CA2455503C - Process to manufacture flexible polyurethane foams - Google Patents
Process to manufacture flexible polyurethane foams Download PDFInfo
- Publication number
- CA2455503C CA2455503C CA2455503A CA2455503A CA2455503C CA 2455503 C CA2455503 C CA 2455503C CA 2455503 A CA2455503 A CA 2455503A CA 2455503 A CA2455503 A CA 2455503A CA 2455503 C CA2455503 C CA 2455503C
- Authority
- CA
- Canada
- Prior art keywords
- polyol
- foam
- polyol compound
- polyols
- autocatalytic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/48—Polyethers
- C08G18/4833—Polyethers containing oxyethylene units
- C08G18/4837—Polyethers containing oxyethylene units and other oxyalkylene units
- C08G18/4841—Polyethers containing oxyethylene units and other oxyalkylene units containing oxyethylene end groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/48—Polyethers
- C08G18/50—Polyethers having heteroatoms other than oxygen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/48—Polyethers
- C08G18/4804—Two or more polyethers of different physical or chemical nature
- C08G18/482—Mixtures of polyethers containing at least one polyether containing nitrogen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/48—Polyethers
- C08G18/50—Polyethers having heteroatoms other than oxygen
- C08G18/5021—Polyethers having heteroatoms other than oxygen having nitrogen
- C08G18/5024—Polyethers having heteroatoms other than oxygen having nitrogen containing primary and/or secondary amino groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G2110/00—Foam properties
- C08G2110/0008—Foam properties flexible
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G2110/00—Foam properties
- C08G2110/0041—Foam properties having specified density
- C08G2110/005—< 50kg/m3
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G2110/00—Foam properties
- C08G2110/0083—Foam properties prepared using water as the sole blowing agent
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyurethanes Or Polyureas (AREA)
- Treatments Of Macromolecular Shaped Articles (AREA)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US31257601P | 2001-08-15 | 2001-08-15 | |
US60/312,576 | 2001-08-15 | ||
PCT/US2002/026222 WO2003016372A1 (en) | 2001-08-15 | 2002-08-15 | Process to manufacture flexible polyurethane foams |
Publications (2)
Publication Number | Publication Date |
---|---|
CA2455503A1 CA2455503A1 (en) | 2003-02-27 |
CA2455503C true CA2455503C (en) | 2011-03-22 |
Family
ID=23212098
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA2455503A Expired - Fee Related CA2455503C (en) | 2001-08-15 | 2002-08-15 | Process to manufacture flexible polyurethane foams |
Country Status (15)
Country | Link |
---|---|
US (1) | US7361695B2 (de) |
EP (1) | EP1419189B1 (de) |
JP (1) | JP4220384B2 (de) |
KR (1) | KR100909946B1 (de) |
CN (1) | CN1262569C (de) |
AT (1) | ATE497983T1 (de) |
BR (1) | BRPI0211861B1 (de) |
CA (1) | CA2455503C (de) |
DE (1) | DE60239136D1 (de) |
ES (1) | ES2357642T3 (de) |
HU (1) | HU229193B1 (de) |
MX (1) | MXPA04001427A (de) |
TW (1) | TW592813B (de) |
WO (1) | WO2003016372A1 (de) |
ZA (1) | ZA200400647B (de) |
Families Citing this family (59)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2002022702A1 (en) * | 2000-09-13 | 2002-03-21 | Dow Global Technologies Inc. | Polyols with autocatalytic characteristics and polyurethane products made therefrom |
