JP7268017B2 - エチレンアミンの製造方法 - Google Patents

エチレンアミンの製造方法 Download PDF

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JP7268017B2
JP7268017B2 JP2020523439A JP2020523439A JP7268017B2 JP 7268017 B2 JP7268017 B2 JP 7268017B2 JP 2020523439 A JP2020523439 A JP 2020523439A JP 2020523439 A JP2020523439 A JP 2020523439A JP 7268017 B2 JP7268017 B2 JP 7268017B2
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mixture
meg
column
stage
ammonia
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JP2021500389A (ja
JP2021500389A5 (https=
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ルイケン ヘアマン
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/82—Purification; Separation; Stabilisation; Use of additives
    • C07C209/84—Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/82—Purification; Separation; Stabilisation; Use of additives
    • C07C209/86—Separation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/04—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups
    • C07C209/14—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups
    • C07C209/16—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups with formation of amino groups bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/02—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reactions involving the formation of amino groups from compounds containing hydroxy groups or etherified or esterified hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/10—Separation; Purification; Stabilisation; Use of additives

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
JP2020523439A 2017-10-27 2018-10-17 エチレンアミンの製造方法 Active JP7268017B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP17198943 2017-10-27
EP17198943.7 2017-10-27
PCT/EP2018/078320 WO2019081283A1 (de) 2017-10-27 2018-10-17 Verfahren zur herstellung von ethylenaminen

Publications (3)

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JP2021500389A JP2021500389A (ja) 2021-01-07
JP2021500389A5 JP2021500389A5 (https=) 2023-01-30
JP7268017B2 true JP7268017B2 (ja) 2023-05-02

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JP2020523439A Active JP7268017B2 (ja) 2017-10-27 2018-10-17 エチレンアミンの製造方法

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US (1) US11339117B2 (https=)
EP (1) EP3700883B1 (https=)
JP (1) JP7268017B2 (https=)
CN (1) CN111263746B (https=)
BR (1) BR112020006425B1 (https=)
WO (1) WO2019081283A1 (https=)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP7277455B2 (ja) * 2017-10-27 2023-05-19 ビーエーエスエフ ソシエタス・ヨーロピア Ｅｄａ含有混合物からのｎ－メチルエチレンジアミンの分離除去
CN111018719B (zh) * 2019-12-19 2023-03-21 西安近代化学研究所 一种提纯乙二胺的方法
CN111747856B (zh) * 2020-07-17 2022-12-13 新中天环保股份有限公司 一种废溶剂的处理方法
CN119451938A (zh) 2022-06-29 2025-02-14 巴斯夫欧洲公司 用于制造亚乙基胺的方法
WO2024002740A1 (en) 2022-06-29 2024-01-04 Basf Se Method for manufacture of ethyleneamines
CN115057784B (zh) * 2022-07-13 2024-04-05 山东胜邦绿野化学有限公司 一种辛菌胺废水处理方法
CN116375665B (zh) * 2023-04-07 2025-02-25 福建钰融科技有限公司 一种含羟乙基哌嗪与羟乙基乙二胺的混合废液精制回收工艺
KR20260039702A (ko) * 2023-07-17 2026-03-20 바스프 에스이 새로운 냉각제 조성물
WO2025125094A1 (en) 2023-12-14 2025-06-19 Basf Se Process for preparing diethylenetriamine and/or ethylene glycol

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2006114417A2 (de) 2005-04-26 2006-11-02 Basf Aktiengesellschaft Verfahren zur herstellung von ethylenaminen
JP2007533637A (ja) 2003-10-17 2007-11-22 ビーエーエスエフ　アクチェンゲゼルシャフト エチレンアミン類を含有している混合物の蒸留による分離方法
JP2009526811A (ja) 2006-02-14 2009-07-23 ビーエーエスエフ ソシエタス・ヨーロピア モノエチレングリコールとジエチレントリアミンとを含有する混合物の蒸留分離方法
JP2012504615A (ja) 2008-10-06 2012-02-23 ダウ グローバル テクノロジーズ エルエルシー エチレンオキサイド及びアンモニアからのエタノールアミン及びエチレンアミンの製造方法並びに関連方法
JP2013512874A (ja) 2009-12-02 2013-04-18 ビーエーエスエフ ソシエタス・ヨーロピア エチレンジアミン、ｎ−メチルエチレンジアミンおよび水を含有する混合物を蒸留する方法、およびそれによって得られた、僅かなｎ−メチルエチレンジアミン含量を有する、エチレンジアミンとｎ−メチルエチレンジアミンとの混合物
CN105585502A (zh) 2014-10-24 2016-05-18 中国石油化工股份有限公司 催化氨化法生产乙二胺的方法
JP2017513924A (ja) 2014-03-13 2017-06-01 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ Ｅｄａを蒸留精製するための方法

