CN100334074C - 六氟异丁烯及其高级同系物的氟代硫酸酯及它们的衍生物 - Google Patents

六氟异丁烯及其高级同系物的氟代硫酸酯及它们的衍生物 Download PDF

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Publication number
CN100334074C
CN100334074C CNB038108488A CN03810848A CN100334074C CN 100334074 C CN100334074 C CN 100334074C CN B038108488 A CNB038108488 A CN B038108488A CN 03810848 A CN03810848 A CN 03810848A CN 100334074 C CN100334074 C CN 100334074C
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CN
China
Prior art keywords
oso
nmr
reaction
hexafluoroisobutene
give
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CNB038108488A
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English (en)
Chinese (zh)
Other versions
CN1665779A (zh
Inventor
V·F·切尔斯特科夫
N·I·德利亚吉纳
R·E·费尔南德斯
V·A·佩特罗夫
W·秋
P·R·雷斯尼克
R·C·惠兰
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Chemours Co FC LLC
Original Assignee
EI Du Pont de Nemours and Co
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Publication of CN1665779A publication Critical patent/CN1665779A/zh
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Publication of CN100334074C publication Critical patent/CN100334074C/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/02—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
    • C07C303/22—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof from sulfonic acids, by reactions not involving the formation of sulfo or halosulfonyl groups; from sulfonic halides by reactions not involving the formation of halosulfonyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C21/00—Acyclic unsaturated compounds containing halogen atoms
    • C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
    • C07C21/18—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/16—Preparation of carboxylic acid nitriles by reaction of cyanides with lactones or compounds containing hydroxy groups or etherified or esterified hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C255/00—Carboxylic acid nitriles
    • C07C255/01—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms
    • C07C255/10—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms containing cyano groups and halogen atoms, or nitro or nitroso groups, bound to the same acyclic carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C305/00—Esters of sulfuric acids
    • C07C305/26—Halogenosulfates, i.e. monoesters of halogenosulfuric acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C43/00—Ethers; Compounds having groups, groups or groups
    • C07C43/02—Ethers
    • C07C43/03—Ethers having all ether-oxygen atoms bound to acyclic carbon atoms
    • C07C43/14—Unsaturated ethers
    • C07C43/17—Unsaturated ethers containing halogen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F14/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
    • C08F14/18—Monomers containing fluorine
    • C08F14/28—Hexafluoropropene
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F214/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
    • C08F214/18—Monomers containing fluorine

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Toxicology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Epoxy Compounds (AREA)
CNB038108488A 2002-05-14 2003-05-14 六氟异丁烯及其高级同系物的氟代硫酸酯及它们的衍生物 Expired - Fee Related CN100334074C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US38052802P 2002-05-14 2002-05-14
US60/380,528 2002-05-14

Related Child Applications (4)

Application Number Title Priority Date Filing Date
CN2007101278546A Division CN101085754B (zh) 2002-05-14 2003-05-14 六氟异丁烯及其高级同系物的氟代硫酸酯及它们的衍生物
CN2007101278565A Division CN101085753B (zh) 2002-05-14 2003-05-14 六氟异丁烯及其高级同系物的氟代硫酸酯及它们的衍生物
CNA2007101278531A Division CN101092378A (zh) 2002-05-14 2003-05-14 六氟异丁烯及其高级同系物的氟代硫酸酯及它们的衍生物
CN2007101278550A Division CN101085752B (zh) 2002-05-14 2003-05-14 六氟异丁烯及其高级同系物的氟代硫酸酯及它们的衍生物

Publications (2)

Publication Number Publication Date
CN1665779A CN1665779A (zh) 2005-09-07
CN100334074C true CN100334074C (zh) 2007-08-29

Family

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Family Applications (5)

Application Number Title Priority Date Filing Date
CNB038108488A Expired - Fee Related CN100334074C (zh) 2002-05-14 2003-05-14 六氟异丁烯及其高级同系物的氟代硫酸酯及它们的衍生物
CN2007101278550A Expired - Fee Related CN101085752B (zh) 2002-05-14 2003-05-14 六氟异丁烯及其高级同系物的氟代硫酸酯及它们的衍生物
CNA2007101278531A Pending CN101092378A (zh) 2002-05-14 2003-05-14 六氟异丁烯及其高级同系物的氟代硫酸酯及它们的衍生物
CN2007101278546A Expired - Fee Related CN101085754B (zh) 2002-05-14 2003-05-14 六氟异丁烯及其高级同系物的氟代硫酸酯及它们的衍生物
CN2007101278565A Expired - Fee Related CN101085753B (zh) 2002-05-14 2003-05-14 六氟异丁烯及其高级同系物的氟代硫酸酯及它们的衍生物

Family Applications After (4)

