CN100471834C - 制备氟化学单异氰酸酯的方法 - Google Patents

制备氟化学单异氰酸酯的方法 Download PDF

Info

Publication number
CN100471834C
CN100471834C CNB2004800396658A CN200480039665A CN100471834C CN 100471834 C CN100471834 C CN 100471834C CN B2004800396658 A CNB2004800396658 A CN B2004800396658A CN 200480039665 A CN200480039665 A CN 200480039665A CN 100471834 C CN100471834 C CN 100471834C
Authority
CN
China
Prior art keywords
solvent
nch
reaction
monoisocyanates
sub
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CNB2004800396658A
Other languages
English (en)
Chinese (zh)
Other versions
CN1902164A (zh
Inventor
托马斯·P·克伦
艾伦·R·柯克
乔治·G·I·摩尔
约翰·C·克拉克
裘再明
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
3M Innovative Properties Co
Original Assignee
3M Innovative Properties Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 3M Innovative Properties Co filed Critical 3M Innovative Properties Co
Publication of CN1902164A publication Critical patent/CN1902164A/zh
Application granted granted Critical
Publication of CN100471834C publication Critical patent/CN100471834C/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/36—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids
    • C07C303/40—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids by reactions not involving the formation of sulfonamide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C311/00—Amides of sulfonic acids, i.e. compounds having singly-bound oxygen atoms of sulfo groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
    • C07C311/01—Sulfonamides having sulfur atoms of sulfonamide groups bound to acyclic carbon atoms
    • C07C311/02—Sulfonamides having sulfur atoms of sulfonamide groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
    • C07C311/09—Sulfonamides having sulfur atoms of sulfonamide groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton the carbon skeleton being further substituted by at least two halogen atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CNB2004800396658A 2003-12-31 2004-12-14 制备氟化学单异氰酸酯的方法 Expired - Fee Related CN100471834C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US10/751,142 US7081545B2 (en) 2003-12-31 2003-12-31 Process for preparing fluorochemical monoisocyanates
US10/751,142 2003-12-31

Publications (2)

Publication Number Publication Date
CN1902164A CN1902164A (zh) 2007-01-24
CN100471834C true CN100471834C (zh) 2009-03-25

Family

ID=34701272

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB2004800396658A Expired - Fee Related CN100471834C (zh) 2003-12-31 2004-12-14 制备氟化学单异氰酸酯的方法

Country Status (8)

Country Link
US (2) US7081545B2 (https=)
EP (1) EP1699755B1 (https=)
JP (1) JP4965264B2 (https=)
KR (1) KR20060107836A (https=)
CN (1) CN100471834C (https=)
AT (1) ATE525348T1 (https=)
CA (1) CA2552000A1 (https=)
WO (1) WO2005065164A2 (https=)

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007523971A (ja) * 2003-12-31 2007-08-23 スリーエム イノベイティブ プロパティズ カンパニー 撥水撥油性フルオロアクリレート
US7411020B2 (en) 2004-12-28 2008-08-12 3M Innovative Properties Company Water-based release coating containing fluorochemical
US7345123B2 (en) * 2004-12-28 2008-03-18 3M Innovative Properties Company Fluoroacrylate-multifunctional acrylate copolymer compositions
US7253241B2 (en) 2004-12-28 2007-08-07 3M Innovative Properties Company Fluorochemical containing low adhesion backsize
US7291688B2 (en) * 2004-12-28 2007-11-06 3M Innovative Properties Company Fluoroacrylate-mercaptofunctional copolymers
US20060142530A1 (en) * 2004-12-28 2006-06-29 Moore George G Water- and oil-repellent fluorourethanes and fluoroureas
KR20080033306A (ko) * 2005-06-29 2008-04-16 쓰리엠 이노베이티브 프로퍼티즈 컴파니 올리고머형 플루오로아크릴레이트로부터 유도된 폴리우레탄
US7279210B2 (en) * 2005-09-07 2007-10-09 3M Innovative Properties Company Curable compositions, methods of making and using the same, and articles therefrom
US7560166B2 (en) * 2005-12-28 2009-07-14 3M Innovative Properties Company Adhesive article, composite article, and methods of making the same
US7981988B2 (en) * 2006-05-25 2011-07-19 3M Innovative Properties Company Ultraviolet radiation-polymerizable compositions
US20080075951A1 (en) * 2006-09-27 2008-03-27 3M Innovative Properties Company Fluoroacrylates and hardcoat compositions including the same
US8530054B2 (en) * 2006-09-27 2013-09-10 3M Innovative Properties Company Solar control multilayer film
WO2008083272A1 (en) * 2006-12-29 2008-07-10 3M Innovative Properties Company Stain and fouling resistant polyurea and polyurethane coatings
US8686179B2 (en) 2009-06-12 2014-04-01 3M Innovative Properties Company Fluorinated aromatic bis(acyl)-containing compounds and polyesters prepared therefrom
EP2516389B1 (en) 2009-12-22 2016-02-17 3M Innovative Properties Company Fluorinated arylene-containing compounds, methods, and polymers prepared therefrom
CN104927024A (zh) * 2014-03-20 2015-09-23 江南大学 一种氟改性光固化聚氨酯丙烯酸酯树脂的制备方法及其作为光固化涂层疏水填料的应用

