP2003300936A (ja) | 2002-04-09 | 2003-10-21 | Mitsui Chemicals Inc | ジアルキルカーボネートとグリコールの連続同時製造方法 |
| JP3963357B2 (ja) | 2002-05-23 | 2007-08-22 | 三菱化学株式会社 | ジメチルカーボネート及びエチレングリコールの製造方法 |
| JP4424898B2 (ja) | 2002-10-08 | 2010-03-03 | 旭化成ケミカルズ株式会社 | ジアルキルカーボネートおよびジオールを製造する方法 |
| US20040104108A1 (en) | 2002-12-03 | 2004-06-03 | Mason Robert Michael | High capacity purification of thermally unstable compounds |
| CN1946660B (zh) * | 2004-06-17 | 2012-11-14 | 旭化成化学株式会社 | 生产碳酸二烷基酯和二醇的方法 |
| EA010603B1 (ru) * | 2004-06-25 | 2008-10-30 | Асахи Касеи Кемикалз Корпорейшн | Способ промышленного производства ароматического карбоната |
| KR100870851B1 (ko) * | 2004-09-17 | 2008-11-27 | 아사히 가세이 케미칼즈 가부시키가이샤 | 부생 알코올류의 공업적 분리 방법 |
| WO2006033288A1 (ja) | 2004-09-21 | 2006-03-30 | Asahi Kasei Chemicals Corporation | 副生アルコール類を工業的に分離する方法 |
| JP2006182683A (ja) | 2004-12-27 | 2006-07-13 | Asahi Kasei Chemicals Corp | ジオールおよびジアルキルカーボネートを製造する方法 |
| JP2006199643A (ja) | 2005-01-21 | 2006-08-03 | Asahi Kasei Chemicals Corp | ジオールおよびジアルキルカーボネートの製造方法 |
| JP2006206497A (ja) | 2005-01-28 | 2006-08-10 | Asahi Kasei Chemicals Corp | ジアルキルカーボネートおよびジオールを製造する方法 |
| EA012516B1 (ru) | 2005-11-25 | 2009-10-30 | Асахи Касеи Кемикалз Корпорейшн | Способ промышленного получения диалкилкарбоната и диола |
| EP1961721A1 (en) | 2005-12-12 | 2008-08-27 | Asahi Kasei Chemicals Corporation | Process for production of dialkyl carbonate and diol in industrial scale |
| TWI308911B (en) | 2005-12-13 | 2009-04-21 | Asahi Kasei Chemcials Corp | Process for industrially producing dialkyl carbonate and diol |
| TW200732291A (en) | 2005-12-14 | 2007-09-01 | Asahi Kasei Chemicals Corp | Process for production of dialkyl carbonate and diol in industrial scale and with high yield |
| TW200726745A (en) | 2005-12-16 | 2007-07-16 | Asahi Kasei Chemicals Corp | Industrial process for production of aromatic carbonate |
| TW200732290A (en) | 2005-12-16 | 2007-09-01 | Asahi Kasei Chemicals Corp | Industrial process for production of high-purity diaryl carbonate |
| JP5362223B2 (ja) | 2005-12-19 | 2013-12-11 | 旭化成ケミカルズ株式会社 | 高純度ジフェニルカーボネートを工業的規模で製造する方法 |
| EP1964829A1 (en) | 2005-12-21 | 2008-09-03 | Asahi Kasei Chemicals Corporation | Process for production of dialkyl carbonate and diol in industrial scale |
| TW200738601A (en) | 2005-12-27 | 2007-10-16 | Asahi Kasei Chemicals Corp | Industrial process for production of dialkyl carbonate and diol |
| TW200738602A (en) | 2006-02-01 | 2007-10-16 | Asahi Kasei Chemicals Corp | Industrial process for producing high-purity diol |
-
2006
- 2006-12-07 TW TW095145698A patent/TWI314549B/zh active
- 2006-12-15 WO PCT/JP2006/325089 patent/WO2007074664A1/ja not_active Ceased
- 2006-12-15 EP EP06834816.8A patent/EP1967508B1/en active Active
- 2006-12-15 BR BRPI0620605A patent/BRPI0620605B1/pt active IP Right Grant
- 2006-12-15 KR KR1020087015406A patent/KR101002863B1/ko active Active
- 2006-12-15 IN IN869KON2008 patent/IN2008KN00869A/en unknown
- 2006-12-15 JP JP2007551903A patent/JP4260212B2/ja active Active
- 2006-12-15 US US11/991,073 patent/US8049028B2/en active Active
- 2006-12-15 CN CN2006800492531A patent/CN101346340B/zh active Active
- 2006-12-15 EA EA200800919A patent/EA012062B1/ru not_active IP Right Cessation
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06196464A (ja) | 1992-12-25 | 1994-07-15 | San Seal:Kk | 半導体洗浄用炭酸ジエチルの製造方法 |
| JPH06228026A (ja) | 1993-02-01 | 1994-08-16 | Mitsubishi Gas Chem Co Inc | メタノールとジメチルカーボネートの分離法 |
| JPH0725830A (ja) | 1993-07-08 | 1995-01-27 | Daicel Chem Ind Ltd | 炭酸ジエステルの精製法及びその精製法によって得られた炭酸ジエステルを用いて製造したポリカーボネート |
| JP2000281630A (ja) * | 1999-03-26 | 2000-10-10 | Mitsubishi Chemicals Corp | 非対称ジアルキルカーボネートの製造方法 |
| JP2002371037A (ja) * | 2001-06-12 | 2002-12-26 | Mitsubishi Chemicals Corp | 高純度ジメチルカーボネートの製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| EP1967508B1 (en) | 2013-11-13 |
| JP4260212B2 (ja) | 2009-04-30 |
| BRPI0620605B1 (pt) | 2016-06-21 |
| IN2008KN00869A (enExample) | 2008-11-28 |
| EA012062B1 (ru) | 2009-08-28 |
| KR20080072936A (ko) | 2008-08-07 |
| WO2007074664A1 (ja) | 2007-07-05 |
| JPWO2007074664A1 (ja) | 2009-06-04 |
| US8049028B2 (en) | 2011-11-01 |
| BRPI0620605A2 (pt) | 2012-07-24 |
| EA200800919A1 (ru) | 2008-08-29 |
| CN101346340A (zh) | 2009-01-14 |
| EP1967508A1 (en) | 2008-09-10 |
| US20090054676A1 (en) | 2009-02-26 |
| KR101002863B1 (ko) | 2010-12-21 |
| TWI314549B (en) | 2009-09-11 |
| EP1967508A4 (en) | 2010-12-29 |
| TW200734299A (en) | 2007-09-16 |
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| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20160425 Address after: Tokyo, Japan, Japan Patentee after: Asahi Kasei Kogyo K. K. Address before: Tokyo, Japan, Japan Patentee before: Asahi Kasei Chemical K. K. |