WO2004113410A1 (en) * | 2003-06-13 | 2004-12-29 | Dow Global Technologies Inc. | Catalyst composition to get polyurethane product with good hydrolysis resistance |
DE10337319A1 (de) | 2003-08-12 | 2005-03-17 | Basf Ag | Verfahren zur Herstellung von Polyetheralkoholen |
US7078443B2 (en) * | 2003-10-22 | 2006-07-18 | Intellectual Property Holdings, Llc | Viscoelastic foam layer and composition |
JP4771367B2 (ja) * | 2003-10-28 | 2011-09-14 | 三井化学株式会社 | 軟質ポリウレタンフォームおよびその用途 |
KR20060121231A (ko) * | 2003-12-23 | 2006-11-28 | 다우 글로벌 테크놀로지스 인크. | 이민 결합 및 3급 아민을 포함하는 비휘산성 촉매, 및그로부터 제조된 폴리우레탄 생성물 |
ATE536383T1 (de) * | 2003-12-23 | 2011-12-15 | Dow Global Technologies Llc | Verfahren zur herstellung von polyurethanprodukten unter verwendung von autokatalytischen tert.-amin-verkappten polyetherpolyolen |
CA2553728C (en) * | 2004-03-31 | 2012-11-27 | Dow Global Technologies Inc. | A urethane-modified isocyanate composition and polyurethane product therefrom |
WO2006055396A1 (en) * | 2004-11-17 | 2006-05-26 | Dow Global Technologies, Inc. | Acid blocked, amine based, autocatalytic polyols and polyurethane foams made therefrom |
CN101287783B (zh) * | 2005-10-14 | 2011-11-09 | 陶氏环球技术有限责任公司 | 复合制品和使用异氰酸酯基封端的预聚物作为粘结剂的制备方法 |
PT2069417E (pt) * | 2006-09-25 | 2013-03-25 | Dow Global Technologies Llc | Espumas de poliuretano feitas a partir de hidroximetilo - contendo polióis poliéster e amina terciária ¿ contendo polióis |
US8552078B2 (en) | 2006-10-17 | 2013-10-08 | Air Products And Chemicals, Inc. | Crosslinkers for improving stability of polyurethane foams |
US8367870B2 (en) | 2007-09-19 | 2013-02-05 | Air Products And Chemicals, Inc. | Autocatalytic polyols |
EP2072556A1 (de) * | 2007-12-17 | 2009-06-24 | Sika Technology AG | Verfahren zur Herstellung von hydroxyfunktionellen Polymeren, die hieraus gewinnbaren Isocyanatgruppen-endständigen Polyadditionsprodukte sowie deren Verwendung |
KR101660999B1 (ko) * | 2008-10-24 | 2016-09-28 | 바스프 에스이 | 점탄성 폴리우레탄 연질 폼의 제조 방법 |
EP2403887A1 (de) * | 2009-03-05 | 2012-01-11 | Dow Global Technologies LLC (formerly Known As Dow Global Technologies Inc.) | Polyole aus hppo und daraus hergestellte polyurethanprodukte |
US10113043B2 (en) * | 2010-02-26 | 2018-10-30 | Twin Brook Capital Partners, Llc | Polyurethane gel particles, methods and use in flexible foams |
US20130296449A1 (en) * | 2010-02-26 | 2013-11-07 | Peterson Chemical Technology, Inc. | Polyurethane Gel-Like Polymers, Methods and Use in Flexible Foams |
JP5759539B2 (ja) | 2010-06-15 | 2015-08-05 | ダウ グローバル テクノロジーズ エルエルシー | 使用済みカーペット繊維を用いるポリウレタンフォーム床材製造物の作製方法 |
US9334382B2 (en) | 2010-07-09 | 2016-05-10 | Air Products And Chemicals, Inc. | Process for producing flexible polyurethane foam |
US10119002B2 (en) | 2010-07-09 | 2018-11-06 | Evonik Degussa Gmbh | Additives for improving polyurethane foam performance |
EP2621987B1 (de) * | 2010-10-01 | 2015-07-29 | Dow Global Technologies LLC | Verfahren zur herstellung eines flexiblen polyurethanschaumstoffes mit niedriger dichter und hoher elastizität |
US9968919B2 (en) | 2011-06-29 | 2018-05-15 | Evonik Degussa Gmbh | Reducing emissions in polyurethane foam |
US9145466B2 (en) | 2011-07-07 | 2015-09-29 | Air Products And Chemicals, Inc. | Process for producing flexible polyurethane foam using natural oil polyols |
