BR112020006425B1 - Processo para purificar uma mistura - Google Patents

Processo para purificar uma mistura Download PDF

Info

Publication number
BR112020006425B1
BR112020006425B1 BR112020006425-4A BR112020006425A BR112020006425B1 BR 112020006425 B1 BR112020006425 B1 BR 112020006425B1 BR 112020006425 A BR112020006425 A BR 112020006425A BR 112020006425 B1 BR112020006425 B1 BR 112020006425B1
Authority
BR
Brazil
Prior art keywords
mixture
stage
meg
column
deta
Prior art date
Application number
BR112020006425-4A
Other languages
English (en)
Portuguese (pt)
Other versions
BR112020006425A2 (pt
Inventor
Hermann Luyken
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of BR112020006425A2 publication Critical patent/BR112020006425A2/pt
Publication of BR112020006425B1 publication Critical patent/BR112020006425B1/pt

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/82Purification; Separation; Stabilisation; Use of additives
    • C07C209/86Separation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/82Purification; Separation; Stabilisation; Use of additives
    • C07C209/84Purification
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/04Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups
    • C07C209/14Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups
    • C07C209/16Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups with formation of amino groups bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/02Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reactions involving the formation of amino groups from compounds containing hydroxy groups or etherified or esterified hydroxy groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/10Separation; Purification; Stabilisation; Use of additives

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
BR112020006425-4A 2017-10-27 2018-10-17 Processo para purificar uma mistura BR112020006425B1 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP17198943 2017-10-27
EP17198943.7 2017-10-27
PCT/EP2018/078320 WO2019081283A1 (de) 2017-10-27 2018-10-17 Verfahren zur herstellung von ethylenaminen

Publications (2)

Publication Number Publication Date
BR112020006425A2 BR112020006425A2 (pt) 2020-09-24
BR112020006425B1 true BR112020006425B1 (pt) 2023-03-21

Family

ID=60190743

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112020006425-4A BR112020006425B1 (pt) 2017-10-27 2018-10-17 Processo para purificar uma mistura

Country Status (6)

Country Link
US (1) US11339117B2 (https=)
EP (1) EP3700883B1 (https=)
JP (1) JP7268017B2 (https=)
CN (1) CN111263746B (https=)
BR (1) BR112020006425B1 (https=)
WO (1) WO2019081283A1 (https=)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP7277455B2 (ja) * 2017-10-27 2023-05-19 ビーエーエスエフ ソシエタス・ヨーロピア Eda含有混合物からのn-メチルエチレンジアミンの分離除去
CN111018719B (zh) * 2019-12-19 2023-03-21 西安近代化学研究所 一种提纯乙二胺的方法
CN111747856B (zh) * 2020-07-17 2022-12-13 新中天环保股份有限公司 一种废溶剂的处理方法
CN119451938A (zh) 2022-06-29 2025-02-14 巴斯夫欧洲公司 用于制造亚乙基胺的方法
WO2024002740A1 (en) 2022-06-29 2024-01-04 Basf Se Method for manufacture of ethyleneamines
CN115057784B (zh) * 2022-07-13 2024-04-05 山东胜邦绿野化学有限公司 一种辛菌胺废水处理方法
CN116375665B (zh) * 2023-04-07 2025-02-25 福建钰融科技有限公司 一种含羟乙基哌嗪与羟乙基乙二胺的混合废液精制回收工艺
KR20260039702A (ko) * 2023-07-17 2026-03-20 바스프 에스이 새로운 냉각제 조성물
WO2025125094A1 (en) 2023-12-14 2025-06-19 Basf Se Process for preparing diethylenetriamine and/or ethylene glycol

