KR102065950B1 - (4-클로로-2-플루오로-3-치환된-페닐) 보로네이트의 단리 방법 및 그의 사용 방법 - Google Patents

(4-클로로-2-플루오로-3-치환된-페닐) 보로네이트의 단리 방법 및 그의 사용 방법 Download PDF

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KR102065950B1
KR102065950B1 KR1020147020893A KR20147020893A KR102065950B1 KR 102065950 B1 KR102065950 B1 KR 102065950B1 KR 1020147020893 A KR1020147020893 A KR 1020147020893A KR 20147020893 A KR20147020893 A KR 20147020893A KR 102065950 B1 KR102065950 B1 KR 102065950B1
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chloro
fluoro
substituted
methyl
solution
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KR20140117443A (ko
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조시안 오펜하이머
캐써린 에이 메닝
대니얼 알 헨튼
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다우 아그로사이언시즈 엘엘씨
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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D213/00Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/78Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C07D213/79Acids; Esters
    • C07D213/803Processes of preparation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F5/00Compounds containing elements of Groups 3 or 13 of the Periodic Table
    • C07F5/02Boron compounds
    • C07F5/025Boronic and borinic acid compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D213/00Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/78Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C07D213/79Acids; Esters
    • C07D213/803Processes of preparation
    • C07D213/807Processes of preparation by oxidation of pyridines or condensed pyridines

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pyridine Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1020147020893A 2011-12-30 2012-12-28 (4-클로로-2-플루오로-3-치환된-페닐) 보로네이트의 단리 방법 및 그의 사용 방법 Active KR102065950B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201161582175P 2011-12-30 2011-12-30
US61/582,175 2011-12-30
PCT/US2012/071920 WO2013101987A1 (en) 2011-12-30 2012-12-28 Methods of isolating (4-chloro-2-fluoro-3-substituted-phenyl) boronates and methods of using the same

Publications (2)

Publication Number Publication Date
KR20140117443A KR20140117443A (ko) 2014-10-07
KR102065950B1 true KR102065950B1 (ko) 2020-01-14

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KR1020147020893A Active KR102065950B1 (ko) 2011-12-30 2012-12-28 (4-클로로-2-플루오로-3-치환된-페닐) 보로네이트의 단리 방법 및 그의 사용 방법

Country Status (16)

Country Link
US (2) US9045502B2 (https=)
EP (1) EP2797932B1 (https=)
JP (1) JP6068501B2 (https=)
KR (1) KR102065950B1 (https=)
CN (1) CN104080791B (https=)
AR (1) AR089629A1 (https=)
AU (1) AU2012362364B2 (https=)
BR (1) BR112014016049B8 (https=)
CA (2) CA2861872C (https=)
CO (1) CO7010844A2 (https=)
IL (1) IL233355A (https=)
IN (1) IN2014DN05755A (https=)
MX (1) MX356476B (https=)
PL (1) PL2797932T3 (https=)
RU (1) RU2626975C2 (https=)
WO (1) WO2013101987A1 (https=)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PL2934139T3 (pl) * 2012-12-21 2019-01-31 Dow Agrosciences Llc Kompozycje chwastobójcze zawierające kwas 4-amino-3-chloro-6-(4-chloro-2-fluoro-3-metoksyfenylo)pirydyno-2-karboksylowy i flurtamon
JP6434522B2 (ja) 2013-09-05 2018-12-05 ダウ アグロサイエンシィズ エルエルシー ホウ素化アレーンを生成する方法
TW201625354A (zh) 2014-06-16 2016-07-16 陶氏農業科學公司 用於製備氧硼基化芳烴之方法
RU2018144344A (ru) * 2016-05-19 2020-06-19 ДАУ АГРОСАЙЕНСИЗ ЭлЭлСи Синтез 6-арил-4-аминопиколинатов и 2-арил-6-аминопиримидин-4-карбоксилатов прямым сочетанием сузуки
CN106450633B (zh) * 2016-10-17 2022-07-01 北京真空电子技术研究所(中国电子科技集团公司第十二研究所) 一种正交场放大器