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4728542A (en) * 1985-06-19 1988-03-01 Bayer Aktiengesellschaft Ionically modified pur spreading pastes and their use
US5446118A (en) * 1994-08-11 1995-08-29 W. L. Gore & Associates, Inc. Fluorinated acrylic monomers containing urethane groups and their polymers

Family Cites Families (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2803656A (en) * 1956-01-23 1957-08-20 Minnesota Mining & Mfg Fluorocarbonsulfonamidoalkanols and sulfates thereof
US3776805A (en) * 1971-09-07 1973-12-04 Minnesota Mining & Mfg Solar control products
US4321404A (en) * 1980-05-20 1982-03-23 Minnesota Mining And Manufacturing Company Compositions for providing abherent coatings
US4540497A (en) * 1982-11-09 1985-09-10 Minnesota Mining And Manufacturing Company Fluoroaliphatic radical-containing, substituted guanidines and fibrous substrates treated therewith
US4566981A (en) * 1984-03-30 1986-01-28 Minnesota Mining And Manufacturing Company Fluorochemicals and fibrous substrates treated therewith: compositions of cationic and non-ionic fluorochemicals
US4668726A (en) * 1984-03-30 1987-05-26 Minnesota Mining And Manufacturing Company Cationic and non-ionic fluorochemicals and fibrous substrates treated therewith
FR2588555B1 (fr) * 1985-10-16 1987-12-11 Atochem Monomeres acryliques fluores, polymeres en derivant et leur application au traitement hydrofuge et oleofuge de substrats divers
US5144056A (en) * 1985-12-03 1992-09-01 Atochem Fluorinated acrylic monomers as hydrophobic and oleophobic agents
FR2590895B1 (fr) * 1985-12-03 1988-01-15 Atochem Monomeres acryliques fluores, polymeres en derivant et leur application comme agents hydrophobes et oleophobes
CA2048232A1 (en) * 1990-09-05 1992-03-06 Jerry W. Williams Energy curable pressure-sensitive compositions
JPH0689462A (ja) 1992-09-07 1994-03-29 Three Bond Co Ltd 光ディスク
TW312700B (https=) * 1994-05-17 1997-08-11 Sony Co Ltd
US6017603A (en) * 1995-04-28 2000-01-25 Nippon Kayaku Kabushiki Kaisha Ultraviolet-curing adhesive composition and article
US5688884A (en) * 1995-08-31 1997-11-18 E. I. Du Pont De Nemours And Company Polymerization process
DE19541174C2 (de) * 1995-11-04 1998-11-26 Spraying Systems Deutschland G Hochleistungsstrahldüse
JPH09291258A (ja) * 1996-04-26 1997-11-11 Lintec Corp 粘着剤組成物およびこれを用いた粘着シート
JP3835857B2 (ja) 1996-06-18 2006-10-18 日本化薬株式会社 光ディスク用接着剤組成物、硬化物、物品及び接着方法
JPH1025453A (ja) 1996-07-08 1998-01-27 Nippon Kayaku Co Ltd 陰極線管用接着剤及びその硬化物
JP3911728B2 (ja) 1996-08-07 2007-05-09 住友化学株式会社 ディジタルビデオディスクの保護コート兼接着用樹脂組成物
JPH10140090A (ja) 1996-11-08 1998-05-26 Daicel U C B Kk 陰極線管用接着剤およびその硬化物
EP0960355A1 (en) 1997-02-13 1999-12-01 Dsm N.V. Photocurable resin composition
TW430672B (en) * 1997-07-03 2001-04-21 Sumitomo Chemical Co A photo-curing resin composition for DVD
US5959775A (en) * 1997-12-23 1999-09-28 3M Innovative Properties Company Urethane/acrylate bead bond for retroreflective articles
US6180200B1 (en) * 1998-06-01 2001-01-30 Dsm N. V. Cationic and hybrid radiation curable pressure sensitive adhesives for bonding of optical discs
EP1246856B1 (en) * 1999-10-27 2009-07-15 3M Innovative Properties Company Fluorochemical sulfonamide surfactants
DE19962272A1 (de) * 1999-12-23 2001-06-28 Basf Ag Isocyanatgruppen aufweisende Bausteine sowie ihre Verwendung zur Funktionalisierung oder Modifizierung von Verbindungen oder Oberflächen
EP1142912A1 (en) 2000-04-05 2001-10-10 Dsm N.V. Radiation curable compositions
US6949297B2 (en) * 2001-11-02 2005-09-27 3M Innovative Properties Company Hybrid adhesives, articles, and methods
JP2007523971A (ja) * 2003-12-31 2007-08-23 スリーエム イノベイティブ プロパティズ カンパニー 撥水撥油性フルオロアクリレート

