BR112017007614B8 - Processo para produção de 1,1,1,3-tetracloropropano de alta qualidade - Google Patents

Processo para produção de 1,1,1,3-tetracloropropano de alta qualidade

Info

Publication number
BR112017007614B8
BR112017007614B8 BR112017007614A BR112017007614A BR112017007614B8 BR 112017007614 B8 BR112017007614 B8 BR 112017007614B8 BR 112017007614 A BR112017007614 A BR 112017007614A BR 112017007614 A BR112017007614 A BR 112017007614A BR 112017007614 B8 BR112017007614 B8 BR 112017007614B8
Authority
BR
Brazil
Prior art keywords
reaction mixture
alkylation zone
extracted
mixture
main alkylation
Prior art date
Application number
BR112017007614A
Other languages
English (en)
Other versions
BR112017007614A2 (pt
BR112017007614B1 (pt
Inventor
Filas Karel
Kubicek Pavel
ONDRUS Zdenek
Sladek Petr
Original Assignee
Spolek Pro Chemickou A Hutni Vyrobu As
Spolchemie Zebra A S
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Spolek Pro Chemickou A Hutni Vyrobu As, Spolchemie Zebra A S filed Critical Spolek Pro Chemickou A Hutni Vyrobu As
Publication of BR112017007614A2 publication Critical patent/BR112017007614A2/pt
Publication of BR112017007614B1 publication Critical patent/BR112017007614B1/pt
Publication of BR112017007614B8 publication Critical patent/BR112017007614B8/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/013—Preparation of halogenated hydrocarbons by addition of halogens
    • C07C17/02—Preparation of halogenated hydrocarbons by addition of halogens to unsaturated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/272—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/272—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions
    • C07C17/275—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions of hydrocarbons and halogenated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/272—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions
    • C07C17/278—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions of only halogenated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00—Acyclic saturated compounds containing halogen atoms
    • C07C19/01—Acyclic saturated compounds containing halogen atoms containing chlorine
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)

Abstract

É descrito um processo para produção de um alcano C3-6 clorado compreendendo prover uma mistura de reação compreendendo um alceno e tetracloreto de carbono em uma zona de alquilação principal para produzir alcano C3-6 clorado na mistura de reação, e extrair uma porção da mistura de reação a partir da zona de alquilação principal, em que: a) a concentração do alcano C3-6 clorado na mistura de reação na zona de alquilação principal é mantida em um nível tal que a razão molar de alcano C3-6 clorado : tetracloreto de carbono na mistura de reação extraída da zona de alquilação não excede 95:5 quando a zona de alquilação principal está em operação contínua; e/ou b) a mistura de reação extraída da zona de alquilação principal compreende adicionalmente alceno e a mistura de reação está sujeita a uma etapa de desalcenização no qual pelo menos cerca de 50% em peso ou mais do alceno presente na mistura de reação é extraído do mesmo e pelo menos cerca de 50% do alceno extraído é realimentado na mistura de reação provida na zona de alquilação principal; e/ou c) a mistura de reação presente na zona de alquilação principal e extraída da zona de alquilação principal compreende adicionalmente um catalisador, e a mistura de reação extraída da zona de alquilação principal está sujeita a uma etapa de tratamento aquoso na qual a mistura de reação entra em contato com um meio aquoso em uma zona de tratamento aquoso, uma mistura bifásica é formada e uma fase orgânica compreendendo catalisador é extraída da mistura bifásica.
BR112017007614A 2014-10-16 2015-10-15 Processo para produção de 1,1,1,3-tetracloropropano de alta qualidade BR112017007614B8 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
CZPV2014-707 2014-10-16
CZ2014707 2014-10-16
PCT/CZ2015/000120 WO2016058566A1 (en) 2014-10-16 2015-10-15 Process

Publications (3)

Publication Number Publication Date
BR112017007614A2 BR112017007614A2 (pt) 2018-01-30
BR112017007614B1 BR112017007614B1 (pt) 2021-06-01
BR112017007614B8 true BR112017007614B8 (pt) 2022-08-23

Family

ID=54478524

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112017007614A BR112017007614B8 (pt) 2014-10-16 2015-10-15 Processo para produção de 1,1,1,3-tetracloropropano de alta qualidade

Country Status (13)

Country Link
US (4) US9896400B2 (pt)
EP (1) EP3207014B1 (pt)
JP (2) JP6867291B2 (pt)
KR (1) KR102599573B1 (pt)
CN (1) CN107001191B (pt)
BR (1) BR112017007614B8 (pt)
CZ (1) CZ309296B6 (pt)
ES (1) ES2911909T3 (pt)
MX (1) MX2017004847A (pt)
RU (1) RU2745702C2 (pt)
SA (1) SA517381316B1 (pt)
TW (1) TWI712579B (pt)
WO (1) WO2016058566A1 (pt)

