CA1201726A - Process for the removal of urea, ammonia and carbon dioxide from dilute aqueous solutions - Google Patents

Process for the removal of urea, ammonia and carbon dioxide from dilute aqueous solutions

Info

Publication number
CA1201726A
CA1201726A CA000390702A CA390702A CA1201726A CA 1201726 A CA1201726 A CA 1201726A CA 000390702 A CA000390702 A CA 000390702A CA 390702 A CA390702 A CA 390702A CA 1201726 A CA1201726 A CA 1201726A
Authority
CA
Canada
Prior art keywords
ammonia
urea
carbon dioxide
solution
column
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
CA000390702A
Other languages
English (en)
French (fr)
Inventor
Jan Zuidam
Petrus J.M. Van Nassau
Pierre G.M.B. Bruls
Kees Jonckers
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Unie Van Kunstmestfabrieken BV
Original Assignee
Unie Van Kunstmestfabrieken BV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Unie Van Kunstmestfabrieken BV filed Critical Unie Van Kunstmestfabrieken BV
Application granted granted Critical
Publication of CA1201726A publication Critical patent/CA1201726A/en
Expired legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/26—Fractionating columns in which vapour and liquid flow past each other, or in which the fluid is sprayed into the vapour, or in which a two-phase mixture is passed in one direction
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F9/00—Multistage treatment of water, waste water or sewage
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/58—Treatment of water, waste water, or sewage by removing specified dissolved compounds
    • C02F1/586—Treatment of water, waste water, or sewage by removing specified dissolved compounds by removing ammoniacal nitrogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
    • C07C273/04—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds from carbon dioxide and ammonia
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/02—Treatment of water, waste water, or sewage by heating
    • C02F1/025—Thermal hydrolysis
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/02—Treatment of water, waste water, or sewage by heating
    • C02F1/04—Treatment of water, waste water, or sewage by heating by distillation or evaporation
    • C02F1/048—Purification of waste water by evaporation
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/58—Treatment of water, waste water, or sewage by removing specified dissolved compounds
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00—Nature of the contaminant
    • C02F2101/10—Inorganic compounds
    • C02F2101/16—Nitrogen compounds, e.g. ammonia

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Water Supply & Treatment (AREA)
  • Hydrology & Water Resources (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Treating Waste Gases (AREA)
  • Gas Separation By Absorption (AREA)
CA000390702A 1980-11-28 1981-11-23 Process for the removal of urea, ammonia and carbon dioxide from dilute aqueous solutions Expired CA1201726A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
NL8006477 1980-11-28
NL8006477A NL8006477A (nl) 1980-11-28 1980-11-28 Werkwijze voor het verwijderen van ureum, ammoniak en kooldioxide uit verdunde waterige oplossing.

Publications (1)

Publication Number Publication Date
CA1201726A true CA1201726A (en) 1986-03-11

Family

ID=19836250

Family Applications (1)

Application Number Title Priority Date Filing Date
CA000390702A Expired CA1201726A (en) 1980-11-28 1981-11-23 Process for the removal of urea, ammonia and carbon dioxide from dilute aqueous solutions

Country Status (33)

Country Link
US (1) US4456535A (xx)
EP (1) EP0053410B1 (xx)
JP (1) JPS57118011A (xx)
KR (2) KR830007109A (xx)
AU (1) AU547371B2 (xx)
BR (1) BR8107728A (xx)
CA (1) CA1201726A (xx)
CS (1) CS227021B2 (xx)
CU (1) CU21419A (xx)
DE (1) DE3171612D1 (xx)
ES (1) ES507512A0 (xx)
FI (1) FI74947C (xx)
GR (1) GR75396B (xx)
HU (1) HU188717B (xx)
IE (1) IE53218B1 (xx)
IL (1) IL64392A (xx)
IN (1) IN156310B (xx)
MA (1) MA19335A1 (xx)
MY (1) MY8600489A (xx)
NL (1) NL8006477A (xx)
NO (1) NO154749C (xx)
NZ (1) NZ199085A (xx)
OA (1) OA06958A (xx)
PH (1) PH19196A (xx)
PL (1) PL134841B1 (xx)
PT (1) PT74046B (xx)
RO (1) RO83971B (xx)
SG (1) SG100285G (xx)
SU (1) SU1378781A3 (xx)
TR (1) TR21827A (xx)
YU (1) YU41999B (xx)
ZA (1) ZA818269B (xx)
ZW (1) ZW28781A1 (xx)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4522727A (en) * 1984-10-22 1985-06-11 Atec Inc. Process for continuous removal of ammoniacal nitrogen from aqueous streams
AT388157B (de) * 1987-07-16 1989-05-10 Vogelbusch Gmbh Verfahren zur aufbereitung von ammoniak und/oder sonstige geruchsaktive substanzen sowie feststoffe enthaltenden organisch belasteten abwaessern
NL8702530A (nl) * 1987-10-23 1989-05-16 Stamicarbon Werkwijze voor de bereiding van ureum en water uitgaande van ammoniak en kooldioxide.
IT1232670B (it) * 1989-09-15 1992-03-02 Snam Progetti Procedimento per la purificazione delle acque reflue prodotte dagli impianti di produzione dell'urea.
EP0538848A1 (en) * 1991-10-23 1993-04-28 Urea Casale S.A. Process and equipment for the hydrolysis of residual urea in the water from urea synthesis plants
US5518626A (en) * 1993-12-23 1996-05-21 United Technologies Corporation Process employing thermally sterilizable aqueous polishing agents
US5525237A (en) * 1993-12-23 1996-06-11 United Technologies Corporation Process for removing free and dissolved CO2 from aqueous solutions
US5597454A (en) * 1995-04-06 1997-01-28 Lee; Jing M. Process for producing urea
KR100398799B1 (ko) * 2001-04-04 2003-09-19 한화석유화학 주식회사 질소 함유 유기물을 포함하는 폐수의 처리공정
US6761868B2 (en) * 2001-05-16 2004-07-13 The Chemithon Corporation Process for quantitatively converting urea to ammonia on demand
US7272953B2 (en) * 2002-01-08 2007-09-25 Masterson James A Method and apparatus for separating and neutralizing ammonia
US20040177644A1 (en) * 2002-01-08 2004-09-16 Masterson James A. Method and apparatus for separating and neutralizing ammonia
US6755029B2 (en) 2002-01-08 2004-06-29 Marvin Ralph Bertrand, Jr. Ammonia separator and neutralizer
US6887449B2 (en) * 2002-11-21 2005-05-03 The Chemithon Corporation Method of quantitatively producing ammonia from urea
CN100400430C (zh) * 2006-05-18 2008-07-09 刘国胜 尿素工艺冷凝液节能净化回收工艺
EP2386346A1 (en) 2010-05-11 2011-11-16 Stamicarbon B.V. Process for the reduction of ammonia emissions in a urea manufacturing process
JP6634342B2 (ja) * 2016-05-24 2020-01-22 東洋エンジニアリング株式会社 尿素水溶液の処理方法および装置
WO2019030196A1 (en) * 2017-08-11 2019-02-14 Akzo Nobel Chemicals International B.V. PROCESS FOR CONVERTING CYCLIC ALKYLENE UREA TO THEIR CORRESPONDING ALKYLENE AMINES
DE102019208859A1 (de) 2019-06-18 2020-12-24 Skw Stickstoffwerke Piesteritz Gmbh Verfahren zur kontinuierlichen Herstellung reiner Harnstofflösungen durch Verwertung von Prozesswasser
CN111137906A (zh) * 2020-03-13 2020-05-12 安徽六国化工股份有限公司 一种尿素稀尿溶液处理装置及方法
CN112744945A (zh) * 2020-11-30 2021-05-04 安徽金禾实业股份有限公司 三氯蔗糖精馏废水氧化碱解的方法及装置

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE146751C (xx) *
DE146752C (xx) *
US3390058A (en) * 1964-06-08 1968-06-25 Toyo Koatsu Ind Inc Plural stage pressure distillation of urea synthesis effluent with liquified gas addition
ES318356A1 (es) * 1964-10-16 1966-05-16 Toyo Koatsu Ind Incorporated Metodo de depuracion de un efluente en la obtencion de urea sintetica.
US4341640A (en) * 1976-09-27 1982-07-27 Standard Oil Company Urea hydrolysis
JPS5826909B2 (ja) * 1979-09-14 1983-06-06 東洋エンジニアリング株式会社 尿素水溶液の濃縮方法

Also Published As

Publication number Publication date
ES8301841A1 (es) 1983-01-01
SU1378781A3 (ru) 1988-02-28
PL234005A1 (xx) 1982-06-21
US4456535A (en) 1984-06-26
RO83971B (ro) 1984-08-30
FI74947B (fi) 1987-12-31
OA06958A (fr) 1983-07-31
MY8600489A (en) 1986-12-31
KR860000189B1 (ko) 1986-03-03
NO154749C (no) 1986-12-17
CU21419A (es) 1983-12-21
BR8107728A (pt) 1982-08-31
AU547371B2 (en) 1985-10-17
PT74046B (fr) 1983-04-26
JPS57118011A (en) 1982-07-22
FI813811L (fi) 1982-05-29
EP0053410B1 (en) 1985-07-31
SG100285G (en) 1986-07-18
ES507512A0 (es) 1983-01-01
IL64392A (en) 1984-10-31
IE812785L (en) 1982-05-28
PH19196A (en) 1986-01-28
GR75396B (xx) 1984-07-13
EP0053410A1 (en) 1982-06-09
IL64392A0 (en) 1982-02-28
MA19335A1 (fr) 1982-07-01
CS227021B2 (en) 1984-04-16
ZW28781A1 (en) 1982-02-24
ZA818269B (en) 1983-06-29
HU188717B (en) 1986-05-28
NL8006477A (nl) 1982-06-16
PT74046A (fr) 1981-12-01
NZ199085A (en) 1985-08-30
PL134841B1 (en) 1985-09-30
NO814070L (no) 1982-06-01
YU274181A (en) 1983-02-28
FI74947C (fi) 1988-04-11
TR21827A (tr) 1985-08-15
AU7794181A (en) 1982-06-03
RO83971A (ro) 1984-06-21
IN156310B (xx) 1985-06-22
NO154749B (no) 1986-09-08
DE3171612D1 (en) 1985-09-05
IE53218B1 (en) 1988-09-14
KR830007109A (ko) 1983-10-14
YU41999B (en) 1988-04-30

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Legal Events

Date Code Title Description
MKEX Expiry