US9447223B2 (en) | 2011-07-07 | 2016-09-20 | Air Products And Chemicals, Inc. | Additives for improving natural oil based polyurethane foam performance |
US10106638B2 (en) | 2011-07-29 | 2018-10-23 | Evonik Degussa Gmbh | Reduced emissions low density spray polyurethane foam |
US9273175B2 (en) | 2011-10-03 | 2016-03-01 | Air Products And Chemicals, Inc. | Tertiary amine composition and method for making the composition |
US9765009B2 (en) | 2011-11-17 | 2017-09-19 | Evonik Degussa Gmbh | Processes, products, and compositions having tetraalkylguanidine salt of aromatic carboxylic acid |
US9644066B2 (en) | 2011-12-29 | 2017-05-09 | Dow Global Technologies Llc | Cyclic amine compounds, compositions, and polyurethane foams made therefrom |
JP5933109B2 (ja) | 2012-03-30 | 2016-06-08 | エア プロダクツ アンド ケミカルズ インコーポレイテッドAir Products And Chemicals Incorporated | ポリウレタンフォーム製造方法、プレミックス、配合物及び製品 |
US10023681B2 (en) | 2012-10-24 | 2018-07-17 | Evonik Degussa Gmbh | Delay action catalyst for improving the stability of polyurethane systems having halogen containing blowing agents |
JP6191244B2 (ja) * | 2013-05-30 | 2017-09-06 | 旭硝子株式会社 | ポリマー分散ポリオール組成物の製造方法および引火点を上昇させる方法 |
MX2016007379A (es) | 2013-12-19 | 2016-08-19 | Air Prod & Chem | Nueva composicion de amina no emisiva para la estabilidad de vida en anaquel del sistema mejorada. |
US20170058077A1 (en) * | 2014-04-01 | 2017-03-02 | Dow Global Technologies Llc | Polyether polyol providing good blow-gel balance for polyurethane products made therefrom |
US20160075817A1 (en) | 2014-09-12 | 2016-03-17 | Air Products And Chemicals, Inc. | Low Emissions Polyurethane Foam Made with Isocyanate Reactive Amine Catalyst |
WO2016061068A1 (en) | 2014-10-13 | 2016-04-21 | Air Products And Chemicals, Inc. | Polyurethane catalysts from sulfur based salts |
CN107567469B (zh) | 2015-05-05 | 2020-12-29 | 赢创运营有限公司 | 延迟作用凝胶催化剂组合物和制备聚氨酯聚合物的方法 |
KR102610948B1 (ko) | 2015-06-01 | 2023-12-06 | 에보닉 오퍼레이션스 게엠베하 | 폴리우레탄 적용물을 위한 반응성 아민 촉매 |
US10696777B2 (en) | 2015-06-16 | 2020-06-30 | Evonik Operations Gmbh | Aldehyde scavengers mixtures for polyurethane foams |
CN107735419A (zh) | 2015-06-16 | 2018-02-23 | 赢创德固赛有限公司 | 用于聚氨酯泡沫的醛清除剂 |
CN107667129A (zh) | 2015-06-19 | 2018-02-06 | 陶氏环球技术有限责任公司 | 适用于聚氨基甲酸酯泡沫制造的自催化多元醇 |
ES2819879T3 (es) | 2016-04-12 | 2021-04-19 | Evonik Operations Gmbh | Composiciones de tensioactivos de copolímeros de siloxano-oxialquileno |
US10815331B2 (en) | 2016-06-13 | 2020-10-27 | Dow Global Technologies Llc | Autocatalytic polyols |
KR20190030214A (ko) | 2016-07-11 | 2019-03-21 | 에보니크 데구사 게엠베하 | 폴리우레탄 발포체의 제조에 유용한 아민 조성물 |
US10767008B2 (en) | 2017-01-16 | 2020-09-08 | Covestro Llc | Polymer polyols comprising amine based polyether polyols and a process for preparing these polymer polyols |
KR102543009B1 (ko) * | 2017-01-23 | 2023-06-14 | 다우 글로벌 테크놀로지스 엘엘씨 | 가요성 폴리우레탄 포움 및 제조 방법 |
CN107189028B (zh) * | 2017-06-23 | 2020-02-28 | 黎明化工研究设计院有限责任公司 | 一种环保高性能快速脱模聚氨酯反应注射成型组合物及其自催化扩链剂的制备方法 |
JP7470636B2 (ja) | 2017-11-10 | 2024-04-18 | ダウ グローバル テクノロジーズ エルエルシー | ポリウレタン発泡体系 |
EP3707184A1 (de) | 2017-11-10 | 2020-09-16 | Dow Global Technologies LLC | Polyurethanschaumsystem |
US10479862B2 (en) | 2017-12-07 | 2019-11-19 | Covestro Llc | Amine based polymer polyol stabilizers |