Family Cites Families (32)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2519803A (en) 1946-02-05 1950-08-22 Du Pont Preparation of ethylene diamines
US2861995A (en) 1956-04-27 1958-11-25 Dow Chemical Co Process for the conversion of ethanolamine
US3112318A (en) 1957-10-09 1963-11-26 Union Carbide Corp Method for producing piperazine
DE1154121B (de) 1959-08-03 1963-09-12 Rohm & Haas Verfahren zur Herstellung von AEthylendiamin
US3137730A (en) 1960-04-12 1964-06-16 Allied Chem Production of ethylenediamine
DE1172268B (de) 1962-02-21 1964-06-18 Basf Ag Verfahren zur Herstellung von Diaminen
US4123462A (en) 1976-01-07 1978-10-31 Union Carbide Corporation Amination process using nickel-rhenium catalysts
WO2000006756A1 (en) 1998-07-28 2000-02-10 E.I. Du Pont De Nemours And Company Sulfur metabolism enzymes
DE10349059A1 (de) 2003-10-17 2005-05-19 Basf Ag Verfahren zur destillativen Auftrennung von Gemischen enthaltend Ethylenamine
DE102005019373A1 (de) * 2005-04-26 2006-11-02 Basf Ag Verfahren zur Herstellung von Ethylenaminen
CN1723887A (zh) 2005-07-20 2006-01-25 重庆福瑞制药有限公司 一种紫杉醇注射剂及其制备方法
US7635790B2 (en) 2006-02-14 2009-12-22 Basf Se Method for producing ethylene amines and ethanol amines by the hydrogenating amination of monoethylene glycol and ammonia in the presence of a catalyst
WO2007093514A1 (de) 2006-02-14 2007-08-23 Basf Se Verfahren zur herstellung von ethylenaminen und ethanolaminen aus monoethylenglykol (meg)
MY144469A (en) 2006-02-14 2011-09-30 Basf Se Process for the distillative separation of mixtures comprising monoethylene glycol and diethylentriamine
US7919655B2 (en) 2006-07-14 2011-04-05 Basf Se Method for producing an amine
RU2009104740A (ru) 2006-07-14 2010-08-27 Басф Се (De) Способ получения амина
US8299249B2 (en) 2007-03-01 2012-10-30 Basf Se Method for producing TETA by means of EDDN
RU2478092C2 (ru) 2007-03-01 2013-03-27 Басф Се Способ получения смесей этиленаминов
EP2132165B1 (de) 2007-03-01 2014-04-23 Basf Se Verfahren zur herstellung von ethylendiamin
EP2166481A4 (en) 2007-07-09 2011-11-02 Fujitsu Ltd DEVICE, METHOD AND USER AUTHENTICATION PROGRAM
ATE553844T1 (de) 2007-12-21 2012-05-15 Basf Se Verfahren zur herstellung eines amins
WO2010042168A2 (en) * 2008-10-06 2010-04-15 Dow Global Technologies Inc. Methods for making ethanolamine(s) and ethyleneamine(s) from ethylene oxide and ammonia, and related methods
JP2012504610A (ja) 2008-10-06 2012-02-23 ユニオン カーバイド ケミカルズ アンド プラスティックス テクノロジー エルエルシー エチレンアミンの製造方法
WO2011067226A1 (de) 2009-12-02 2011-06-09 Basf Se Verfahren zur destillation von gemischen enthaltend ethylendiamin, n-methylethylendiamin und wasser und damit erhältliche gemische aus ethylendiamin und n-methylethylendiamin mit einem geringen n-methylethylendiamingehalt
CN102190588A (zh) 2010-03-16 2011-09-21 张家港惠尔化学科技有限公司 乙二醇与氨制乙二胺的方法
CN102233272A (zh) 2010-04-22 2011-11-09 张家港惠尔化学科技有限公司 乙二醇氨化制乙二胺的催化剂及其制备方法
SG11201401354QA (en) 2011-11-17 2014-08-28 Basf Se Process for producing sn-containing catalysts
WO2015135971A1 (de) 2014-03-13 2015-09-17 Basf Se Verfahren zur destillativen reinigung von eda
CN105585502B (zh) * 2014-10-24 2018-09-14 中国石油化工股份有限公司 催化氨化法生产乙二胺的方法
CN106607060B (zh) 2015-10-26 2019-08-20 中国石油化工股份有限公司 催化剂及其制备方法和应用以及乙二醇临氢胺化制乙二胺的方法
EP3634935B1 (de) 2017-06-09 2022-03-09 Basf Se Verfahren zur herstellung von ethylenaminen
US11214535B2 (en) 2017-06-09 2022-01-04 Basf Se Method for producing ethyleneamines

Also Published As

Publication number Publication date
JP7268017B2 (ja) 2023-05-02
US20200308097A1 (en) 2020-10-01
CN111263746B (zh) 2024-01-19
EP3700883B1 (de) 2022-04-20
BR112020006425A2 (pt) 2020-09-24
US11339117B2 (en) 2022-05-24
WO2019081283A1 (de) 2019-05-02
JP2021500389A (ja) 2021-01-07
CN111263746A (zh) 2020-06-09
EP3700883A1 (de) 2020-09-02

Similar Documents

Publication Publication Date Title
BR112020006425B1 (pt) Processo para purificar uma mistura
US11021434B2 (en) Method for producing ethyleneamines
EP2346810B1 (en) Methods for making ethanolamine(s) and ethyleneamine(s) from ethylene oxide and ammonia, and related methods
JP6169151B2 (ja) エチレンジアミン、n−メチルエチレンジアミンおよび水を含有する混合物を蒸留する方法、およびそれによって得られた、僅かなn−メチルエチレンジアミン含量を有する、エチレンジアミンとn−メチルエチレンジアミンとの混合物
KR101648653B1 (ko) 아세토니트릴의 정제 방법
JP6377183B2 (ja) Edaを蒸留精製するための方法
RU2717556C1 (ru) Объединенный способ получения пропена и пропеноксида из пропана
WO2014072803A1 (en) Synthesis of methyl carbamate and dimethyl carbonate (dmc) in presence of stripping with inert gas or superheated vapours and a reactor for the same
TW201546026A (zh) 觸媒製備及氫化方法
BR112020006431B1 (pt) Processo para remover nmeda de uma mistura
EP4073026B1 (en) Separation of n-methylethylenediamine from eda-containing mixtures
BR112020002390A2 (pt) processo de conversão da monoureia cíclica de compostos de etileno amina em composto de etileno amina
WO2006118070A1 (ja) 尿素合成装置
BR112020006442B1 (pt) Processo de purificação de etilenodiamina
CN107777705B (zh) 液氨原料的处理方法
CN105531254A (zh) 从二腈制造二胺的氢化方法
WO2026057498A1 (en) Method for separating and recovering ammonia from an amination product mixture
BR112023018085B1 (pt) Processo e instalação para recuperar isoprenol essencialmente livre de formaldeído de uma corrente de isoprenol bruto contendo isoprenol, água e formaldeído
CS235886B1 (cs) Způsob výroby morfolinu

Legal Events

Date Code Title Description
B350 Update of information on the portal [chapter 15.35 patent gazette]
B06W Patent application suspended after preliminary examination (for patents with searches from other patent authorities) chapter 6.23 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 17/10/2018, OBSERVADAS AS CONDICOES LEGAIS