CH152485A - Process for the preparation of a vat dye. - Google Patents
Process for the preparation of a vat dye.Info
- Publication number
- CH152485A CH152485A CH152485DA CH152485A CH 152485 A CH152485 A CH 152485A CH 152485D A CH152485D A CH 152485DA CH 152485 A CH152485 A CH 152485A
- Authority
- CH
- Switzerland
- Prior art keywords
- preparation
- dye
- vat dye
- anthanthrone
- biomizing
- Prior art date
Links
Landscapes
- Pyridine Compounds (AREA)
- Removal Of Specific Substances (AREA)
Description
Verfahren mir Darstellung eines IKfipenfarbstoffes. lm Hauptpatent ist ein Verfahren zur Darstellung eines Küpenfarbstoffes beschrie ben, bei dem Anthanthron mit jodierenden Mitteln behandelt wird.
Es wurde nun gefunden, dass man einen Farbstoff von ähnlichen Eigenschaften er halten kann, wenn man Monobromarrthan- thron, erhalten z. B. durch Biomieren von Anthanthron oder durch Überführen von Monoaminoanthanthron nach Sandrneyer in Bromanthanthron, jodiert.
Der erhaltene Farbstoff, ein Bromjod- anthanthron, stimmt in seinen Eigenschaften mit dem des gemäss dem Schweiz. Patent Nr. 149901 erhaltenen Farbstoff überein.
<I>Beispiel:</I> 76 Teile Monobromanthanthron (darge stellt durch Diazotieren von Monoaminoanth- anthron und Ersatz der Diazogruppe durch Brom nach Sandmeyer mittelst Kupferbromür) werden in<B>360</B> Teilen lllonohydrat gelöst und mit 26 Teilen Jod jodiert.
Nach Beendigung der Reaktion @.vird das gebildete Bromjod- anthanthron durch Zugabe vorn verdünnter Schwefelsäure oder Eis in Form seines Sul fates abgeschieden, abgesaugt und dieses in der üblichen Weise mit Wasser zersetzt.
Method with representation of an IKfipen dye. The main patent describes a process for preparing a vat dye in which anthanthrone is treated with iodine agents.
It has now been found that you can keep a dye of similar properties, if you get Monobromarrthan- thron, z. B. by biomizing of anthanthrone or by converting monoaminoanthanthrone to Sandrneyer in bromanthanthron, iodized.
The dye obtained, a bromoiodanthanthrone, has the same properties as that of Switzerland. U.S. Patent No. 149901.
<I> Example: </I> 76 parts of monobromoanthanthrone (represented by diazotizing monoaminoantanthanthrone and replacing the diazo group by bromine according to Sandmeyer using copper bromur) are dissolved in <B> 360 </B> parts of ilonohydrate and 26 parts of iodine iodized.
After the end of the reaction, the bromoiodanthanthrone formed is separated out in the form of its sulphate by adding dilute sulfuric acid or ice, filtered off with suction and this is decomposed with water in the usual way.
Claims (1)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE152485X | 1928-05-29 | ||
CH143400T | 1929-05-21 |
Publications (1)
Publication Number | Publication Date |
---|---|
CH152485A true CH152485A (en) | 1932-01-31 |
Family
ID=25714279
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CH152485D CH152485A (en) | 1928-05-29 | 1929-05-21 | Process for the preparation of a vat dye. |
Country Status (1)
Country | Link |
---|---|
CH (1) | CH152485A (en) |
-
1929
- 1929-05-21 CH CH152485D patent/CH152485A/en unknown
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