CA2454355C - High quality colloidal nanocrystals and methods of preparing the same in non-coordinating solvents - Google Patents

High quality colloidal nanocrystals and methods of preparing the same in non-coordinating solvents Download PDF

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Publication number
CA2454355C
CA2454355C CA2454355A CA2454355A CA2454355C CA 2454355 C CA2454355 C CA 2454355C CA 2454355 A CA2454355 A CA 2454355A CA 2454355 A CA2454355 A CA 2454355A CA 2454355 C CA2454355 C CA 2454355C
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Prior art keywords
nanocrystals
metal
ligand
cation
precursor
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Expired - Fee Related
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CA2454355A
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English (en)
French (fr)
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CA2454355A1 (en
Inventor
Xiaogang Peng
Weiyong Yu
David Battaglia
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University of Arkansas
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University of Arkansas
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Publication of CA2454355A1 publication Critical patent/CA2454355A1/en
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    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B5/00Single-crystal growth from gels
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/10Inorganic compounds or compositions
    • C30B29/40AIIIBV compounds wherein A is B, Al, Ga, In or Tl and B is N, P, As, Sb or Bi
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/10Inorganic compounds or compositions
    • C30B29/46Sulfur-, selenium- or tellurium-containing compounds
    • C30B29/48AIIBVI compounds wherein A is Zn, Cd or Hg, and B is S, Se or Te
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/60Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape characterised by shape
    • C30B29/605Products containing multiple oriented crystallites, e.g. columnar crystallites
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B7/00Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume, or surface-area of porous materials
    • G01N15/02Investigating particle size or size distribution
    • G01N15/0205Investigating particle size or size distribution by optical means, e.g. by light scattering, diffraction, holography or imaging
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume, or surface-area of porous materials
    • G01N2015/0038Investigating nanoparticles
CA2454355A 2001-07-30 2002-07-30 High quality colloidal nanocrystals and methods of preparing the same in non-coordinating solvents Expired - Fee Related CA2454355C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US30868901P 2001-07-30 2001-07-30
US60/308,689 2001-07-30
PCT/US2002/024215 WO2003050329A2 (en) 2001-07-30 2002-07-30 High quality colloidal nanocrystals and methods of preparation of the same in non-coordinating solvents

Publications (2)

Publication Number Publication Date
CA2454355A1 CA2454355A1 (en) 2003-06-19
CA2454355C true CA2454355C (en) 2011-05-10

Family

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Family Applications (1)

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CA2454355A Expired - Fee Related CA2454355C (en) 2001-07-30 2002-07-30 High quality colloidal nanocrystals and methods of preparing the same in non-coordinating solvents

Country Status (8)

Country Link
US (1) US7105051B2 (en29)
EP (1) EP1412563B1 (en29)
JP (1) JP4344613B2 (en29)
AT (1) ATE457373T1 (en29)
AU (1) AU2002365069A1 (en29)
CA (1) CA2454355C (en29)
DE (1) DE60235306D1 (en29)
WO (1) WO2003050329A2 (en29)

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Also Published As

Publication number Publication date
DE60235306D1 (de) 2010-03-25
CA2454355A1 (en) 2003-06-19
EP1412563A4 (en) 2007-08-22
US7105051B2 (en) 2006-09-12
AU2002365069A1 (en) 2003-06-23
EP1412563B1 (en) 2010-02-10
JP4344613B2 (ja) 2009-10-14
AU2002365069A8 (en) 2003-06-23
EP1412563A2 (en) 2004-04-28
WO2003050329A2 (en) 2003-06-19
WO2003050329A3 (en) 2003-09-12
ATE457373T1 (de) 2010-02-15
US20060130741A1 (en) 2006-06-22
JP2005521755A (ja) 2005-07-21

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