BR112013014808B1 - processo para produzir ácido acético - Google Patents

processo para produzir ácido acético Download PDF

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Publication number
BR112013014808B1
BR112013014808B1 BR112013014808-0A BR112013014808A BR112013014808B1 BR 112013014808 B1 BR112013014808 B1 BR 112013014808B1 BR 112013014808 A BR112013014808 A BR 112013014808A BR 112013014808 B1 BR112013014808 B1 BR 112013014808B1
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BR
Brazil
Prior art keywords
supernatant
methanol
acetic acid
acetaldehyde
weight
Prior art date
Application number
BR112013014808-0A
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English (en)
Portuguese (pt)
Other versions
BR112013014808A2 (pt
Inventor
Masahiko Shimizu
Ryuji Saito
Hiroyuki Miura
Original Assignee
Daicel Corporation
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
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Application filed by Daicel Corporation filed Critical Daicel Corporation
Publication of BR112013014808A2 publication Critical patent/BR112013014808A2/pt
Publication of BR112013014808B1 publication Critical patent/BR112013014808B1/pt

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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/10Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide
    • C07C51/12Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide on an oxygen-containing group in organic compounds, e.g. alcohols
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07BGENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B61/00Other general methods
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/10Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/43Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/43Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C07C51/46Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation by azeotropic distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/50Use of additives, e.g. for stabilisation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C53/00Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
    • C07C53/08Acetic acid
BR112013014808-0A 2010-12-15 2011-12-01 processo para produzir ácido acético BR112013014808B1 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2010279799 2010-12-15
JP2010-279799 2010-12-15
PCT/JP2011/077846 WO2012081418A1 (ja) 2010-12-15 2011-12-01 酢酸の製造方法

Publications (2)

Publication Number Publication Date
BR112013014808A2 BR112013014808A2 (pt) 2020-08-11
BR112013014808B1 true BR112013014808B1 (pt) 2021-03-02

Family

ID=46244527

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112013014808-0A BR112013014808B1 (pt) 2010-12-15 2011-12-01 processo para produzir ácido acético

Country Status (13)

Country Link
US (3) USRE46999E1 (de)
EP (1) EP2653458B2 (de)
JP (1) JP5914358B2 (de)
KR (1) KR101874661B1 (de)
CN (1) CN103402964B (de)
BR (1) BR112013014808B1 (de)
ES (1) ES2646749T5 (de)
MX (1) MX338849B (de)
MY (1) MY161174A (de)
SA (1) SA111330055B1 (de)
SG (1) SG190941A1 (de)
TW (1) TWI511950B (de)
WO (1) WO2012081418A1 (de)

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JP5872477B2 (ja) 2010-10-06 2016-03-01 株式会社ダイセル 酢酸の製造方法
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TWI547477B (zh) 2012-03-14 2016-09-01 大賽璐股份有限公司 醋酸之製造方法
AR094541A1 (es) * 2013-01-25 2015-08-12 Daicel Corp Procedimiento para producir ácido carboxílico
EP3201165B1 (de) 2014-10-02 2019-08-21 Celanese International Corporation Verfahren zur herstellung von essigsäure
US9340481B1 (en) 2014-11-14 2016-05-17 Celanese International Corporation Process for flashing a reaction medium comprising lithium acetate
SG11201703380PA (en) * 2014-11-14 2017-05-30 Celanese Int Corp Processes for producing acetic acid with decanter control
US9260369B1 (en) 2014-11-14 2016-02-16 Celanese International Corporation Processes for producing acetic acid product having low butyl acetate content
WO2016077672A1 (en) 2014-11-14 2016-05-19 Celanese International Corporation Processes for improving acetic acid yield by removing iron
US9458077B2 (en) 2014-11-14 2016-10-04 Celanese International Corporation Reducing hydrogen iodide content in carbonylation processes
US9302975B1 (en) 2015-07-01 2016-04-05 Celanese International Corporation Process for flashing a reaction medium
US9540304B2 (en) 2014-11-14 2017-01-10 Celanese International Corporation Processes for producing an acetic acid product having low butyl acetate content
US9458078B2 (en) 2014-11-14 2016-10-04 Celanese International Corporation Processes for producing acetic acid from a reaction medium having low ethyl iodide content
US9233907B1 (en) 2014-11-14 2016-01-12 Celanese International Corporation Reducing hydrogen iodide content in carbonylation processes
CN107108431B (zh) 2014-11-14 2023-02-03 国际人造丝公司 通过引入锂化合物生产乙酸的方法
US9487464B2 (en) 2015-01-30 2016-11-08 Celanese International Corporation Processes for producing acetic acid
KR102493738B1 (ko) 2015-01-30 2023-01-30 셀라니즈 인터내셔날 코포레이션 아세트산의 제조 방법
US9540302B2 (en) 2015-04-01 2017-01-10 Celanese International Corporation Processes for producing acetic acid
US9561994B2 (en) 2015-01-30 2017-02-07 Celanese International Corporation Processes for producing acetic acid
WO2016122728A1 (en) 2015-01-30 2016-08-04 Celanese International Corporation Processes for producing acetic acid
US9505696B2 (en) 2015-02-04 2016-11-29 Celanese International Corporation Process to control HI concentration in residuum stream
US9512056B2 (en) 2015-02-04 2016-12-06 Celanese International Corporation Process to control HI concentration in residuum stream
US10413840B2 (en) 2015-02-04 2019-09-17 Celanese International Coporation Process to control HI concentration in residuum stream
US9540303B2 (en) 2015-04-01 2017-01-10 Celanese International Corporation Processes for producing acetic acid
US9302974B1 (en) 2015-07-01 2016-04-05 Celanese International Corporation Process for producing acetic acid
US9382183B1 (en) 2015-07-01 2016-07-05 Celanese International Corporation Process for flashing a reaction medium
US9382186B1 (en) 2015-07-01 2016-07-05 Celanese International Corporation Process for producing acetic acid
US9416088B1 (en) 2015-10-02 2016-08-16 Celanese International Corporation Process to produce acetic acid with recycle of water
US9957216B2 (en) 2015-11-13 2018-05-01 Celanese International Corporation Processes for producing acetic acid
US9908835B2 (en) 2015-11-13 2018-03-06 Celanese International Corporation Processes for purifying acetic and hydrating anhydride
CN109415291B (zh) * 2016-07-07 2022-01-04 株式会社大赛璐 乙酸制造工艺
WO2018135014A1 (ja) 2017-01-18 2018-07-26 株式会社ダイセル 酢酸の製造方法
CN110049963B (zh) * 2017-01-18 2022-02-18 株式会社大赛璐 乙酸的制备方法
ES2779805T3 (es) * 2017-03-28 2020-08-19 Daicel Corp Método para la producción de ácido acético
US10308581B2 (en) 2017-03-28 2019-06-04 Daicel Corporation Method for producing acetic acid
WO2019224358A1 (en) 2018-05-24 2019-11-28 Vkr Holding A/S Vig unit lamination
KR102594450B1 (ko) * 2018-07-02 2023-10-27 주식회사 다이셀 아세트산의 제조 방법