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US2519803A (en) 1946-02-05 1950-08-22 Du Pont Preparation of ethylene diamines
US2861995A (en) 1956-04-27 1958-11-25 Dow Chemical Co Process for the conversion of ethanolamine
US3112318A (en) 1957-10-09 1963-11-26 Union Carbide Corp Method for producing piperazine
DE1154121B (de) 1959-08-03 1963-09-12 Rohm & Haas Verfahren zur Herstellung von AEthylendiamin
US3137730A (en) 1960-04-12 1964-06-16 Allied Chem Production of ethylenediamine
DE1172268B (de) 1962-02-21 1964-06-18 Basf Ag Verfahren zur Herstellung von Diaminen
US4123462A (en) 1976-01-07 1978-10-31 Union Carbide Corporation Amination process using nickel-rhenium catalysts
WO2000006756A1 (en) 1998-07-28 2000-02-10 E.I. Du Pont De Nemours And Company Sulfur metabolism enzymes
CN1723887A (zh) 2005-07-20 2006-01-25 重庆福瑞制药有限公司 一种紫杉醇注射剂及其制备方法
US7635790B2 (en) 2006-02-14 2009-12-22 Basf Se Method for producing ethylene amines and ethanol amines by the hydrogenating amination of monoethylene glycol and ammonia in the presence of a catalyst
WO2007093514A1 (de) 2006-02-14 2007-08-23 Basf Se Verfahren zur herstellung von ethylenaminen und ethanolaminen aus monoethylenglykol (meg)
US7919655B2 (en) 2006-07-14 2011-04-05 Basf Se Method for producing an amine
RU2009104740A (ru) 2006-07-14 2010-08-27 Басф Се (De) Способ получения амина
US8299249B2 (en) 2007-03-01 2012-10-30 Basf Se Method for producing TETA by means of EDDN
RU2478092C2 (ru) 2007-03-01 2013-03-27 Басф Се Способ получения смесей этиленаминов
EP2132165B1 (de) 2007-03-01 2014-04-23 Basf Se Verfahren zur herstellung von ethylendiamin
EP2166481A4 (en) 2007-07-09 2011-11-02 Fujitsu Ltd DEVICE, METHOD AND USER AUTHENTICATION PROGRAM
ATE553844T1 (de) 2007-12-21 2012-05-15 Basf Se Verfahren zur herstellung eines amins
JP2012504610A (ja) 2008-10-06 2012-02-23 ユニオン カーバイド ケミカルズ アンド プラスティックス テクノロジー エルエルシー エチレンアミンの製造方法
CN102190588A (zh) 2010-03-16 2011-09-21 张家港惠尔化学科技有限公司 乙二醇与氨制乙二胺的方法
CN102233272A (zh) 2010-04-22 2011-11-09 张家港惠尔化学科技有限公司 乙二醇氨化制乙二胺的催化剂及其制备方法
SG11201401354QA (en) 2011-11-17 2014-08-28 Basf Se Process for producing sn-containing catalysts
CN106607060B (zh) 2015-10-26 2019-08-20 中国石油化工股份有限公司 催化剂及其制备方法和应用以及乙二醇临氢胺化制乙二胺的方法
EP3634935B1 (de) 2017-06-09 2022-03-09 Basf Se Verfahren zur herstellung von ethylenaminen
US11214535B2 (en) 2017-06-09 2022-01-04 Basf Se Method for producing ethyleneamines

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007533637A (ja) 2003-10-17 2007-11-22 ビーエーエスエフ　アクチェンゲゼルシャフト エチレンアミン類を含有している混合物の蒸留による分離方法
WO2006114417A2 (de) 2005-04-26 2006-11-02 Basf Aktiengesellschaft Verfahren zur herstellung von ethylenaminen
JP2009526811A (ja) 2006-02-14 2009-07-23 ビーエーエスエフ ソシエタス・ヨーロピア モノエチレングリコールとジエチレントリアミンとを含有する混合物の蒸留分離方法
JP2012504615A (ja) 2008-10-06 2012-02-23 ダウ グローバル テクノロジーズ エルエルシー エチレンオキサイド及びアンモニアからのエタノールアミン及びエチレンアミンの製造方法並びに関連方法
JP2013512874A (ja) 2009-12-02 2013-04-18 ビーエーエスエフ ソシエタス・ヨーロピア エチレンジアミン、ｎ−メチルエチレンジアミンおよび水を含有する混合物を蒸留する方法、およびそれによって得られた、僅かなｎ−メチルエチレンジアミン含量を有する、エチレンジアミンとｎ−メチルエチレンジアミンとの混合物
JP2017513924A (ja) 2014-03-13 2017-06-01 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ Ｅｄａを蒸留精製するための方法
CN105585502A (zh) 2014-10-24 2016-05-18 中国石油化工股份有限公司 催化氨化法生产乙二胺的方法

Also Published As

Publication number Publication date
US20200308097A1 (en) 2020-10-01
CN111263746B (zh) 2024-01-19
EP3700883B1 (de) 2022-04-20
BR112020006425A2 (pt) 2020-09-24
US11339117B2 (en) 2022-05-24
WO2019081283A1 (de) 2019-05-02
BR112020006425B1 (pt) 2023-03-21
JP2021500389A (ja) 2021-01-07
CN111263746A (zh) 2020-06-09
EP3700883A1 (de) 2020-09-02

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