BRPI0904998A2

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Info

Publication number: BRPI0904998A2
Authority: BR; Brazil
Prior art keywords: poly; adipate; alkaline; succinate; sebacate
Prior art date: 2008-12-01

Application number

BRPI0904998-3A

Other languages

English (en)

Portuguese (pt)

Inventor

Maria N V Mcdougall

Ke Zhou

Edward G Zwartz

Daryl W Vanbesien

John Pawlak

Paul J Gerroir

Suxia Yang

Richard P N Veregin

Karen A Moffat

Original Assignee

Xerox Corp

Priority date

2008-12-01

Filing date

2009-12-01

Publication date

2010-11-03

2009-12-01 Application filed by Xerox Corp filed Critical Xerox Corp

2010-11-03 Publication of BRPI0904998A2 publication Critical patent/BRPI0904998A2/pt

Links

239000000203 mixture Substances 0.000 title abstract description 79
239000002245 particle Substances 0.000 claims abstract description 127
229920000728 polyester Polymers 0.000 claims abstract description 65
229920005989 resin Polymers 0.000 claims description 163
239000011347 resin Substances 0.000 claims description 163
-1 octylene adipate Chemical compound 0.000 claims description 108
IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 claims description 75
238000000034 method Methods 0.000 claims description 43
229920001225 polyester resin Polymers 0.000 claims description 39
239000004645 polyester resin Substances 0.000 claims description 39
239000001993 wax Substances 0.000 claims description 34
229930185605 Bisphenol Natural products 0.000 claims description 31
239000000839 emulsion Substances 0.000 claims description 30
230000008569 process Effects 0.000 claims description 26
WNLRTRBMVRJNCN-UHFFFAOYSA-L adipate(2-) Chemical compound [O-]C(=O)CCCCC([O-])=O WNLRTRBMVRJNCN-UHFFFAOYSA-L 0.000 claims description 25
238000004220 aggregation Methods 0.000 claims description 21
230000002776 aggregation Effects 0.000 claims description 19
229920006038 crystalline resin Polymers 0.000 claims description 18
238000004581 coalescence Methods 0.000 claims description 16
239000003513 alkali Substances 0.000 claims description 15
VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 claims description 14
AXKZIDYFAMKWSA-UHFFFAOYSA-N 1,6-dioxacyclododecane-7,12-dione Chemical compound O=C1CCCCC(=O)OCCCCO1 AXKZIDYFAMKWSA-UHFFFAOYSA-N 0.000 claims description 12
VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims description 12
239000005977 Ethylene Substances 0.000 claims description 12
QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 claims description 12
PAALZGOZEUHCET-UHFFFAOYSA-N 1,4-dioxecane-5,10-dione Chemical compound O=C1CCCCC(=O)OCCO1 PAALZGOZEUHCET-UHFFFAOYSA-N 0.000 claims description 10
238000000576 coating method Methods 0.000 claims description 10
125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 claims description 10
239000004094 surface-active agent Substances 0.000 claims description 10
NYUNHMRXBVASOA-UHFFFAOYSA-N 1,7-dioxacyclotridecane-8,13-dione Chemical compound O=C1CCCCC(=O)OCCCCCO1 NYUNHMRXBVASOA-UHFFFAOYSA-N 0.000 claims description 9
