CN101031542B - 3-(甲硫基)丙醛和2-羟基-4-(甲硫基)丁腈的制备方法 - Google Patents

3-(甲硫基)丙醛和2-羟基-4-(甲硫基)丁腈的制备方法 Download PDF

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Publication number
CN101031542B
CN101031542B CN2005800265919A CN200580026591A CN101031542B CN 101031542 B CN101031542 B CN 101031542B CN 2005800265919 A CN2005800265919 A CN 2005800265919A CN 200580026591 A CN200580026591 A CN 200580026591A CN 101031542 B CN101031542 B CN 101031542B
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CN
China
Prior art keywords
catalyst
acrolein
mmp
reaction
methylthio
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Expired - Fee Related
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CN2005800265919A
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English (en)
Chinese (zh)
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CN101031542A (zh
Inventor
弗兰克·迪布纳尔
克里斯托夫·韦克贝克
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Evonik Operations GmbH
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Degussa GmbH
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/14—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
    • C07C319/20—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides by reactions not involving the formation of sulfide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/14—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
    • C07C319/18—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides by addition of thiols to unsaturated compounds

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
CN2005800265919A 2004-08-05 2005-07-14 3-(甲硫基)丙醛和2-羟基-4-(甲硫基)丁腈的制备方法 Expired - Fee Related CN101031542B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102004038053A DE102004038053A1 (de) 2004-08-05 2004-08-05 Verfahren zur Herstellung von 3-(Methylthio)propanal
DE102004038053.8 2004-08-05
PCT/EP2005/007666 WO2006015684A2 (de) 2004-08-05 2005-07-14 Verfahren zur herstellung von 3-(methylthio)propanal und 2-hydroxy-4-(methylthio)butannitril

Related Child Applications (1)

Application Number Title Priority Date Filing Date
CN2010101447601A Division CN101812004B (zh) 2004-08-05 2005-07-14 3-(甲硫基)丙醛和2-羟基-4-(甲硫基)丁腈的制备方法

Publications (2)

Publication Number Publication Date
CN101031542A CN101031542A (zh) 2007-09-05
CN101031542B true CN101031542B (zh) 2010-05-12

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ID=35149290

Family Applications (2)

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CN2005800265919A Expired - Fee Related CN101031542B (zh) 2004-08-05 2005-07-14 3-(甲硫基)丙醛和2-羟基-4-(甲硫基)丁腈的制备方法
CN2010101447601A Expired - Fee Related CN101812004B (zh) 2004-08-05 2005-07-14 3-(甲硫基)丙醛和2-羟基-4-(甲硫基)丁腈的制备方法

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Country Status (11)

Country Link
US (1) US7119233B2 (enExample)
EP (2) EP1778631B1 (enExample)
JP (2) JP4773441B2 (enExample)
CN (2) CN101031542B (enExample)
BR (1) BRPI0513072A (enExample)
CA (1) CA2573047A1 (enExample)
DE (1) DE102004038053A1 (enExample)
ES (2) ES2560447T3 (enExample)
MX (1) MX2007000345A (enExample)
RU (1) RU2383531C2 (enExample)
WO (1) WO2006015684A2 (enExample)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102005003990A1 (de) * 2005-01-28 2006-08-03 Degussa Ag Herstellung von 3-(Alkylthio)propanal
JP5182198B2 (ja) * 2009-04-06 2013-04-10 住友化学株式会社 ３−メチルチオプロパナールの製造方法
JP5402864B2 (ja) * 2010-07-20 2014-01-29 住友化学株式会社 ３−メチルチオプロパナールの製造方法
FR2966456B1 (fr) * 2010-10-26 2013-03-15 Adisseo France Sas Procede d'obtention d'acroleine par deshydratation catalytique de glycerol ou de glycerine
EP2468383A1 (de) * 2010-12-22 2012-06-27 Evonik Degussa GmbH Verfahren zur thermischen Nachverbrennung von Abgasen aus der Acrolein- und aus der Blausäureherstellung
MY161682A (en) * 2011-02-23 2017-05-15 Evonik Degussa Gmbh Storage-stable 2-hydroxy-4- (methylthio) butyronitrile
KR101911563B1 (ko) 2011-02-23 2018-10-24 에보니크 데구사 게엠베하 3-(메틸티오)프로판알 및 시안화수소로부터 2-히드록시-4-(메틸티오)부탄니트릴을 제조하는 방법
CN105452210B (zh) 2013-06-03 2018-11-20 赢创德固赛有限公司 制备丙烯醛的方法
CN107417570B (zh) * 2017-09-14 2020-04-14 哈尔滨理工大学 利用丙酮氰醇制备α-羟基腈的方法
CN111116437B (zh) 2018-11-01 2021-02-05 山东新和成氨基酸有限公司 制备2-羟基-4-甲硫基丁酸及其中间体的方法和装置
CN109651215B (zh) * 2019-02-14 2023-12-22 天宝动物营养科技股份有限公司 一种2-羟基-4-甲硫基丁腈的连续制备工艺和装置
WO2025018942A1 (en) 2023-07-17 2025-01-23 Mojia Biotech Pte. Ltd. Production of methionine via condensation of methional and c1-derived formyl-coa
CN119912370B (zh) * 2025-04-03 2025-08-05 山东新和成氨基酸有限公司 一种2-羟基-4-甲硫基丁腈的制备方法及反应装置

