BR112014011308B1 - Processo sintético livre de organotemplate para a produção de um material zeolítico, material zeolítico livre de organotemplate sintético e uso do mesmo - Google Patents

Processo sintético livre de organotemplate para a produção de um material zeolítico, material zeolítico livre de organotemplate sintético e uso do mesmo Download PDF

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Publication number
BR112014011308B1
BR112014011308B1 BR112014011308-4A BR112014011308A BR112014011308B1 BR 112014011308 B1 BR112014011308 B1 BR 112014011308B1 BR 112014011308 A BR112014011308 A BR 112014011308A BR 112014011308 B1 BR112014011308 B1 BR 112014011308B1
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BR
Brazil
Prior art keywords
cha
frame structure
ppm
group
zeolitic material
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BR112014011308-4A
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English (en)
Portuguese (pt)
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BR112014011308A2 (pt
Inventor
Stefan Maurer
Hanpeng Jin
Jeff Yang
Ulrich Müller
Original Assignee
Basf Se
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Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of BR112014011308A2 publication Critical patent/BR112014011308A2/pt
Publication of BR112014011308B1 publication Critical patent/BR112014011308B1/pt

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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7015—CHA-type, e.g. Chabazite, LZ-218
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/06—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
    • C01B39/10—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis the replacing atoms being at least phosphorus atoms
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10—After treatment, characterised by the effect to be obtained
    • B01J2229/18—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself
    • B01J2229/186—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself not in framework positions

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Compositions Of Oxide Ceramics (AREA)
BR112014011308-4A 2011-11-11 2012-11-09 Processo sintético livre de organotemplate para a produção de um material zeolítico, material zeolítico livre de organotemplate sintético e uso do mesmo BR112014011308B1 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP11188857 2011-11-11
EP11188857.4 2011-11-11
PCT/IB2012/056292 WO2013068976A1 (en) 2011-11-11 2012-11-09 Organotemplate-free synthetic process for the production of a zeolitic material of the cha-type structure

Publications (2)

Publication Number Publication Date
BR112014011308A2 BR112014011308A2 (pt) 2017-05-09
BR112014011308B1 true BR112014011308B1 (pt) 2021-04-13

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BR112014011308-4A BR112014011308B1 (pt) 2011-11-11 2012-11-09 Processo sintético livre de organotemplate para a produção de um material zeolítico, material zeolítico livre de organotemplate sintético e uso do mesmo

Country Status (12)

Country Link
EP (1) EP2776369B1 (https=)
JP (1) JP6324895B2 (https=)
KR (1) KR102032584B1 (https=)
CN (1) CN104039704B (https=)
BR (1) BR112014011308B1 (https=)
CA (1) CA2855572C (https=)
IN (1) IN2014CN03353A (https=)
MX (1) MX375064B (https=)
PL (1) PL2776369T3 (https=)
RU (1) RU2612697C2 (https=)
WO (1) WO2013068976A1 (https=)
ZA (1) ZA201404210B (https=)

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EP2928824B1 (en) * 2012-12-10 2017-08-09 ExxonMobil Research and Engineering Company Seeded synthesis of aluminosilicate cha molecular sieve
EP3233273A1 (en) * 2014-12-17 2017-10-25 SABIC Global Technologies B.V. Silicoaluminophosphate catalyst for chloromethane conversion
ES2574500B1 (es) * 2014-12-17 2017-03-31 Consejo Superior De Investigaciones Científicas (Csic) Síntesis de la zeolita con la estructura cristalina CHA, procedimiento de síntesis y su uso en aplicaciones catalíticas
US10710059B2 (en) * 2015-12-22 2020-07-14 Basf Corporation Process for preparing iron(III)-exchanged zeolite composition
CN121800199A (zh) * 2016-06-08 2026-04-07 巴斯夫公司 来自无有机模板的合成的cha骨架结构的铜助催化沸石材料及其在nox的选择性催化还原中的用途
CN109311006B (zh) 2016-06-08 2022-09-27 巴斯夫公司 铜助催化的钠菱沸石及其在NOx的选择性催化还原中的用途
CN106145138B (zh) * 2016-06-27 2018-05-08 杨晓波 一种合成具有菱沸石结构的沸石分子筛的方法
CN106145137B (zh) * 2016-06-27 2018-06-05 杨晓波 一种直接水热合成中硅铝比菱沸石的方法
WO2018102555A1 (en) * 2016-12-02 2018-06-07 Ecolab USA, Inc. Polyaluminum salts and their uses in preparation of high-purity colloidal aluminum-silica composite particles and zeolites
JP7229175B2 (ja) 2017-05-15 2023-02-27 ビーエーエスエフ コーポレーション 金属ｍを含み、フレームワークタイプａｅｉを有するゼオライト系材料を製造する方法
EP3625171B1 (en) 2017-05-15 2024-03-13 BASF Corporation A process for preparing a zeolitic material having framework type aei
AU2018299887B2 (en) * 2017-07-11 2021-07-29 Shell Internationale Research Maatschappij B.V. A catalyst and method of use thereof
JP2020533164A (ja) * 2017-09-07 2020-11-19 ビーエーエスエフ コーポレーション 骨格外アルミニウムを減じたゼオライト
CN108217681B (zh) * 2018-01-19 2021-07-06 山东齐鲁华信高科有限公司 一种高铁含量的Fe-ZSM-5分子筛的制备方法
CN108083292B (zh) * 2018-01-31 2020-12-29 吉林大学 一种磷掺杂cha分子筛、制备方法及其应用
JP7412354B2 (ja) 2018-05-25 2024-01-12 ビーエーエスエフ ソシエタス・ヨーロピア アルミニウムに富む希土類元素含有ゼオライト材料
EP3830031A1 (en) 2018-07-27 2021-06-09 Basf Se Process for preparing a zeolitic material having a framework type fer
EP3969420A1 (en) 2019-05-15 2022-03-23 Basf Se Process for the production of the cha-aft zeolite intergrowth coe-10 and use thereof in heterogeneous catalysis
CN111348660B (zh) * 2020-03-16 2022-08-09 江西师范大学 一种中硅cha型分子筛及其制备方法和应用
CN111762795B (zh) * 2020-07-13 2022-10-14 包头稀土研究院 含有稀土元素的分子筛及其生产方法
CN111762794B (zh) * 2020-07-13 2022-08-05 包头稀土研究院 分子筛及其制备方法
EP4015454A1 (en) * 2020-12-21 2022-06-22 Tosoh Corporation Cha-type zeolite and manufacturing method thereof
CN112919493B (zh) * 2021-02-05 2022-10-14 正大能源材料(大连)有限公司 一种低成本制备ssz-13分子筛的方法及应用