ZLUFYQVHJAVDHU-IHWYPQMZSA-N (6z)-2-methyl-2,3-dihydro-1,4-dioxocine-5,8-dione Chemical compound CC1COC(=O)\C=C/C(=O)O1 ZLUFYQVHJAVDHU-IHWYPQMZSA-N 0.000 claims description 8
GJJSUPSPZIZYPM-UHFFFAOYSA-N 1,4-dioxacyclohexadecane-5,16-dione Chemical compound O=C1CCCCCCCCCCC(=O)OCCO1 GJJSUPSPZIZYPM-UHFFFAOYSA-N 0.000 claims description 8
AFGNPFWWBHDPEN-UHFFFAOYSA-N 1,6-dioxacyclododecane-2,5-dione Chemical compound O=C1CCC(=O)OCCCCCCO1 AFGNPFWWBHDPEN-UHFFFAOYSA-N 0.000 claims description 8
AMCTYGGTIWUNMF-UHFFFAOYSA-N 1,6-dioxacyclohexadecane-7,16-dione Chemical compound O=C1CCCCCCCCC(=O)OCCCCO1 AMCTYGGTIWUNMF-UHFFFAOYSA-N 0.000 claims description 8
LJEUDWSEILCUFG-UHFFFAOYSA-N 1,7-dioxacycloheptadecane-8,17-dione Chemical compound O=C1CCCCCCCCC(=O)OCCCCCO1 LJEUDWSEILCUFG-UHFFFAOYSA-N 0.000 claims description 8
SXWPIGKEISLSNQ-UHFFFAOYSA-N 1,8-dioxacyclooctadecane-9,18-dione Chemical compound O=C1CCCCCCCCC(=O)OCCCCCCO1 SXWPIGKEISLSNQ-UHFFFAOYSA-N 0.000 claims description 8
JOZILNCSRASEMU-UHFFFAOYSA-N 2-methyl-1,4-dioxacyclotetradecane-5,14-dione Chemical compound CC1COC(=O)CCCCCCCCC(=O)O1 JOZILNCSRASEMU-UHFFFAOYSA-N 0.000 claims description 8
VGHCVSPDKSEROA-UHFFFAOYSA-N 2-methyl-1,4-dioxecane-5,10-dione Chemical compound CC1COC(=O)CCCCC(=O)O1 VGHCVSPDKSEROA-UHFFFAOYSA-N 0.000 claims description 8
239000011248 coating agent Substances 0.000 claims description 8
239000003086 colorant Substances 0.000 claims description 8
229920001577 copolymer Polymers 0.000 claims description 8
229940116351 sebacate Drugs 0.000 claims description 8
XFQHIELVPOKJIM-UHFFFAOYSA-N 1,4-dioxacyclotetradecane-5,14-dione Chemical compound O=C1CCCCCCCCC(=O)OCCO1 XFQHIELVPOKJIM-UHFFFAOYSA-N 0.000 claims description 7
ZWXGXPQZTIWOEK-UHFFFAOYSA-N 1,6-dioxacycloundecane-2,5-dione Chemical compound O=C1CCC(=O)OCCCCCO1 ZWXGXPQZTIWOEK-UHFFFAOYSA-N 0.000 claims description 7
KYRZZPALUVQDRB-UHFFFAOYSA-N 2-methyl-1,4-dioxocane-5,8-dione Chemical compound CC1COC(=O)CCC(=O)O1 KYRZZPALUVQDRB-UHFFFAOYSA-N 0.000 claims description 7
DJIHQRBJGCGSIR-UHFFFAOYSA-N 2-methylidene-1,3-dioxepane-4,7-dione Chemical compound C1(CCC(=O)OC(=C)O1)=O DJIHQRBJGCGSIR-UHFFFAOYSA-N 0.000 claims description 7
229910052751 metal Inorganic materials 0.000 claims description 7
239000002184 metal Substances 0.000 claims description 7
ZMKVBUOZONDYBW-UHFFFAOYSA-N 1,6-dioxecane-2,5-dione Chemical compound O=C1CCC(=O)OCCCCO1 ZMKVBUOZONDYBW-UHFFFAOYSA-N 0.000 claims description 6
FMJOVSFCQGLPEU-UHFFFAOYSA-N 1,7-dioxacyclononadecane-8,19-dione Chemical compound C1(CCCCCCCCCCC(=O)OCCCCCO1)=O FMJOVSFCQGLPEU-UHFFFAOYSA-N 0.000 claims description 6
RNQBCZCPNUHWLV-UHFFFAOYSA-N 1,8-dioxacyclotetradecane-2,7-dione Chemical compound O=C1CCCCC(=O)OCCCCCCO1 RNQBCZCPNUHWLV-UHFFFAOYSA-N 0.000 claims description 6
WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims description 6
HDQCSTSCUIZZMY-UHFFFAOYSA-N O=C1CCCCCCCCCCC(=O)OCCCCCCCCCCCCO1 Chemical compound O=C1CCCCCCCCCCC(=O)OCCCCCCCCCCCCO1 HDQCSTSCUIZZMY-UHFFFAOYSA-N 0.000 claims description 6