Application Number Title Priority Date Filing Date
CN2007101278550A Expired - Fee Related CN101085752B (zh) 2002-05-14 2003-05-14 六氟异丁烯及其高级同系物的氟代硫酸酯及它们的衍生物
CNA2007101278531A Pending CN101092378A (zh) 2002-05-14 2003-05-14 六氟异丁烯及其高级同系物的氟代硫酸酯及它们的衍生物
CN2007101278546A Expired - Fee Related CN101085754B (zh) 2002-05-14 2003-05-14 六氟异丁烯及其高级同系物的氟代硫酸酯及它们的衍生物
CN2007101278565A Expired - Fee Related CN101085753B (zh) 2002-05-14 2003-05-14 六氟异丁烯及其高级同系物的氟代硫酸酯及它们的衍生物

Country Status (7)

Country Link
US (6) US7276624B2 (https=)
EP (1) EP1513801B1 (https=)
JP (2) JP4472519B2 (https=)
CN (5) CN100334074C (https=)
DE (1) DE60336720D1 (https=)
RU (1) RU2004136314A (https=)
WO (1) WO2003097588A2 (https=)

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US7276624B2 (en) * 2002-05-14 2007-10-02 E. I. Du Pont De Nemours And Company Fluorosulfates of hexafluoroisobutylene and its higher homologs
WO2006069107A2 (en) * 2004-12-22 2006-06-29 E.I. Dupont De Nemours And Company Copolymers of perfluoro (alkyl venyl ether) for photochemical reactor, process for increasing fluorine content and production of olefinic compound by photochlorination
EP1855795A1 (en) * 2004-12-22 2007-11-21 E.I.Du pont de nemours and company Functionalized copolymers of terminally functionalized perfluoro (alkyl vinyl ether) reactor wall for photochemical reactions, process for increasing fluorine content in hydrocarbons and halohydrocarbons and olefin production
AU2007316613B2 (en) * 2006-11-09 2013-11-28 Boehringer Ingelheim International Gmbh Combination therapy with SGLT-2 inhibitors and their pharmaceutical compositions
JP5136070B2 (ja) * 2008-01-15 2013-02-06 旭硝子株式会社 パーフルオロアリルブロミドの製造方法
US20100004518A1 (en) * 2008-07-03 2010-01-07 Masimo Laboratories, Inc. Heat sink for noninvasive medical sensor
EP2554530B2 (en) * 2010-03-29 2019-06-12 Daikin Industries, Ltd. Method for producing 3-chloro-pentafluoropropene
RU2430914C1 (ru) * 2010-04-09 2011-10-10 Федеральное государственное унитарное предприятие "Ордена Ленина и ордена Трудового Красного Знамени научно-исследовательский институт синтетического каучука имени академика С.В. Лебедева" Перфтор[(2-фторсульфат)этилаллиловый] эфир
US8940846B2 (en) * 2010-07-01 2015-01-27 Solvay Specialty Polymers Italy S.P.A. Process for the treatment of sulfonyl fluoride polymers
CN102225980B (zh) * 2011-04-29 2012-11-21 内蒙古三爱富万豪氟化工有限公司 一种含氟醚端基结构的聚偏氟乙烯树脂及其制备方法
JP5793996B2 (ja) * 2011-06-29 2015-10-14 セントラル硝子株式会社 フルオロ硫酸芳香環エステル類の製造方法
JP6868623B2 (ja) * 2015-12-02 2021-05-12 スリーエム イノベイティブ プロパティズ カンパニー アリル末端不飽和ヒドロフルオロアミン及びアリル末端不飽和ヒドロフルオロエーテル化合物並びにこれらの使用方法
EP3455322B1 (en) * 2016-05-09 2021-03-03 3M Innovative Properties Company Hydrofluoroolefins and methods of using same
CN107286061A (zh) * 2017-06-09 2017-10-24 武汉理工大学 一种酚类化合物脱氧还原方法
WO2020115197A1 (en) * 2018-12-06 2020-06-11 Grillo-Werke Ag Method for the recycling or disposal of halocarbons
CN114644539B (zh) * 2022-04-01 2023-07-14 安徽农业大学 一种含烯烃的二氟芳氧醚的合成方法及其在农药中的用途

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1219063A (en) * 1968-09-10 1971-01-13 Allied Chem Process for preparing fluoroisobutylenes
GB2027709A (en) * 1978-08-08 1980-02-27 Du Pont Perfluorallyl Fluorosulfate and its Sultone and Processes for their Preparation

