CA1091907A - Method of manufacturing an object of silicon nitride - Google Patents
Method of manufacturing an object of silicon nitrideInfo
- Publication number
- CA1091907A CA1091907A CA270,575A CA270575A CA1091907A CA 1091907 A CA1091907 A CA 1091907A CA 270575 A CA270575 A CA 270575A CA 1091907 A CA1091907 A CA 1091907A
- Authority
- CA
- Canada
- Prior art keywords
- layer
- porous layer
- temperature
- pressure medium
- impermeable
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229910052581 Si3N4 Inorganic materials 0.000 title claims abstract description 26
- HQVNEWCFYHHQES-UHFFFAOYSA-N silicon nitride Chemical compound N12[Si]34N5[Si]62N3[Si]51N64 HQVNEWCFYHHQES-UHFFFAOYSA-N 0.000 title claims abstract description 26
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 8
- 239000000843 powder Substances 0.000 claims abstract description 49
- 239000000463 material Substances 0.000 claims abstract description 21
- 238000005245 sintering Methods 0.000 claims abstract description 18
- 238000010438 heat treatment Methods 0.000 claims abstract description 13
- 238000000462 isostatic pressing Methods 0.000 claims abstract description 10
- 238000007872 degassing Methods 0.000 claims abstract description 8
- 230000015572 biosynthetic process Effects 0.000 claims abstract 6
- 239000011521 glass Substances 0.000 claims description 28
- 238000002844 melting Methods 0.000 claims description 13
- 238000000034 method Methods 0.000 claims description 11
- 238000005056 compaction Methods 0.000 claims description 5
- 238000007496 glass forming Methods 0.000 claims description 4
- 239000007769 metal material Substances 0.000 claims description 2
- 208000036366 Sensation of pressure Diseases 0.000 abstract description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 16
- 239000011230 binding agent Substances 0.000 description 9
- 229910052681 coesite Inorganic materials 0.000 description 8
- 229910052906 cristobalite Inorganic materials 0.000 description 8
- 239000000377 silicon dioxide Substances 0.000 description 8
- 235000012239 silicon dioxide Nutrition 0.000 description 8
- 229910052682 stishovite Inorganic materials 0.000 description 8
- 229910052905 tridymite Inorganic materials 0.000 description 8
- 239000002775 capsule Substances 0.000 description 6
- 239000000654 additive Substances 0.000 description 5
- 230000000996 additive effect Effects 0.000 description 5
- 238000003825 pressing Methods 0.000 description 5
- 239000007789 gas Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000000395 magnesium oxide Substances 0.000 description 3
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 239000001993 wax Substances 0.000 description 3
- 239000005995 Aluminium silicate Substances 0.000 description 2
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 239000000020 Nitrocellulose Substances 0.000 description 2
- FJWGYAHXMCUOOM-QHOUIDNNSA-N [(2s,3r,4s,5r,6r)-2-[(2r,3r,4s,5r,6s)-4,5-dinitrooxy-2-(nitrooxymethyl)-6-[(2r,3r,4s,5r,6s)-4,5,6-trinitrooxy-2-(nitrooxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-3,5-dinitrooxy-6-(nitrooxymethyl)oxan-4-yl] nitrate Chemical compound O([C@@H]1O[C@@H]([C@H]([C@H](O[N+]([O-])=O)[C@H]1O[N+]([O-])=O)O[C@H]1[C@@H]([C@@H](O[N+]([O-])=O)[C@H](O[N+]([O-])=O)[C@@H](CO[N+]([O-])=O)O1)O[N+]([O-])=O)CO[N+](=O)[O-])[C@@H]1[C@@H](CO[N+]([O-])=O)O[C@@H](O[N+]([O-])=O)[C@H](O[N+]([O-])=O)[C@H]1O[N+]([O-])=O FJWGYAHXMCUOOM-QHOUIDNNSA-N 0.000 description 2
- 235000012211 aluminium silicate Nutrition 0.000 description 2
- PZZYQPZGQPZBDN-UHFFFAOYSA-N aluminium silicate Chemical compound O=[Al]O[Si](=O)O[Al]=O PZZYQPZGQPZBDN-UHFFFAOYSA-N 0.000 description 2
- 229910000323 aluminium silicate Inorganic materials 0.000 description 2
- 239000007900 aqueous suspension Substances 0.000 description 2
- 230000001419 dependent effect Effects 0.000 description 2
- 238000007598 dipping method Methods 0.000 description 2