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4728542A (en) * 1985-06-19 1988-03-01 Bayer Aktiengesellschaft Ionically modified pur spreading pastes and their use
US5446118A (en) * 1994-08-11 1995-08-29 W. L. Gore & Associates, Inc. Fluorinated acrylic monomers containing urethane groups and their polymers

Also Published As

Publication number Publication date
CN1902164A (zh) 2007-01-24
EP1699755B1 (en) 2011-09-21
JP2007517033A (ja) 2007-06-28
CA2552000A1 (en) 2005-07-21
US7361782B2 (en) 2008-04-22
JP4965264B2 (ja) 2012-07-04
EP1699755A4 (en) 2007-11-07
WO2005065164A3 (en) 2005-09-09
WO2005065164A2 (en) 2005-07-21
US7081545B2 (en) 2006-07-25
EP1699755A2 (en) 2006-09-13
ATE525348T1 (de) 2011-10-15
US20060247460A1 (en) 2006-11-02
US20050143595A1 (en) 2005-06-30
KR20060107836A (ko) 2006-10-16

Similar Documents

Publication Publication Date Title
CN100471834C (zh) 制备氟化学单异氰酸酯的方法
EP1709089B1 (en) Water-and oil-repellent fluoroacrylates
EP1462434B1 (en) Process for preparing hydrofluoroethers
CA1116177A (en) Process for the preparation of diphenylmethane dicarbamates and polymethylene polyphenyl carbamates
US6384167B2 (en) Sulfonated perfluorovinyl functional monomers
Ying et al. Utilization of carbon dioxide to build a basic block for polymeric materials: an isocyanate-free route to synthesize a soluble oligourea
CN103044649B (zh) 一种含氟阳离子水性聚氨酯及其制备方法
CN101691342A (zh) 一种含氟丙烯酸酯单体及其制备方法和应用
WO2021004286A1 (zh) 一种化合物及其制备方法、用途和组成的组合物
JP2000508619A (ja) イソシアネート誘導体を含むフルオロカーボンおよび耐汚水剤
JPS63183553A (ja) メチルカルバメートのリモネンへの付加によるシクロヘキシルモノーおよびジーウレタンの製造法
US7285600B2 (en) Reagents for heat activated polymer crosslinking
JPS6131101B2 (https=)
Liou et al. Novel adhesives based on poly (isocyanates)
CN1469888A (zh) 氟化酸和三价金属的盐用作形成尿烷的催化剂、包含它们的组合物及其用途
JP3849372B2 (ja) ポリテトラメチレンエーテルグリコールジカルボン酸エステルの連続製造方法
CN101691341B (zh) 含全氟烯烃基的烯丙氧乙基氨基甲酸酯及制备方法和应用
EP1301565B1 (en) Reagents for heat activated polymer crosslinking
CN113121779B (zh) 双全氟支化醚链氧杂环丁烷系列含氟聚合物及其制备方法
JPS5855462A (ja) ウレトジオン基含有ジイソシアネ−ト及びそれからオリゴ付加生成物を製造する方法
JP2997501B2 (ja) ウレタン樹脂製造用組成物
JP2002037834A (ja) 頭−尾定序性ポリウレタンの製造法
Reimann Synthesis, crystallization and aggregation of supramolecular precision polymers
JP2008127293A (ja) カルバミン酸エステル化合物
JPH07149889A (ja) 含フッ素アルキルポリエーテル重合体の製造方法

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20090325

Termination date: 20171214

CF01 Termination of patent right due to non-payment of annual fee