KDYFGRWQOYBRFD-UHFFFAOYSA-L succinate(2-) Chemical compound [O-]C(=O)CCC([O-])=O KDYFGRWQOYBRFD-UHFFFAOYSA-L 0.000 claims description 6
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 5
ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 5
229910052744 lithium Inorganic materials 0.000 claims description 5
239000000178 monomer Substances 0.000 claims description 5
229910052700 potassium Inorganic materials 0.000 claims description 5
239000011591 potassium Substances 0.000 claims description 5
239000011734 sodium Substances 0.000 claims description 5
CGTQWXFRVNBMHK-OWOJBTEDSA-N (6e)-2,3-dihydro-1,4-dioxocine-5,8-dione Chemical compound O=C/1OCCOC(=O)\C=C\1 CGTQWXFRVNBMHK-OWOJBTEDSA-N 0.000 claims description 4
ZLUFYQVHJAVDHU-NSCUHMNNSA-N (6e)-2-methyl-2,3-dihydro-1,4-dioxocine-5,8-dione Chemical compound CC1COC(=O)\C=C\C(=O)O1 ZLUFYQVHJAVDHU-NSCUHMNNSA-N 0.000 claims description 4
PAMGQOCXAUZSIM-ONEGZZNKSA-N (8e)-2,3,4,5-tetrahydro-1,6-dioxecine-7,10-dione Chemical compound O=C/1OCCCCOC(=O)\C=C\1 PAMGQOCXAUZSIM-ONEGZZNKSA-N 0.000 claims description 4
UBHPFQGYQOBUFF-UHFFFAOYSA-N 1,11-dioxacyclohenicosane-12,21-dione Chemical compound C1(CCCCCCCCC(=O)OCCCCCCCCCO1)=O UBHPFQGYQOBUFF-UHFFFAOYSA-N 0.000 claims description 4
CSODJSBVFSGYDM-UHFFFAOYSA-N 1,12-dioxacyclodocosane-2,11-dione Chemical compound O=C1CCCCCCCCC(=O)OCCCCCCCCCCO1 CSODJSBVFSGYDM-UHFFFAOYSA-N 0.000 claims description 4
KGBZIXNVGIOBBV-UHFFFAOYSA-N 1,12-dioxacyclotetracosane-13,24-dione Chemical compound O=C1CCCCCCCCCCC(=O)OCCCCCCCCCCO1 KGBZIXNVGIOBBV-UHFFFAOYSA-N 0.000 claims description 4
CPWOEKUTRFZDFA-UHFFFAOYSA-N 1,12-dioxacyclotetracosane-2,11-dione Chemical compound O=C1CCCCCCCCC(=O)OCCCCCCCCCCCCO1 CPWOEKUTRFZDFA-UHFFFAOYSA-N 0.000 claims description 4
OREVWQRRKZACKB-UHFFFAOYSA-N 1,12-dioxacyclotricosane-2,11-dione Chemical compound O=C1CCCCCCCCC(=O)OCCCCCCCCCCCO1 OREVWQRRKZACKB-UHFFFAOYSA-N 0.000 claims description 4
QWUVDMOLNYRJTI-UHFFFAOYSA-N 1,6-dioxacyclohexadecane-2,5-dione Chemical compound O=C1CCC(=O)OCCCCCCCCCCO1 QWUVDMOLNYRJTI-UHFFFAOYSA-N 0.000 claims description 4
PJMKWDFEIQYPSE-UHFFFAOYSA-N 1,6-dioxacyclooctadecane-2,5-dione Chemical compound O=C1CCC(=O)OCCCCCCCCCCCCO1 PJMKWDFEIQYPSE-UHFFFAOYSA-N 0.000 claims description 4
WDCPTDRLVGJRDK-UHFFFAOYSA-N 1,6-dioxacyclooctadecane-7,18-dione Chemical compound O=C1CCCCCCCCCCC(=O)OCCCCO1 WDCPTDRLVGJRDK-UHFFFAOYSA-N 0.000 claims description 4
BDORCUNAKFCZFY-UHFFFAOYSA-N 1,6-dioxacyclopentadecane-2,5-dione Chemical compound C1(CCC(=O)OCCCCCCCCCO1)=O BDORCUNAKFCZFY-UHFFFAOYSA-N 0.000 claims description 4
ZISGFPVFMHXZLO-UHFFFAOYSA-N 1,8-dioxacycloheptadecane-2,7-dione Chemical compound O=C1CCCCC(=O)OCCCCCCCCCO1 ZISGFPVFMHXZLO-UHFFFAOYSA-N 0.000 claims description 4
DQORZVDGEBZWMI-UHFFFAOYSA-N 1,8-dioxacycloicosane-2,7-dione Chemical compound O=C1CCCCC(=O)OCCCCCCCCCCCCO1 DQORZVDGEBZWMI-UHFFFAOYSA-N 0.000 claims description 4
VPNRJIKJACGVJW-UHFFFAOYSA-N 1,8-dioxacycloicosane-9,20-dione Chemical compound O=C1CCCCCCCCCCC(=O)OCCCCCCO1 VPNRJIKJACGVJW-UHFFFAOYSA-N 0.000 claims description 4