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US2352554A (en) * 1939-06-02 1944-06-27 Redington Co F B Stamp feeding and gluing mechanism
US2852554A (en) 1956-07-12 1958-09-16 Du Pont Alpha-sulfopolyfluoromonocarboxylic acids and derivatives hydrolyzable thereto
US3862978A (en) * 1967-08-24 1975-01-28 Dow Chemical Co Catalytic synthesis of organic halogen compounds from an ethylenically unsaturated compound and a halogenated organic compound
US3655786A (en) * 1968-09-10 1972-04-11 Allied Chem Process for preparing fluoroisobutylenes and novel product
US3706723A (en) 1970-04-29 1972-12-19 Allied Chem Copolymer of 3,3,3 - trifluoro-2-trifluoromethyl propene and vinylidene fluoride
US4131740A (en) 1977-04-20 1978-12-26 E. I. Du Pont De Nemours And Company Alkyl perfluoro-ω-fluoroformyl esters and their preparation
US4235804A (en) 1978-08-08 1980-11-25 E. I. Du Pont De Nemours And Company Preparation of perfluoroallyl fluorosulfate
US4273728A (en) * 1979-03-14 1981-06-16 E. I. Du Pont De Nemours And Company Polyfluoroallyloxy compounds, their preparation and copolymers therefrom
EP0121073B1 (en) 1983-03-07 1987-07-22 Ausimont, U.S.A., Inc. A process of rotational molding fluoropolymers
US4704324A (en) * 1985-04-03 1987-11-03 The Dow Chemical Company Semi-permeable membranes prepared via reaction of cationic groups with nucleophilic groups
CA2168794A1 (en) 1994-06-09 1995-12-14 Takayuki Araki Fluoroolefin, fluoropolymer, and thermoplastic resin composition containing the polymer
US6025092A (en) 1998-02-13 2000-02-15 E. I. Du Pont De Nemours And Company Fluorinated ionomers and their uses
CA2360903A1 (en) * 1999-03-16 2000-09-21 E.I. Du Pont De Nemours And Company Fluoropolymer low reflecting layers for plastic lenses and devices
CN1391664A (zh) 1999-11-17 2003-01-15 纳幕尔杜邦公司 紫外和真空紫外透明的聚合物组合物及其应用
IT1318488B1 (it) 2000-04-21 2003-08-25 Ausimont Spa Fluorovinileteri e polimeri da essi ottenibili.
US7438995B2 (en) 2001-05-14 2008-10-21 E.I. Du Pont De Nemours And Company Use of partially fluorinated polymers in applications requiring transparency in the ultraviolet and vacuum ultraviolet
US6713567B2 (en) 2001-07-13 2004-03-30 E. I. Du Pont De Nemours And Company Method for forming fluorinated ionomers
US6653515B2 (en) * 2001-12-14 2003-11-25 Ballard Power Systems Inc. Synthesis of α, β, β-trifluorostyrene via in-situ formation of trifluorovinyl metal halide
US7129009B2 (en) * 2002-05-14 2006-10-31 E. I. Du Pont De Nemours And Company Polymer-liquid compositions useful in ultraviolet and vacuum ultraviolet uses
US7276624B2 (en) * 2002-05-14 2007-10-02 E. I. Du Pont De Nemours And Company Fluorosulfates of hexafluoroisobutylene and its higher homologs

Patent Citations (2)

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GB1219063A (en) * 1968-09-10 1971-01-13 Allied Chem Process for preparing fluoroisobutylenes
GB2027709A (en) * 1978-08-08 1980-02-27 Du Pont Perfluorallyl Fluorosulfate and its Sultone and Processes for their Preparation

Also Published As

Publication number Publication date
CN101092378A (zh) 2007-12-26
US7531689B2 (en) 2009-05-12
JP2010031058A (ja) 2010-02-12
DE60336720D1 (de) 2011-05-26
JP5149885B2 (ja) 2013-02-20
CN101085753B (zh) 2012-07-18
CN101085752A (zh) 2007-12-12
US7276624B2 (en) 2007-10-02
US7579499B2 (en) 2009-08-25
EP1513801B1 (en) 2011-04-13
US20040019237A1 (en) 2004-01-29
WO2003097588A3 (en) 2004-04-22
CN1665779A (zh) 2005-09-07
US20070167652A1 (en) 2007-07-19
WO2003097588A2 (en) 2003-11-27
US20070167651A1 (en) 2007-07-19
US20090203865A1 (en) 2009-08-13
RU2004136314A (ru) 2005-05-10
US20070167589A1 (en) 2007-07-19
CN101085754B (zh) 2013-01-23
CN101085754A (zh) 2007-12-12
US7301059B2 (en) 2007-11-27
US20070167640A1 (en) 2007-07-19
JP2005525428A (ja) 2005-08-25
CN101085753A (zh) 2007-12-12
CN101085752B (zh) 2012-07-11
JP4472519B2 (ja) 2010-06-02
EP1513801A2 (en) 2005-03-16

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C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
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GR01 Patent grant
TR01 Transfer of patent right
TR01 Transfer of patent right

Effective date of registration: 20180105

Address after: Delaware, USA

Patentee after: Como Efsee Co.,Ltd.

Address before: Wilmington, Delaware, USA

Patentee before: E. I. du Pont de Nemours and Co.

CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20070829

Termination date: 20200514