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SU833498A1 (ru) * 1979-06-25 1981-05-30 Институт Общей И Неорганической Химииан Армянской Ccp Способ получени шабазита
SU1640112A1 (ru) * 1987-12-28 1991-04-07 Предприятие П/Я Р-6518 Синтетический натриево-цезиевый цеолит типа шабазит
JP4693239B2 (ja) 1998-07-29 2011-06-01 エクソン ケミカル パテンツ インコーポレイテッド 結晶性分子ふるい
ES2279105T3 (es) * 2002-03-15 2007-08-16 Exxonmobil Chemical Patents, Inc. Chabacita rica en silice, su sintesis y su utilizacion en la conversion de compuestos oxigenados en olefinas.
EP1701913B1 (en) * 2003-12-23 2017-01-25 ExxonMobil Chemical Patents Inc. Chabazite-type molecular sieve and its synthesis method
US20090196812A1 (en) * 2008-01-31 2009-08-06 Basf Catalysts Llc Catalysts, Systems and Methods Utilizing Non-Zeolitic Metal-Containing Molecular Sieves Having the CHA Crystal Structure
US10583424B2 (en) * 2008-11-06 2020-03-10 Basf Corporation Chabazite zeolite catalysts having low silica to alumina ratios
CN104876237A (zh) * 2009-06-18 2015-09-02 巴斯夫欧洲公司 生产沸石材料的无有机模板合成方法
CN102665902A (zh) * 2009-11-24 2012-09-12 巴斯夫欧洲公司 制备具有cha结构的沸石的方法
CN102134081A (zh) * 2010-01-25 2011-07-27 天津海赛纳米材料有限公司 无模板剂存在下一种sapo-34分子筛的合成方法
CN102285666B (zh) * 2010-06-18 2015-02-04 江西师范大学 一种菱沸石及菱沸石膜的制备方法
WO2012145323A1 (en) * 2011-04-18 2012-10-26 Pq Corporation Large crystal, organic-free chabazite, methods of making and using the same
CN102442679B (zh) * 2011-09-29 2013-08-14 南开大学 一种菱沸石的合成方法

Also Published As

Publication number Publication date
KR102032584B1 (ko) 2019-10-15
PL2776369T3 (pl) 2022-06-20
KR20140093982A (ko) 2014-07-29
CN104039704B (zh) 2017-10-24
CN104039704A (zh) 2014-09-10
EP2776369A1 (en) 2014-09-17
IN2014CN03353A (https=) 2015-07-03
WO2013068976A1 (en) 2013-05-16
BR112014011308A2 (pt) 2017-05-09
EP2776369B1 (en) 2022-02-23
RU2014123614A (ru) 2015-12-20
CA2855572C (en) 2020-04-28
JP6324895B2 (ja) 2018-05-16
MX375064B (es) 2025-03-06
EP2776369A4 (en) 2015-08-05
MX2014005537A (es) 2014-09-16
RU2612697C2 (ru) 2017-03-13
CA2855572A1 (en) 2013-05-16
JP2015511919A (ja) 2015-04-23
ZA201404210B (en) 2015-08-26

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B06F Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette]
B06U Preliminary requirement: requests with searches performed by other patent offices: procedure suspended [chapter 6.21 patent gazette]
B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 09/11/2012, OBSERVADAS AS CONDICOES LEGAIS.

B25A Requested transfer of rights approved

Owner name: BASF CATALYSTS LLC (US)

B25A Requested transfer of rights approved

Owner name: BASF MOBILE EMISSIONS CATALYSTS LLC (US)