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US10029962B2 (en) 2015-08-19 2018-07-24 Spolek Pro Chemickou A Hutni Vyrobu A.S. Process for producing C3 chlorinated alkane and alkene compounds
CZ309497B6 (cs) 2016-04-13 2023-03-01 Spolchemie Zebra, A.S. Způsob výroby chlorovaného alkanu
US20190169100A1 (en) * 2016-06-23 2019-06-06 Blue Cube Ip Llc Process for the dehydrochlorination of a chloroalkane
EP3490964B1 (en) * 2016-07-27 2021-08-25 The Chemours Company FC, LLC Process for producing halogenated olefins
CZ309472B6 (cs) 2016-09-02 2023-02-08 Spolek Pro Chemickou A Hutní Výrobu, Akciová Společnost Způsob výroby tetrachlormethanu
CN111902385A (zh) * 2018-04-03 2020-11-06 蓝立方知识产权有限责任公司 改进的制备卤化烷烃的方法
US11192840B2 (en) 2018-04-03 2021-12-07 Blue Cube Ip Llc Method for recycling catalyst in the production of chlorinated alkanes
CN114478876A (zh) * 2020-10-23 2022-05-13 中国石油化工股份有限公司 一种采用间歇液相法生产聚乙烯的方法和聚乙烯
WO2022115151A1 (en) * 2020-11-30 2022-06-02 Blue Cube Ip Llc Method for treating a heavy byproduct stream from chlorinated propane production

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ATE22877T1 (de) * 1983-07-06 1986-11-15 Monsanto Co Verfahren zur herstellung von monoaddukten von olefinen und damit reagierfaehigen telogenen.
US5902914A (en) 1995-08-14 1999-05-11 Alliedsignal Inc. Process for the preparation of halogenated alkanes
US6187978B1 (en) 1999-05-12 2001-02-13 Alliedsignal Inc. Continuous process for manufacturing halogenated compounds
ATE420063T1 (de) * 1999-10-06 2009-01-15 Solvay Verfahren zur herstellung von halogenierten kohlenwasserstoffen in gegenwart eines cokatalysators
JP2001335517A (ja) * 2000-05-29 2001-12-04 Central Glass Co Ltd １，１，１，３，３−ペンタクロロプロパンの製造方法
US6313360B1 (en) 2000-09-29 2001-11-06 Vulcan Materials Company Process for the manufacture of 1, 1, 1, 3, 3-pentachloropropane
US20050177012A1 (en) * 2001-07-20 2005-08-11 Pcbu Services, Inc. Halocarbon production processes, halocarbon separation processes, and halocarbon separation systems
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US20040225166A1 (en) * 2003-05-05 2004-11-11 Vulcan Chemicals A Business Group Of Vulcan Materials Company Method for producing 1,1,1,3-tetrachloropropane and other haloalkanes with iron catalyst
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JP5858830B2 (ja) 2012-03-14 2016-02-10 株式会社トクヤマ ポリクロロプロパンの製造方法
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US8889928B2 (en) * 2013-03-12 2014-11-18 Honeywell International Inc. Method to improve 1,1,3-trichloropropene and/or 3,3,3-trichloropropene selectivity during the dehydrochlorination of 1,1,1,3-tetrachloropropane
US9255045B2 (en) * 2014-01-13 2016-02-09 Arkema France E-1-chloro-3,3,3-trifluoropropene production process from 1,1,3,3-tetrachloropropene
FR3036398B1 (fr) * 2015-05-22 2019-05-03 Arkema France Compositions a base de 1,1,3,3-tetrachloropropene

Also Published As

Publication number Publication date
WO2016058566A9 (en) 2016-09-09
KR20170070071A (ko) 2017-06-21
US9896400B2 (en) 2018-02-20
CN107001191A (zh) 2017-08-01
CZ2016129A3 (cs) 2016-08-10
US20190233352A1 (en) 2019-08-01
BR112017007614A2 (pt) 2018-01-30
JP2021088574A (ja) 2021-06-10
JP2017532379A (ja) 2017-11-02
EP3207014B1 (en) 2022-02-23
MX2017004847A (es) 2017-12-07
EP3207014A1 (en) 2017-08-23
CZ309296B6 (cs) 2022-08-10
KR102599573B1 (ko) 2023-11-06
US10294179B2 (en) 2019-05-21
TWI712579B (zh) 2020-12-11
US20210188742A1 (en) 2021-06-24
CN107001191B (zh) 2021-08-10
US20180141884A1 (en) 2018-05-24
SA517381316B1 (ar) 2021-08-31
JP7064112B2 (ja) 2022-05-10
US11325876B2 (en) 2022-05-10
JP6867291B2 (ja) 2021-04-28
US20160107955A1 (en) 2016-04-21
WO2016058566A1 (en) 2016-04-21
RU2017116146A (ru) 2018-11-16
BR112017007614B1 (pt) 2021-06-01
US10934232B2 (en) 2021-03-02
RU2017116146A3 (pt) 2019-01-24
TW201623200A (zh) 2016-07-01
RU2745702C2 (ru) 2021-03-30
ES2911909T3 (es) 2022-05-23

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Legal Events

Date Code Title Description
B06U Preliminary requirement: requests with searches performed by other patent offices: procedure suspended [chapter 6.21 patent gazette]
B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 15/10/2015, OBSERVADAS AS CONDICOES LEGAIS.

B25A Requested transfer of rights approved

Owner name: SPOLCHEMIE ZEBRA, A.S. (CZ)