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5705675A (en) * 1995-06-07 1998-01-06 Novus International, Inc. Processes for the preparation of 3-(methylthio)propanal and 2-hydroxy-4-(methylthio)butanenitrile
WO2003009936A2 (en) * 2001-07-23 2003-02-06 Andrew Bruce Holmes Palladium-catalysed carbon-carbon bond forming reactions in compressed carbon dioxide

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2542768A (en) * 1945-10-24 1951-02-20 Du Pont Hydroxy-methylmercaptobutyronitrile
DE2320544C2 (de) 1973-04-21 1975-06-05 Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt Verfahren zur Herstellung von 3-Methylmercaptopropionaldehyd
FR2314917A1 (fr) 1975-06-20 1977-01-14 Rhone Poulenc Ind Procede de fabrication de l'aldehyde beta-methylthiopropionique
DE2623285C3 (de) 1976-05-25 1980-10-02 Gebrueder Grau Und Co Kg Chem. Fabrik, 7070 Schwaebisch Gmuend Riechstoffkomposition
FR2460925A1 (fr) 1979-07-10 1981-01-30 Rhone Poulenc Ind Procede de preparation directe d'aldehyde beta-methylthiopropionique
FR2480925A1 (fr) 1980-04-22 1981-10-23 Electricite De France Echangeur thermique modulaire
US4440676A (en) 1981-12-24 1984-04-03 The British Petroleum Company P.L.C. Process for the production of a dipeptide, a polypeptide or a protein
JP3219544B2 (ja) * 1992-05-21 2001-10-15 ダイセル化学工業株式会社 ２−ヒドロキシ−４−メチルチオブタン酸の製造法
US5905171A (en) 1995-06-22 1999-05-18 Novus International, Inc. Process for the preparation of 3-(methylthio)propanal
US5352837A (en) 1993-06-08 1994-10-04 Novus International, Inc. Process for the preparation of 3-(methylthio)propanal
AR002174A1 (es) * 1995-06-07 1998-01-07 Novus Int Inc Proceso para la preparacion de 3-(metiltio)propanal y 2-hidroxi-4-metiltio) butanonitrilo
AU2594797A (en) * 1996-04-01 1997-10-22 Jonathan Lester Brockwell Processes for the manufacture of methylmercaptopropanal
JP4517486B2 (ja) * 2000-09-25 2010-08-04 住友化学株式会社 ２−ヒドロキシ−４−メチルチオブタンニトリルの製造方法
JP4186572B2 (ja) * 2002-09-27 2008-11-26 住友化学株式会社 ３−メチルチオプロパナールの製造方法

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5705675A (en) * 1995-06-07 1998-01-06 Novus International, Inc. Processes for the preparation of 3-(methylthio)propanal and 2-hydroxy-4-(methylthio)butanenitrile
WO2003009936A2 (en) * 2001-07-23 2003-02-06 Andrew Bruce Holmes Palladium-catalysed carbon-carbon bond forming reactions in compressed carbon dioxide

Also Published As

Publication number Publication date
JP5306402B2 (ja) 2013-10-02
WO2006015684A3 (de) 2006-08-03
RU2383531C2 (ru) 2010-03-10
MX2007000345A (es) 2007-03-07
EP1778631A2 (de) 2007-05-02
US20060030739A1 (en) 2006-02-09
EP2987785A1 (de) 2016-02-24
CN101812004A (zh) 2010-08-25
JP2008508330A (ja) 2008-03-21
JP2011132256A (ja) 2011-07-07
CA2573047A1 (en) 2006-02-16
BRPI0513072A (pt) 2008-04-22
CN101031542A (zh) 2007-09-05
CN101812004B (zh) 2012-09-19
EP2987785B1 (de) 2018-03-14
ES2667220T3 (es) 2018-05-10
RU2007108071A (ru) 2008-09-20
DE102004038053A1 (de) 2006-04-27
EP1778631B1 (de) 2015-11-18
US7119233B2 (en) 2006-10-10
JP4773441B2 (ja) 2011-09-14
WO2006015684A2 (de) 2006-02-16
ES2560447T3 (es) 2016-02-19

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Owner name: EVONIK DEGUSSA CO., LTD.

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