NUOQMJUJPAHTBJ-UHFFFAOYSA-N 1,8-dioxacyclononadecane-2,7-dione Chemical compound C1(CCCCC(=O)OCCCCCCCCCCCO1)=O NUOQMJUJPAHTBJ-UHFFFAOYSA-N 0.000 claims description 4
KFNVCNYZNJSFJG-UHFFFAOYSA-N 1,8-dioxacyclooctadecane-2,7-dione Chemical compound O=C1CCCCC(=O)OCCCCCCCCCCO1 KFNVCNYZNJSFJG-UHFFFAOYSA-N 0.000 claims description 4
RCOKMWAKYZDWAA-UHFFFAOYSA-N 2-methyl-1,4-dioxacyclohexadecane-5,16-dione Chemical compound CC1COC(=O)CCCCCCCCCCC(=O)O1 RCOKMWAKYZDWAA-UHFFFAOYSA-N 0.000 claims description 4
JCSSBRMVXRPRDX-UHFFFAOYSA-N 2-methyl-6-methylidene-1,4-dioxocane-5,8-dione Chemical compound CC1COC(=O)C(=C)CC(=O)O1 JCSSBRMVXRPRDX-UHFFFAOYSA-N 0.000 claims description 4
CUZFTCIAWWXKLK-UHFFFAOYSA-N C1(C=CC(=O)OCCCCCCCCCO1)=O Chemical compound C1(C=CC(=O)OCCCCCCCCCO1)=O CUZFTCIAWWXKLK-UHFFFAOYSA-N 0.000 claims description 4
WYMXCAJPPSDBEC-UHFFFAOYSA-N C1(C=CC(=O)OCCCCCO1)=O Chemical compound C1(C=CC(=O)OCCCCCO1)=O WYMXCAJPPSDBEC-UHFFFAOYSA-N 0.000 claims description 4
ISWCYPUKRLCRSG-MDZDMXLPSA-N O=C/1OCCCCCCCCCCOC(=O)\C=C\1 Chemical compound O=C/1OCCCCCCCCCCOC(=O)\C=C\1 ISWCYPUKRLCRSG-MDZDMXLPSA-N 0.000 claims description 4
229910052708 sodium Inorganic materials 0.000 claims description 4
GUNLFCZMCDYCMU-AATRIKPKSA-N (3e)-1,6-dioxacyclododec-3-ene-2,5-dione Chemical compound O=C/1OCCCCCCOC(=O)\C=C\1 GUNLFCZMCDYCMU-AATRIKPKSA-N 0.000 claims description 3
OWLXKQZPEUPNCR-UHFFFAOYSA-N 1,11-dioxacyclotricosane-12,23-dione Chemical compound C1(CCCCCCCCCCC(=O)OCCCCCCCCCO1)=O OWLXKQZPEUPNCR-UHFFFAOYSA-N 0.000 claims description 3
UZOSFBHTEPXZLG-UHFFFAOYSA-N 1,13-dioxacyclopentacosane-14,25-dione Chemical compound C1(CCCCCCCCCCC(=O)OCCCCCCCCCCCO1)=O UZOSFBHTEPXZLG-UHFFFAOYSA-N 0.000 claims description 3
125000004836 hexamethylene group Chemical group [H]C([H])([*:2])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[*:1] 0.000 claims description 3
239000000155 melt Substances 0.000 claims description 3
125000004817 pentamethylene group Chemical group [H]C([H])([*:2])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[*:1] 0.000 claims description 3
239000007787 solid Substances 0.000 claims description 3
125000000217 alkyl group Chemical group 0.000 claims description 2
239000004615 ingredient Substances 0.000 claims description 2
238000011084 recovery Methods 0.000 claims description 2
125000000383 tetramethylene group Chemical group [H]C([H])([*:1])C([H])([H])C([H])([H])C([H])([H])[*:2] 0.000 claims 4
IWXITRXCELDPJQ-UHFFFAOYSA-N 1,6-dioxacycloheptadecane-2,5-dione Chemical compound C1(CCC(=O)OCCCCCCCCCCCO1)=O IWXITRXCELDPJQ-UHFFFAOYSA-N 0.000 claims 3
WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims 3
KWKAKUADMBZCLK-UHFFFAOYSA-N 1-octene Chemical group CCCCCCC=C KWKAKUADMBZCLK-UHFFFAOYSA-N 0.000 claims 2
RNERBJNDXXEXTK-VOTSOKGWSA-N (e)-4-hexoxy-4-oxobut-2-enoic acid Chemical compound CCCCCCOC(=O)\C=C\C(O)=O RNERBJNDXXEXTK-VOTSOKGWSA-N 0.000 claims 1
JRZJOMJEPLMPRA-UHFFFAOYSA-N 1-nonene Chemical group CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 claims 1
