CN111263746B - 制备亚乙基胺的方法 - Google Patents
制备亚乙基胺的方法 Download PDFInfo
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- CN111263746B CN111263746B CN201880069384.9A CN201880069384A CN111263746B CN 111263746 B CN111263746 B CN 111263746B CN 201880069384 A CN201880069384 A CN 201880069384A CN 111263746 B CN111263746 B CN 111263746B
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Classifications
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/82—Purification; Separation; Stabilisation; Use of additives
- C07C209/84—Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/82—Purification; Separation; Stabilisation; Use of additives
- C07C209/86—Separation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/04—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups
- C07C209/14—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups
- C07C209/16—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups with formation of amino groups bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/02—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reactions involving the formation of amino groups from compounds containing hydroxy groups or etherified or esterified hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/10—Separation; Purification; Stabilisation; Use of additives
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP17198943 | 2017-10-27 | ||
| EP17198943.7 | 2017-10-27 | ||
| PCT/EP2018/078320 WO2019081283A1 (de) | 2017-10-27 | 2018-10-17 | Verfahren zur herstellung von ethylenaminen |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN111263746A CN111263746A (zh) | 2020-06-09 |
| CN111263746B true CN111263746B (zh) | 2024-01-19 |
Family
ID=60190743
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201880069384.9A Active CN111263746B (zh) | 2017-10-27 | 2018-10-17 | 制备亚乙基胺的方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US11339117B2 (https=) |
| EP (1) | EP3700883B1 (https=) |
| JP (1) | JP7268017B2 (https=) |
| CN (1) | CN111263746B (https=) |
| BR (1) | BR112020006425B1 (https=) |
| WO (1) | WO2019081283A1 (https=) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP7277455B2 (ja) * | 2017-10-27 | 2023-05-19 | ビーエーエスエフ ソシエタス・ヨーロピア | Ｅｄａ含有混合物からのｎ－メチルエチレンジアミンの分離除去 |
| CN111018719B (zh) * | 2019-12-19 | 2023-03-21 | 西安近代化学研究所 | 一种提纯乙二胺的方法 |
| CN111747856B (zh) * | 2020-07-17 | 2022-12-13 | 新中天环保股份有限公司 | 一种废溶剂的处理方法 |
| CN119451938A (zh) | 2022-06-29 | 2025-02-14 | 巴斯夫欧洲公司 | 用于制造亚乙基胺的方法 |
| WO2024002740A1 (en) | 2022-06-29 | 2024-01-04 | Basf Se | Method for manufacture of ethyleneamines |
| CN115057784B (zh) * | 2022-07-13 | 2024-04-05 | 山东胜邦绿野化学有限公司 | 一种辛菌胺废水处理方法 |
| CN116375665B (zh) * | 2023-04-07 | 2025-02-25 | 福建钰融科技有限公司 | 一种含羟乙基哌嗪与羟乙基乙二胺的混合废液精制回收工艺 |
| KR20260039702A (ko) * | 2023-07-17 | 2026-03-20 | 바스프 에스이 | 새로운 냉각제 조성물 |
| WO2025125094A1 (en) | 2023-12-14 | 2025-06-19 | Basf Se | Process for preparing diethylenetriamine and/or ethylene glycol |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101384543A (zh) * | 2006-02-14 | 2009-03-11 | 巴斯夫欧洲公司 | 蒸馏分离含有单乙二醇和二亚乙基三胺的混合物的方法 |
| CN102639485A (zh) * | 2009-12-02 | 2012-08-15 | 巴斯夫欧洲公司 | 蒸馏包含乙二胺、n-甲基乙二胺和水的混合物的方法以及可由此得到的具有低n-甲基乙二胺含量的乙二胺和n-甲基乙二胺的混合物 |
| CN106103405A (zh) * | 2014-03-13 | 2016-11-09 | 巴斯夫欧洲公司 | 蒸馏提纯eda的方法 |
Family Cites Families (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2519803A (en) | 1946-02-05 | 1950-08-22 | Du Pont | Preparation of ethylene diamines |
| US2861995A (en) | 1956-04-27 | 1958-11-25 | Dow Chemical Co | Process for the conversion of ethanolamine |
| US3112318A (en) | 1957-10-09 | 1963-11-26 | Union Carbide Corp | Method for producing piperazine |
| DE1154121B (de) | 1959-08-03 | 1963-09-12 | Rohm & Haas | Verfahren zur Herstellung von AEthylendiamin |
| US3137730A (en) | 1960-04-12 | 1964-06-16 | Allied Chem | Production of ethylenediamine |
| DE1172268B (de) | 1962-02-21 | 1964-06-18 | Basf Ag | Verfahren zur Herstellung von Diaminen |