- 238000010494 dissociation reaction Methods 0.000 description 2
- 230000005593 dissociations Effects 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
- 150000004767 nitrides Chemical class 0.000 description 2
- 229920001220 nitrocellulos Polymers 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 101150034533 ATIC gene Proteins 0.000 description 1
- RZVAJINKPMORJF-UHFFFAOYSA-N Acetaminophen Chemical compound CC(=O)NC1=CC=C(O)C=C1 RZVAJINKPMORJF-UHFFFAOYSA-N 0.000 description 1
- 101100536354 Drosophila melanogaster tant gene Proteins 0.000 description 1
- 101710083262 Ectin Proteins 0.000 description 1
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 1
- 101100001347 Mus musculus Akt1s1 gene Proteins 0.000 description 1
- 101100128231 Streptomyces exfoliatus lieB gene Proteins 0.000 description 1
- 230000035508 accumulation Effects 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 229920005822 acrylic binder Polymers 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 230000000332 continued effect Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000000156 glass melt Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000006060 molten glass Substances 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- 239000011733 molybdenum Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 229920000915 polyvinyl chloride Polymers 0.000 description 1
- 239000004800 polyvinyl chloride Substances 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000005297 pyrex Substances 0.000 description 1
- 239000003870 refractory metal Substances 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- 239000010937 tungsten Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
- C04B35/58—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on borides, nitrides, i.e. nitrides, oxynitrides, carbonitrides or oxycarbonitrides or silicides
- C04B35/584—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on borides, nitrides, i.e. nitrides, oxynitrides, carbonitrides or oxycarbonitrides or silicides based on silicon nitride
- C04B35/593—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on borides, nitrides, i.e. nitrides, oxynitrides, carbonitrides or oxycarbonitrides or silicides based on silicon nitride obtained by pressure sintering
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F3/00—Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
- B22F3/12—Both compacting and sintering
- B22F3/1208—Containers or coating used therefor
- B22F3/1216—Container composition
- B22F3/1241—Container composition layered
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F3/00—Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
- B22F3/12—Both compacting and sintering
- B22F3/1208—Containers or coating used therefor
- B22F3/125—Initially porous container
Landscapes
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Ceramic Products (AREA)
- Powder Metallurgy (AREA)
- Laminated Bodies (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE7600919-0 | 1976-01-29 | ||
| SE7600919A SE396371B (sv) | 1976-01-29 | 1976-01-29 | Tisk pressning av en av kiselnitridpulver forformad kropp sett att framstella ett foremal av kiselnitrid genom isosta |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1091907A true CA1091907A (en) | 1980-12-23 |
Family
ID=20326840
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA270,575A Expired CA1091907A (en) | 1976-01-29 | 1977-01-27 | Method of manufacturing an object of silicon nitride |
Country Status (10)
| Country | Link |
|---|---|
| JP (1) | JPS5935870B2 (cs) |
| AU (1) | AU507155B2 (cs) |
| CA (1) | CA1091907A (cs) |
| DE (1) | DE2702073C2 (cs) |
| FR (1) | FR2339582A1 (cs) |
| GB (1) | GB1564851A (cs) |
| IT (1) | IT1192228B (cs) |
| SE (1) | SE396371B (cs) |
| SU (1) | SU651687A3 (cs) |