ASERZHTZQPEFDE-UHFFFAOYSA-N 2-[2-(2-hydroxyphenyl)propyl]phenol Chemical compound C=1C=CC=C(O)C=1C(C)CC1=CC=CC=C1O ASERZHTZQPEFDE-UHFFFAOYSA-N 0.000 claims 1
SKBCSCHPOLWLCN-UHFFFAOYSA-N 2-sulfohexanedioic acid Chemical compound OC(=O)CCCC(C(O)=O)S(O)(=O)=O SKBCSCHPOLWLCN-UHFFFAOYSA-N 0.000 claims 1
241001136782 Alca Species 0.000 claims 1
241000272525 Anas platyrhynchos Species 0.000 claims 1
239000000654 additive Substances 0.000 abstract description 24
230000000052 comparative effect Effects 0.000 description 21
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 18
239000000049 pigment Substances 0.000 description 16
239000002253 acid Substances 0.000 description 15
230000015572 biosynthetic process Effects 0.000 description 15
VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 14
230000000903 blocking effect Effects 0.000 description 13
239000000975 dye Substances 0.000 description 13
238000011068 loading method Methods 0.000 description 13
229920006127 amorphous resin Polymers 0.000 description 12
239000004816 latex Substances 0.000 description 12
229920000126 latex Polymers 0.000 description 12
229910044991 metal oxide Inorganic materials 0.000 description 12
150000004706 metal oxides Chemical class 0.000 description 12
238000002156 mixing Methods 0.000 description 12
XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Natural products CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 11
230000000996 additive effect Effects 0.000 description 11
239000003795 chemical substances by application Substances 0.000 description 11
239000000499 gel Substances 0.000 description 11
229920000642 polymer Polymers 0.000 description 11
239000000126 substance Substances 0.000 description 11
PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 10
KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 10
238000007792 addition Methods 0.000 description 10
239000011541 reaction mixture Substances 0.000 description 10
PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 9
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
150000002148 esters Chemical class 0.000 description 9
229910052799 carbon Inorganic materials 0.000 description 8
DNIAPMSPPWPWGF-UHFFFAOYSA-N monopropylene glycol Natural products CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 8
229920005862 polyol Polymers 0.000 description 8
150000003077 polyols Chemical class 0.000 description 8
239000002243 precursor Substances 0.000 description 8
238000002360 preparation method Methods 0.000 description 8
PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 7
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 7
239000004698 Polyethylene Substances 0.000 description 7
150000007513 acids Chemical class 0.000 description 7
230000004931 aggregating effect Effects 0.000 description 7
125000004432 carbon atom Chemical group C* 0.000 description 7
238000011161 development Methods 0.000 description 7
230000018109 developmental process Effects 0.000 description 7
150000005690 diesters Chemical class 0.000 description 7
239000011521 glass Substances 0.000 description 7