US10526484B2 (en) | 2017-12-20 | 2020-01-07 | Covestro Llc | Dithiocarbonate containing polyols as polymer polyol stabilizers |
EP3584726A1 (de) * | 2018-06-18 | 2019-12-25 | Covestro Deutschland AG | Verfahren und computersystem zur bestimmung von polymerprodukteigenschaften |
CN109971007B (zh) * | 2019-04-01 | 2021-05-28 | 江南大学 | 一种常温固化聚氨酯类防雾薄膜及其制备方法 |
EP3760659A1 (de) * | 2019-07-01 | 2021-01-06 | Covestro Deutschland AG | Amingestartete polyole als einbaubare katalysatoren im hr-schaum |
US11814566B2 (en) | 2020-07-13 | 2023-11-14 | L&P Property Management Company | Thermally conductive nanomaterials in flexible foam |
EP3954722A1 (de) | 2020-07-30 | 2022-02-16 | Evonik Operations GmbH | Verfahren und zusammensetzung zur herstellung von polyurethanweichschaum |
US11738487B2 (en) * | 2021-01-22 | 2023-08-29 | Covestro Llc | Processes for making molded flexible foams and flexible foams produced thereby |
US20220235168A1 (en) * | 2021-01-22 | 2022-07-28 | Covestro Llc | Processes for making molded flexible foams and flexible foams produced thereby |
US11597862B2 (en) | 2021-03-10 | 2023-03-07 | L&P Property Management Company | Thermally conductive nanomaterial coatings on flexible foam or fabrics |
Family Cites Families (22)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE235878C (de) | ||||
US3838076A (en) | 1973-03-12 | 1974-09-24 | Jefferson Chem Co Inc | Polyurethane foams from partially aminated polyether polyols |
US4049931A (en) | 1975-05-29 | 1977-09-20 | Union Carbide Corporation | Catalyst systems containing dimethylamino ether mono-ols for polyurethane foam formation |
US4383070A (en) * | 1982-05-27 | 1983-05-10 | Mobay Chemical Corporation | Storage stable polyurethane compositions |
US4530941A (en) * | 1983-01-26 | 1985-07-23 | The Dow Chemical Company | Reaction injection molded polyurethanes employing high molecular weight polyols |
US4517313A (en) | 1984-04-11 | 1985-05-14 | Abbott Laboratories | Method of making polyurethane foam |
DE3435070A1 (de) | 1984-09-25 | 1986-04-03 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von gegebenenfalls geschaeumten polyurethanen, die mit einem anderen werkstoff verbunden oder konfektioniert worden sind |
DD235878B5 (de) * | 1985-04-02 | 1994-04-28 | Basf Schwarzheide Gmbh | Verfahren zur Herstellung autokatalytisch wirkender Polyetheralkohole |
GB2199504A (en) * | 1987-01-06 | 1988-07-13 | Peter Egan | Directional dice |
US4963399A (en) | 1987-03-31 | 1990-10-16 | Union Carbide Chemicals And Plastics Company, Inc. | Polyurethane foam with low vinyl-staining tendencies |
US5223547A (en) | 1990-11-27 | 1993-06-29 | Kao Corporation | Polyurethane, process for producing the same, and process for producing polyurethane foam |
DE4135588A1 (de) | 1991-10-29 | 1993-05-06 | Basf Ag, 6700 Ludwigshafen, De | Hochreaktive, tertiaere aminogruppen gebunden enthaltende polyoxyalkylenpolyole, verfahren zu ihrer herstellung und ihre verwendung zur herstellung von polyisocyanat-polyadditionsprodukten |
GB9215488D0 (en) | 1992-07-21 | 1992-09-02 | Polyol Int Bv | Isocyanate modified amines as catalysts useful for the preparation of polyurethane materials |
US5508340A (en) * | 1993-03-10 | 1996-04-16 | R. E. Hart Labs, Inc. | Water-based, solvent-free or low voc, two-component polyurethane coatings |