| ZA (1) | ZA77476B (cs) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2737266C2 (de) * | 1977-08-18 | 1987-08-20 | MTU Motoren- und Turbinen-Union München GmbH, 8000 München | Verfahren zur Kapselung eines Formkörpers aus Siliziumkeramik für das heißisostatische Pressen |
| DE2737208C2 (de) * | 1977-08-18 | 1986-06-19 | MTU Motoren- und Turbinen-Union München GmbH, 8000 München | Verfahren zur Kapselung eines Formkörpers aus Keramik |
| SE414922B (sv) * | 1978-05-02 | 1980-08-25 | Asea Ab | Sett att framstella ett foremal av kiselnitrid genom isostatisk pressning av en av kiselnitridpulver forformad kropp med ett gasformigt tryckmedium |
| SE414920C (sv) * | 1978-05-02 | 1982-03-15 | Asea Ab | Sett att framstella ett foremal av ett material i form av ett pulver genom isostatisk pressning av en av pulvret forformad kropp |
| SE413400B (sv) * | 1978-08-29 | 1980-05-27 | Asea Ab | Sett att framstella ett foremal av kiselnitrid genom isostatisk pressning av en av kiselnitridpulver forformad kropp med ett gasformigt tryckmedium i ett tryckkerl vid en for sintring av kiselnitriden erforderlig ... |
| SE425360B (sv) * | 1979-05-07 | 1982-09-27 | Asea Ab | Sett vid isostatisk pressning av pulver for framstellning av foremal av keramiskt eller metalliskt material |
| DE3009240A1 (de) * | 1980-03-11 | 1981-10-15 | Elektroschmelzwerk Kempten GmbH, 8000 München | Verfahren zur herstellung von praktisch porenfreien polykristallinen formkoerpern durch isostatisches heisspressen |
| SE430481B (sv) * | 1982-03-29 | 1983-11-21 | Asea Ab | Sett att sammanfoga delar av solitt material genom varm isostatisk pressning |
| JPS59198690A (ja) * | 1983-04-25 | 1984-11-10 | いすゞ自動車株式会社 | セラミツクヒ−タ−及びその製造方法 |
| SE456651B (sv) * | 1987-03-02 | 1988-10-24 | Asea Cerama Ab | Saett att framstaella ett foeremaal av i en kapsel inneslutet pulverformigt material genom isostatisk pressning |
| JPH02279575A (ja) * | 1989-04-18 | 1990-11-15 | Nkk Corp | 緻密なセラミック膜を有するセラミック焼結体の製造方法 |
| SE464620B (sv) * | 1989-09-26 | 1991-05-27 | Asea Cerama Ab | Saett att framstaella ett foeremaal av keramik genom isostatisk pressning i en glasomslutning |
| CN112341207B (zh) * | 2020-11-20 | 2022-08-12 | 哈尔滨工业大学 | 一种氮化硅-氧氮化硅柱孔复相陶瓷材料及其制备方法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1533020A1 (de) * | 1966-02-25 | 1970-03-05 | Philips Patentverwaltung | Verfahren und Ofen zum isostatischen Heisspressen von Presslingen |
| SE348961C (sv) * | 1971-03-15 | 1982-08-30 | Asea Ab | Forfarande for framstellning av en sintrad pulverkropp |
| DE2349277A1 (de) * | 1973-10-01 | 1975-04-24 | Feldmuehle Anlagen Prod | Verfahren zur herstellung dichter formkoerper aus siliziumnitrid |
| GB1522705A (en) * | 1974-11-11 | 1978-08-23 | Asea Ab | Method of manufacturing bodies of silicon nitride |
-
1976
- 1976-01-24 AU AU21574/77A patent/AU507155B2/en not_active Expired
- 1976-01-29 SE SE7600919A patent/SE396371B/xx not_active IP Right Cessation
-
1977
- 1977-01-19 DE DE2702073A patent/DE2702073C2/de not_active Expired
- 1977-01-26 SU SU772444414A patent/SU651687A3/ru active
- 1977-01-26 FR FR7702106A patent/FR2339582A1/fr active Granted
- 1977-01-27 ZA ZA770476A patent/ZA77476B/xx unknown
- 1977-01-27 CA CA270,575A patent/CA1091907A/en not_active Expired
- 1977-01-27 JP JP52008198A patent/JPS5935870B2/ja not_active Expired
- 1977-01-28 GB GB3490/77A patent/GB1564851A/en not_active Expired
- 1977-01-28 IT IT67184/77A patent/IT1192228B/it active
Also Published As
| Publication number | Publication date |
|---|---|
| DE2702073A1 (de) | 1977-08-04 |
| FR2339582A1 (fr) | 1977-08-26 |
| AU2157477A (en) | 1978-08-03 |
| ZA77476B (en) | 1977-12-28 |
| GB1564851A (en) | 1980-04-16 |
| FR2339582B1 (cs) | 1980-04-25 |
| DE2702073C2 (de) | 1983-12-08 |
| JPS5935870B2 (ja) | 1984-08-31 |
| IT1192228B (it) | 1988-03-31 |
| SE7600919L (sv) | 1977-07-30 |
| AU507155B2 (en) | 1980-02-07 |
| JPS5293699A (en) | 1977-08-06 |
| SU651687A3 (ru) | 1979-03-05 |
| SE396371B (sv) | 1977-09-19 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEX | Expiry |