238000000265 homogenisation Methods 0.000 description 7
239000000377 silicon dioxide Substances 0.000 description 7
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
125000001931 aliphatic group Chemical group 0.000 description 6
WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical compound OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 description 6
239000007771 core particle Substances 0.000 description 6
235000014113 dietary fatty acids Nutrition 0.000 description 6
150000002009 diols Chemical class 0.000 description 6
239000000194 fatty acid Substances 0.000 description 6
229930195729 fatty acid Natural products 0.000 description 6
238000005227 gel permeation chromatography Methods 0.000 description 6
230000009477 glass transition Effects 0.000 description 6
239000000463 material Substances 0.000 description 6
ARCGXLSVLAOJQL-UHFFFAOYSA-N trimellitic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C(C(O)=O)=C1 ARCGXLSVLAOJQL-UHFFFAOYSA-N 0.000 description 6
OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 5
GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 5
150000007933 aliphatic carboxylic acids Chemical class 0.000 description 5
238000009826 distribution Methods 0.000 description 5
239000001530 fumaric acid Substances 0.000 description 5
230000004927 fusion Effects 0.000 description 5
229920003229 poly(methyl methacrylate) Polymers 0.000 description 5
229920000573 polyethylene Polymers 0.000 description 5
239000004926 polymethyl methacrylate Substances 0.000 description 5
238000012360 testing method Methods 0.000 description 5
239000004743 Polypropylene Substances 0.000 description 4
239000004793 Polystyrene Substances 0.000 description 4
WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 4
239000003945 anionic surfactant Substances 0.000 description 4
239000007864 aqueous solution Substances 0.000 description 4
125000004429 atom Chemical group 0.000 description 4
239000002585 base Substances 0.000 description 4
239000006085 branching agent Substances 0.000 description 4
XCJYREBRNVKWGJ-UHFFFAOYSA-N copper(II) phthalocyanine Chemical compound [Cu+2].C12=CC=CC=C2C(N=C2[N-]C(C3=CC=CC=C32)=N2)=NC1=NC([C]1C=CC=CC1=1)=NC=1N=C1[C]3C=CC=CC3=C2[N-]1 XCJYREBRNVKWGJ-UHFFFAOYSA-N 0.000 description 4
MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 4
WOZVHXUHUFLZGK-UHFFFAOYSA-N dimethyl terephthalate Chemical compound COC(=O)C1=CC=C(C(=O)OC)C=C1 WOZVHXUHUFLZGK-UHFFFAOYSA-N 0.000 description 4
239000006185 dispersion Substances 0.000 description 4
TVIDDXQYHWJXFK-UHFFFAOYSA-N dodecanedioic acid Chemical compound OC(=O)CCCCCCCCCCC(O)=O TVIDDXQYHWJXFK-UHFFFAOYSA-N 0.000 description 4
238000004108 freeze drying Methods 0.000 description 4
QQVIHTHCMHWDBS-UHFFFAOYSA-N isophthalic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=C1 QQVIHTHCMHWDBS-UHFFFAOYSA-N 0.000 description 4
BDJRBEYXGGNYIS-UHFFFAOYSA-N nonanedioic acid Chemical compound OC(=O)CCCCCCCC(O)=O BDJRBEYXGGNYIS-UHFFFAOYSA-N 0.000 description 4
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