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20090182168A1 (en) * 2008-01-11 2009-07-16 Dow Agrosciences Llc Process for the selective deprotonation and functionalization of 1-fluoro-2-substituted-3-chlorobenzenes
US7964758B2 (en) 2006-02-13 2011-06-21 Nissan Chemical Industries, Ltd. Process for production of 2-(substituted phenyl)-3,3,3-trifluoropropene compound

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AR037228A1 (es) * 2001-07-30 2004-11-03 Dow Agrosciences Llc Compuestos del acido 6-(aril o heteroaril)-4-aminopicolinico, composicion herbicida que los comprende y metodo para controlar vegetacion no deseada
DE10150615A1 (de) * 2001-10-12 2003-04-30 Clariant Gmbh Verfahren zur metallorganischen Herstellung organischer Zwischenprodukte
DE602007008052D1 (de) * 2006-01-13 2010-09-09 Dow Agrosciences Llc 2-(polysubstituiertes aryl)-6-amino-5-halogen-4-pyrimidincarbonsäuren und deren verwendung als herbizide
MY143535A (en) * 2006-01-13 2011-05-31 Dow Agrosciences Llc 6-(poly-substituted aryl)-4-aminopicolinates and their use as herbicides
WO2009023438A1 (en) * 2007-08-13 2009-02-19 Dow Agrosciences Llc 2-(2-fluoro-substituted phenyl)-6-amino-5-chloro-4-pyrimidinecarboxylates and their use as herbicides
BRPI0816075A2 (pt) * 2007-08-30 2015-02-24 Dow Agrosciences Llc 2-(fenil substituído)-6-amino-5-alcóxi, tioalcóxi e aminoalquil-4-pirimidinacarboxilatos e seus usos como herbicidas
HUE030847T2 (hu) * 2007-10-02 2017-06-28 Dow Agrosciences Llc 2-szubsztituált-6-amino-5-alkil-, alkenil- vagy alkinil-4-pirimidin-karbonsavak és 6-szubsztituált-4-amino-3-alkil-, alkenil- vagy alkinil-pikolinsavak és alkalmazásuk herbicidként
AU2012275201B2 (en) * 2011-06-30 2016-05-12 Corteva Agriscience Llc 3-alkoxy, thioalkyl and amino-4-amino-6-(substituted)picolinates and their use as herbicides

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7964758B2 (en) 2006-02-13 2011-06-21 Nissan Chemical Industries, Ltd. Process for production of 2-(substituted phenyl)-3,3,3-trifluoropropene compound
US20090182168A1 (en) * 2008-01-11 2009-07-16 Dow Agrosciences Llc Process for the selective deprotonation and functionalization of 1-fluoro-2-substituted-3-chlorobenzenes

Also Published As

Publication number Publication date
JP2015507633A (ja) 2015-03-12
BR112014016049A2 (pt) 2017-06-13
IL233355A0 (en) 2014-08-31
BR112014016049B1 (pt) 2019-12-17
WO2013101987A1 (en) 2013-07-04
MX2014008010A (es) 2015-03-05
CA2861872A1 (en) 2013-07-04
US9045502B2 (en) 2015-06-02
KR20140117443A (ko) 2014-10-07
AR089629A1 (es) 2014-09-03
US9376390B2 (en) 2016-06-28
CA3085614A1 (en) 2013-07-04
EP2797932A4 (en) 2015-10-07
AU2012362364B2 (en) 2017-06-29
JP6068501B2 (ja) 2017-01-25
BR112014016049A8 (pt) 2017-07-04
RU2626975C2 (ru) 2017-08-02
EP2797932B1 (en) 2017-02-01
CN104080791A (zh) 2014-10-01
BR112014016049B8 (pt) 2022-10-11
IL233355A (en) 2017-12-31
AU2012362364A1 (en) 2014-07-31
MX356476B (es) 2018-05-30
NZ627196A (en) 2015-09-25
CA3085614C (en) 2023-01-24
CA2861872C (en) 2020-09-15
US20150239843A1 (en) 2015-08-27
US20130172567A1 (en) 2013-07-04
CO7010844A2 (es) 2014-07-31
PL2797932T3 (pl) 2017-08-31
EP2797932A1 (en) 2014-11-05
IN2014DN05755A (https=) 2015-04-10
RU2014131453A (ru) 2016-02-20
CN104080791B (zh) 2016-12-07

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