CH165420A - Process for obtaining a highly concentrated aqueous solution of a salt of 3,5-diiodo-2-pyridone-N-acetic acid. - Google Patents

Process for obtaining a highly concentrated aqueous solution of a salt of 3,5-diiodo-2-pyridone-N-acetic acid.

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Publication number
CH165420A
CH165420A CH165420DA CH165420A CH 165420 A CH165420 A CH 165420A CH 165420D A CH165420D A CH 165420DA CH 165420 A CH165420 A CH 165420A
Authority
CH
Switzerland
Prior art keywords
acetic acid
diiodo
pyridone
salt
obtaining
Prior art date
Application number
Other languages
German (de)
Inventor
Aktiengesellsc Farbenindustrie
Original Assignee
Ig Farbenindustrie Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ig Farbenindustrie Ag filed Critical Ig Farbenindustrie Ag
Publication of CH165420A publication Critical patent/CH165420A/en

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  • Pyridine Compounds (AREA)

Description

  

  Verfahren zur Gewinnung einer     hochkonzentrierten        wässerigen        Lösung     eines Salzes der     3.ü-Dijod-2-pyridon-N-essigsäure.       Das Hauptpatent     betrifft    ein Verfahren zur  Gewinnung einer     hochkonzentrierten    wässeri  gen     Lösung        eines    Salzes der 3.

   5 -     Dijod    -     4-          pyridon    - N -     essigsäure,    welches dadurch ge  kennzeichnet ist, dass man die     3.5-Dijod-4-          pyridoii-N-essigsäure    in wässerigem Medium  mit     Diäthylamin    behandelt.  



  Das Zusatzpatent Nr. 163441     betrifft    die  Herstellung einer konzentrierten Lösung eines  Salzes der     3.5-Dijod-4-pyridon-N-essigsäure     durch Behandlung dieser Säure mit     Bis-oxy-          äthylamin.     



  Es wurde nun gefunden, dass man auch  zu einer hochkonzentrierten Lösung eines  Salzes der     3.5-Dijod-2-pyridon-N-essigsäui-e     gelangen kann, wenn mau diese     Säure    in  wässerigem Medium mit Bis -     oxyäthylamin     behandelt. Die Lösung soll als Röntgenkon  trastmittel Verwendung finden.    <I>Beispiel:</I>  10,1     gr        3.5-Dijod-2-pyridon-N-essigsäure     werden in 2,6     gr    Bis      oxyäthylamin    und 20     cm3     Wasser unter Erwärmung gelöst.

   Die Lösung  in 100 eins enthält 50,5     gr        3.5-Dijod-2-pyri-          don-N-essigsäui#e    in Form des     Bis-oxyäthyl-          aminsalzes.  



  Process for obtaining a highly concentrated aqueous solution of a salt of 3.ü-Diiodo-2-pyridone-N-acetic acid. The main patent relates to a method for obtaining a highly concentrated aqueous solution of a salt of the 3rd

   5 - diiodo - 4 - pyridone - N - acetic acid, which is characterized in that the 3,5-diiodo-4-pyridoii-N-acetic acid is treated with diethylamine in an aqueous medium.



  The additional patent no. 163441 relates to the preparation of a concentrated solution of a salt of 3,5-diiodo-4-pyridone-N-acetic acid by treating this acid with bis-oxyethylamine.



  It has now been found that a highly concentrated solution of a salt of 3,5-diiodo-2-pyridone-N-acetic acid can also be obtained if this acid is treated with bis-oxyethylamine in an aqueous medium. The solution should be used as an X-ray contrast medium. <I> Example: </I> 10.1 g of 3.5-diiodo-2-pyridone-N-acetic acid are dissolved in 2.6 g of bis-oxyethylamine and 20 cm3 of water while heating.

   The solution in 100 one contains 50.5 grams of 3.5-diiodine-2-pyridone-N-acetic acid in the form of the bis-oxyethylamine salt.

 

Claims (1)

PATENTANSPRUCH: Verfahren zur Gewinnung einer hochkon zentrierten wässerigen Lösung eines Salzes der 3.5-Dijod-2-pyridon-N-essigsäui e, dadurch gekennzeichnet, dass man die 3 . 5 -Dijod - 2- pyi@idon-N-essigsäure mit Bis - oxyäthylamin behandelt. PATENT CLAIM: Process for obtaining a highly concentrated aqueous solution of a salt of 3.5-diiodo-2-pyridone-N-acetic acid, characterized in that the 3. 5 -diiodine-2- pyi @ idon-N-acetic acid treated with bis-oxyethylamine.
CH165420D 1931-10-15 1932-06-02 Process for obtaining a highly concentrated aqueous solution of a salt of 3,5-diiodo-2-pyridone-N-acetic acid. CH165420A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE165420X 1931-10-15
CH161687T 1932-06-02

Publications (1)

Publication Number Publication Date
CH165420A true CH165420A (en) 1933-11-15

Family

ID=25717451

Family Applications (1)

Application Number Title Priority Date Filing Date
CH165420D CH165420A (en) 1931-10-15 1932-06-02 Process for obtaining a highly concentrated aqueous solution of a salt of 3,5-diiodo-2-pyridone-N-acetic acid.

Country Status (1)

Country Link
CH (1) CH165420A (en)

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