| US4123462A (en) | 1976-01-07 | 1978-10-31 | Union Carbide Corporation | Amination process using nickel-rhenium catalysts |
| WO2000006756A1 (en) | 1998-07-28 | 2000-02-10 | E.I. Du Pont De Nemours And Company | Sulfur metabolism enzymes |
| DE10349059A1 (de) | 2003-10-17 | 2005-05-19 | Basf Ag | Verfahren zur destillativen Auftrennung von Gemischen enthaltend Ethylenamine |
| DE102005019373A1 (de) * | 2005-04-26 | 2006-11-02 | Basf Ag | Verfahren zur Herstellung von Ethylenaminen |
| CN1723887A (zh) | 2005-07-20 | 2006-01-25 | 重庆福瑞制药有限公司 | 一种紫杉醇注射剂及其制备方法 |
| US7635790B2 (en) | 2006-02-14 | 2009-12-22 | Basf Se | Method for producing ethylene amines and ethanol amines by the hydrogenating amination of monoethylene glycol and ammonia in the presence of a catalyst |
| WO2007093514A1 (de) | 2006-02-14 | 2007-08-23 | Basf Se | Verfahren zur herstellung von ethylenaminen und ethanolaminen aus monoethylenglykol (meg) |
| US7919655B2 (en) | 2006-07-14 | 2011-04-05 | Basf Se | Method for producing an amine |
| RU2009104740A (ru) | 2006-07-14 | 2010-08-27 | Басф Се (De) | Способ получения амина |
| US8299249B2 (en) | 2007-03-01 | 2012-10-30 | Basf Se | Method for producing TETA by means of EDDN |
| RU2478092C2 (ru) | 2007-03-01 | 2013-03-27 | Басф Се | Способ получения смесей этиленаминов |
| EP2132165B1 (de) | 2007-03-01 | 2014-04-23 | Basf Se | Verfahren zur herstellung von ethylendiamin |
| EP2166481A4 (en) | 2007-07-09 | 2011-11-02 | Fujitsu Ltd | DEVICE, METHOD AND USER AUTHENTICATION PROGRAM |
| ATE553844T1 (de) | 2007-12-21 | 2012-05-15 | Basf Se | Verfahren zur herstellung eines amins |
| WO2010042168A2 (en) * | 2008-10-06 | 2010-04-15 | Dow Global Technologies Inc. | Methods for making ethanolamine(s) and ethyleneamine(s) from ethylene oxide and ammonia, and related methods |
| JP2012504610A (ja) | 2008-10-06 | 2012-02-23 | ユニオン カーバイド ケミカルズ アンド プラスティックス テクノロジー エルエルシー | エチレンアミンの製造方法 |
| CN102190588A (zh) | 2010-03-16 | 2011-09-21 | 张家港惠尔化学科技有限公司 | 乙二醇与氨制乙二胺的方法 |
| CN102233272A (zh) | 2010-04-22 | 2011-11-09 | 张家港惠尔化学科技有限公司 | 乙二醇氨化制乙二胺的催化剂及其制备方法 |
| SG11201401354QA (en) | 2011-11-17 | 2014-08-28 | Basf Se | Process for producing sn-containing catalysts |
| CN105585502B (zh) * | 2014-10-24 | 2018-09-14 | 中国石油化工股份有限公司 | 催化氨化法生产乙二胺的方法 |
| CN106607060B (zh) | 2015-10-26 | 2019-08-20 | 中国石油化工股份有限公司 | 催化剂及其制备方法和应用以及乙二醇临氢胺化制乙二胺的方法 |
| EP3634935B1 (de) | 2017-06-09 | 2022-03-09 | Basf Se | Verfahren zur herstellung von ethylenaminen |
| US11214535B2 (en) | 2017-06-09 | 2022-01-04 | Basf Se | Method for producing ethyleneamines |
-
2018
- 2018-10-17 US US16/759,347 patent/US11339117B2/en active Active
- 2018-10-17 JP JP2020523439A patent/JP7268017B2/ja active Active
- 2018-10-17 WO PCT/EP2018/078320 patent/WO2019081283A1/de not_active Ceased
- 2018-10-17 EP EP18785384.1A patent/EP3700883B1/de active Active
- 2018-10-17 BR BR112020006425-4A patent/BR112020006425B1/pt active IP Right Grant
- 2018-10-17 CN CN201880069384.9A patent/CN111263746B/zh active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101384543A (zh) * | 2006-02-14 | 2009-03-11 | 巴斯夫欧洲公司 | 蒸馏分离含有单乙二醇和二亚乙基三胺的混合物的方法 |
| CN102639485A (zh) * | 2009-12-02 | 2012-08-15 | 巴斯夫欧洲公司 | 蒸馏包含乙二胺、n-甲基乙二胺和水的混合物的方法以及可由此得到的具有低n-甲基乙二胺含量的乙二胺和n-甲基乙二胺的混合物 |
| CN106103405A (zh) * | 2014-03-13 | 2016-11-09 | 巴斯夫欧洲公司 | 蒸馏提纯eda的方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JP7268017B2 (ja) | 2023-05-02 |
| US20200308097A1 (en) | 2020-10-01 |
| EP3700883B1 (de) | 2022-04-20 |
| BR112020006425A2 (pt) | 2020-09-24 |
| US11339117B2 (en) | 2022-05-24 |
| WO2019081283A1 (de) | 2019-05-02 |
| BR112020006425B1 (pt) | 2023-03-21 |
| JP2021500389A (ja) | 2021-01-07 |
| CN111263746A (zh) | 2020-06-09 |
| EP3700883A1 (de) | 2020-09-02 |
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| PB01 | Publication | ||
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| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |