CA2861872C - Methods of isolating (4-chloro-2-fluoro-3-substituted-phenyl)boronates and methods of using the same - Google Patents
Methods of isolating (4-chloro-2-fluoro-3-substituted-phenyl)boronates and methods of using the same Download PDFInfo
- Publication number
- CA2861872C CA2861872C CA2861872A CA2861872A CA2861872C CA 2861872 C CA2861872 C CA 2861872C CA 2861872 A CA2861872 A CA 2861872A CA 2861872 A CA2861872 A CA 2861872A CA 2861872 C CA2861872 C CA 2861872C
- Authority
- CA
- Canada
- Prior art keywords
- chloro
- fluoro
- substituted
- carbon dioxide
- solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
- C07D213/79—Acids; Esters
- C07D213/803—Processes of preparation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
- C07D213/79—Acids; Esters
- C07D213/803—Processes of preparation
- C07D213/807—Processes of preparation by oxidation of pyridines or condensed pyridines
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
- C07F5/02—Boron compounds
- C07F5/025—Boronic and borinic acid compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pyridine Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CA3085614A CA3085614C (en) | 2011-12-30 | 2012-12-28 | Methods of isolating (4-chloro-2-fluoro-3-substituted-phenyl)boronates and methods of using the same |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201161582175P | 2011-12-30 | 2011-12-30 | |
| US61/582,175 | 2011-12-30 | ||
| PCT/US2012/071920 WO2013101987A1 (en) | 2011-12-30 | 2012-12-28 | Methods of isolating (4-chloro-2-fluoro-3-substituted-phenyl) boronates and methods of using the same |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA3085614A Division CA3085614C (en) | 2011-12-30 | 2012-12-28 | Methods of isolating (4-chloro-2-fluoro-3-substituted-phenyl)boronates and methods of using the same |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2861872A1 CA2861872A1 (en) | 2013-07-04 |
| CA2861872C true CA2861872C (en) | 2020-09-15 |
Family
ID=48695352
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2861872A Active CA2861872C (en) | 2011-12-30 | 2012-12-28 | Methods of isolating (4-chloro-2-fluoro-3-substituted-phenyl)boronates and methods of using the same |
| CA3085614A Active CA3085614C (en) | 2011-12-30 | 2012-12-28 | Methods of isolating (4-chloro-2-fluoro-3-substituted-phenyl)boronates and methods of using the same |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA3085614A Active CA3085614C (en) | 2011-12-30 | 2012-12-28 | Methods of isolating (4-chloro-2-fluoro-3-substituted-phenyl)boronates and methods of using the same |
Country Status (16)
| Country | Link |
|---|---|
| US (2) | US9045502B2 (https=) |
| EP (1) | EP2797932B1 (https=) |
| JP (1) | JP6068501B2 (https=) |
| KR (1) | KR102065950B1 (https=) |
| CN (1) | CN104080791B (https=) |
| AR (1) | AR089629A1 (https=) |
| AU (1) | AU2012362364B2 (https=) |
| BR (1) | BR112014016049B8 (https=) |
| CA (2) | CA2861872C (https=) |
| CO (1) | CO7010844A2 (https=) |
| IL (1) | IL233355A (https=) |
| IN (1) | IN2014DN05755A (https=) |
| MX (1) | MX356476B (https=) |
| PL (1) | PL2797932T3 (https=) |
| RU (1) | RU2626975C2 (https=) |
| WO (1) | WO2013101987A1 (https=) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| PL2934139T3 (pl) * | 2012-12-21 | 2019-01-31 | Dow Agrosciences Llc | Kompozycje chwastobójcze zawierające kwas 4-amino-3-chloro-6-(4-chloro-2-fluoro-3-metoksyfenylo)pirydyno-2-karboksylowy i flurtamon |
| JP6434522B2 (ja) | 2013-09-05 | 2018-12-05 | ダウ アグロサイエンシィズ エルエルシー | ホウ素化アレーンを生成する方法 |
| TW201625354A (zh) | 2014-06-16 | 2016-07-16 | 陶氏農業科學公司 | 用於製備氧硼基化芳烴之方法 |
| RU2018144344A (ru) * | 2016-05-19 | 2020-06-19 | ДАУ АГРОСАЙЕНСИЗ ЭлЭлСи | Синтез 6-арил-4-аминопиколинатов и 2-арил-6-аминопиримидин-4-карбоксилатов прямым сочетанием сузуки |
| CN106450633B (zh) * | 2016-10-17 | 2022-07-01 | 北京真空电子技术研究所(中国电子科技集团公司第十二研究所） | 一种正交场放大器 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AR037228A1 (es) * | 2001-07-30 | 2004-11-03 | Dow Agrosciences Llc | Compuestos del acido 6-(aril o heteroaril)-4-aminopicolinico, composicion herbicida que los comprende y metodo para controlar vegetacion no deseada |
| DE10150615A1 (de) * | 2001-10-12 | 2003-04-30 | Clariant Gmbh | Verfahren zur metallorganischen Herstellung organischer Zwischenprodukte |
| DE602007008052D1 (de) * | 2006-01-13 | 2010-09-09 | Dow Agrosciences Llc | 2-(polysubstituiertes aryl)-6-amino-5-halogen-4-pyrimidincarbonsäuren und deren verwendung als herbizide |
| MY143535A (en) * | 2006-01-13 | 2011-05-31 | Dow Agrosciences Llc | 6-(poly-substituted aryl)-4-aminopicolinates and their use as herbicides |
| US7964758B2 (en) * | 2006-02-13 | 2011-06-21 | Nissan Chemical Industries, Ltd. | Process for production of 2-(substituted phenyl)-3,3,3-trifluoropropene compound |
| WO2009023438A1 (en) * | 2007-08-13 | 2009-02-19 | Dow Agrosciences Llc | 2-(2-fluoro-substituted phenyl)-6-amino-5-chloro-4-pyrimidinecarboxylates and their use as herbicides |
| BRPI0816075A2 (pt) * | 2007-08-30 | 2015-02-24 | Dow Agrosciences Llc | 2-(fenil substituído)-6-amino-5-alcóxi, tioalcóxi e aminoalquil-4-pirimidinacarboxilatos e seus usos como herbicidas |
| HUE030847T2 (hu) * | 2007-10-02 | 2017-06-28 | Dow Agrosciences Llc | 2-szubsztituált-6-amino-5-alkil-, alkenil- vagy alkinil-4-pirimidin-karbonsavak és 6-szubsztituált-4-amino-3-alkil-, alkenil- vagy alkinil-pikolinsavak és alkalmazásuk herbicidként |
| JP5501979B2 (ja) * | 2008-01-11 | 2014-05-28 | ダウ アグロサイエンシィズ エルエルシー | １−フルオロ−２−置換−３−クロロベンゼンの選択的脱プロトン化及び官能化の方法 |
| AU2012275201B2 (en) * | 2011-06-30 | 2016-05-12 | Corteva Agriscience Llc | 3-alkoxy, thioalkyl and amino-4-amino-6-(substituted)picolinates and their use as herbicides |
-
2012
- 2012-12-28 US US13/729,580 patent/US9045502B2/en active Active
- 2012-12-28 CA CA2861872A patent/CA2861872C/en active Active
- 2012-12-28 CA CA3085614A patent/CA3085614C/en active Active
- 2012-12-28 RU RU2014131453A patent/RU2626975C2/ru active
- 2012-12-28 WO PCT/US2012/071920 patent/WO2013101987A1/en not_active Ceased
- 2012-12-28 AU AU2012362364A patent/AU2012362364B2/en active Active
- 2012-12-28 EP EP12861211.6A patent/EP2797932B1/en active Active
- 2012-12-28 IN IN5755DEN2014 patent/IN2014DN05755A/en unknown
- 2012-12-28 PL PL12861211T patent/PL2797932T3/pl unknown
- 2012-12-28 CN CN201280068666.XA patent/CN104080791B/zh active Active
- 2012-12-28 JP JP2014550485A patent/JP6068501B2/ja active Active
- 2012-12-28 MX MX2014008010A patent/MX356476B/es active IP Right Grant
- 2012-12-28 KR KR1020147020893A patent/KR102065950B1/ko active Active
- 2012-12-28 BR BR112014016049A patent/BR112014016049B8/pt active IP Right Grant
-
2013
- 2013-01-02 AR ARP130100012A patent/AR089629A1/es active IP Right Grant
-
2014
- 2014-06-24 IL IL233355A patent/IL233355A/en active IP Right Grant
- 2014-07-18 CO CO14156101A patent/CO7010844A2/es unknown
-
2015
- 2015-05-13 US US14/711,540 patent/US9376390B2/en active Active
Also Published As
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CA2861631C (en) | Methods of forming 4-chloro-2-fluoro-3-substituted-phenylboronic acid pinacol esters and methods of using the same | |
| CA2861872C (en) | Methods of isolating (4-chloro-2-fluoro-3-substituted-phenyl)boronates and methods of using the same | |
| RU2616621C2 (ru) | Способы получения метил 4-амино-3-хлор-6-(4-хлор-2-фтор-3-метоксифенил)пиридин-2-карбоксилата | |
| JP6491475B2 (ja) | ４−クロロ−２−フルオロ−３−置換−フェニルボロン酸を単離する方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request |
Effective date: 20171220 |
|
| MPN | Maintenance fee for patent paid |
Free format text: FEE DESCRIPTION TEXT: MF (PATENT, 12TH ANNIV.) - STANDARD Year of fee payment: 12 |
|
| U00 | Fee paid |
Free format text: ST27 STATUS EVENT CODE: A-4-4-U10-U00-U101 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: MAINTENANCE REQUEST RECEIVED Effective date: 20241206 |
|
| U11 | Full renewal or maintenance fee paid |
Free format text: ST27 STATUS EVENT CODE: A-4-4-U10-U11-U102 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: MAINTENANCE FEE PAYMENT DETERMINED COMPLIANT Effective date: 20241206 Free format text: ST27 STATUS EVENT CODE: A-4-4-U10-U11-U102 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: MAINTENANCE FEE PAYMENT PAID IN FULL Effective date: 20241206 |
|
| MPN | Maintenance fee for patent paid |
Free format text: FEE DESCRIPTION TEXT: MF (PATENT, 13TH ANNIV.) - STANDARD Year of fee payment: 13 |
|
| U00 | Fee paid |
Free format text: ST27 STATUS EVENT CODE: A-4-4-U10-U00-U101 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: MAINTENANCE REQUEST RECEIVED Effective date: 20251209 |
|
| U11 | Full renewal or maintenance fee paid |
Free format text: ST27 STATUS EVENT CODE: A-4-4-U10-U11-U102 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: MAINTENANCE FEE PAYMENT PAID IN FULL Effective date: 20251209 |