IT1270979B (it) | 1993-09-30 | 1997-05-26 | Afros Spa | Procedimento e apparecchiatura per la produzione in continuo di schiume poliuretaniche in blocchi |
DE4437878A1 (de) | 1994-10-22 | 1996-04-25 | Basf Ag | Verfahren zur Herstellung von fogging-armen Polyurethan-Schaumstoffen und hierfür verwendbare spezielle Polyoxyalkylen-polyole |
DE69601328T2 (de) | 1995-06-05 | 1999-05-27 | Air Prod & Chem | Hydroxymethylchinuclidin-Katalysatorzusammensetzungen zur Herstellung von Polyurethanschäumen |
DE19744747A1 (de) | 1997-10-10 | 1999-04-15 | Basf Ag | Verfahren zur Herstellung von Polyurethan-Weichschaumstoffen |
US5874485A (en) * | 1997-11-10 | 1999-02-23 | Bayer Corporation | Flexible foams and flexible molded foams based on allophanate-modified diphenylmethane diisocyanates and processes for the production of these foams |
US6762274B2 (en) * | 2000-02-10 | 2004-07-13 | Dow Global Technologies Inc. | Low emission polyurethane polymers made with autocatalytic polyols |
CA2399835C (en) * | 2000-02-10 | 2009-11-03 | The Dow Chemical Company | Low emission polyurethane polymers made with autocatalytic polyols |
US6924321B2 (en) * | 2001-08-16 | 2005-08-02 | Dow Global Technologies Inc. | Polyols with autocatalytic characteristics and polyurethane products made therefrom |
-
2002
- 2002-08-14 TW TW091118315A patent/TW592813B/zh not_active IP Right Cessation
- 2002-08-15 DE DE60239136T patent/DE60239136D1/de not_active Expired - Lifetime
- 2002-08-15 CN CNB028158555A patent/CN1262569C/zh not_active Expired - Fee Related
- 2002-08-15 MX MXPA04001427A patent/MXPA04001427A/es active IP Right Grant
- 2002-08-15 JP JP2003521695A patent/JP4220384B2/ja not_active Expired - Fee Related
- 2002-08-15 WO PCT/US2002/026222 patent/WO2003016372A1/en active Application Filing
- 2002-08-15 CA CA2455503A patent/CA2455503C/en not_active Expired - Fee Related
- 2002-08-15 ES ES02794917T patent/ES2357642T3/es not_active Expired - Lifetime
- 2002-08-15 EP EP02794917A patent/EP1419189B1/de not_active Expired - Lifetime
- 2002-08-15 US US10/486,776 patent/US7361695B2/en not_active Expired - Lifetime
- 2002-08-15 BR BRPI0211861A patent/BRPI0211861B1/pt not_active IP Right Cessation
- 2002-08-15 HU HU0401049A patent/HU229193B1/hu not_active IP Right Cessation
- 2002-08-15 KR KR1020047002193A patent/KR100909946B1/ko active IP Right Grant
- 2002-08-15 AT AT02794917T patent/ATE497983T1/de not_active IP Right Cessation
-
2004
- 2004-01-27 ZA ZA2004/00647A patent/ZA200400647B/en unknown
Also Published As
Publication number | Publication date |
---|---|
KR20040030084A (ko) | 2004-04-08 |
TW592813B (en) | 2004-06-21 |
US20040242718A1 (en) | 2004-12-02 |
CN1541234A (zh) | 2004-10-27 |
BRPI0211861B1 (pt) | 2015-09-08 |
EP1419189B1 (de) | 2011-02-09 |
JP4220384B2 (ja) | 2009-02-04 |
ES2357642T3 (es) | 2011-04-28 |
HUP0401049A3 (en) | 2008-04-28 |
KR100909946B1 (ko) | 2009-07-30 |
US7361695B2 (en) | 2008-04-22 |
EP1419189A1 (de) | 2004-05-19 |
BR0211861A (pt) | 2004-09-21 |
HUP0401049A2 (hu) | 2004-08-30 |
ZA200400647B (en) | 2005-03-30 |
WO2003016372A1 (en) | 2003-02-27 |
DE60239136D1 (de) | 2011-03-24 |
MXPA04001427A (es) | 2004-06-03 |
HU229193B1 (hu) | 2013-09-30 |
CN1262569C (zh) | 2006-07-05 |
CA2455503A1 (en) | 2003-02-27 |
JP2005500416A (ja) | 2005-01-06 |
ATE497983T1 (de) | 2011-02-15 |
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