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US3769329A (en) 1970-03-12 1973-10-30 Monsanto Co Production of carboxylic acids and esters
US5001259A (en) 1984-05-03 1991-03-19 Hoechst Celanese Corporation Methanol carbonylation process
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JP3244385B2 (ja) 1994-06-15 2002-01-07 ダイセル化学工業株式会社 高純度酢酸の製造方法
JP3581725B2 (ja) 1994-06-30 2004-10-27 ダイセル化学工業株式会社 アセトアルデヒドとヨウ化メチルの分離方法
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US6339171B1 (en) 1996-10-18 2002-01-15 Celanese International Corporation Removal or reduction of permanganate reducing compounds and alkyl iodides from a carbonylation process stream
JP4242952B2 (ja) * 1998-08-31 2009-03-25 ダイセル化学工業株式会社 酢酸の製造方法
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US7271293B2 (en) * 2004-03-02 2007-09-18 Celanese International Corporation Control method for process of removing permanganate reducing compounds from methanol carbonylation process
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JP4489487B2 (ja) * 2004-04-02 2010-06-23 ダイセル化学工業株式会社 ヨウ化水素の分離方法
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US7820855B2 (en) 2008-04-29 2010-10-26 Celanese International Corporation Method and apparatus for carbonylating methanol with acetic acid enriched flash stream
JP5933168B2 (ja) 2010-09-24 2016-06-08 株式会社三共 遊技機
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MX338849B (es) * 2010-12-15 2016-05-02 Daicel Corp Procedimiento para producir acido acetico.
JP6166043B2 (ja) * 2010-12-15 2017-07-19 株式会社ダイセル 酢酸の製造方法
KR101879006B1 (ko) * 2010-12-15 2018-07-16 주식회사 다이셀 아세트산의 제조 방법

Also Published As

Publication number Publication date
MX338849B (es) 2016-05-02
MX2013006884A (es) 2013-07-05
JP5914358B2 (ja) 2016-05-11
ES2646749T5 (es) 2021-10-21
EP2653458A4 (de) 2015-12-09
ES2646749T3 (es) 2017-12-15
MY161174A (en) 2017-04-14
US20130281735A1 (en) 2013-10-24
CN103402964A (zh) 2013-11-20
US9162958B2 (en) 2015-10-20
EP2653458B2 (de) 2021-03-17
WO2012081418A1 (ja) 2012-06-21
EP2653458B1 (de) 2017-09-13
SG190941A1 (en) 2013-08-30
KR20140032367A (ko) 2014-03-14
JPWO2012081418A1 (ja) 2014-05-22
USRE46999E1 (en) 2018-08-21
TW201231450A (en) 2012-08-01
CN103402964B (zh) 2015-09-02
EP2653458A1 (de) 2013-10-23
SA111330055B1 (ar) 2015-03-31
USRE47569E1 (en) 2019-08-13
BR112013014808A2 (pt) 2020-08-11
TWI511950B (zh) 2015-12-11
KR101874661B1 (ko) 2018-07-04

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B06F Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette]
B06U Preliminary requirement: requests with searches performed by other patent offices: procedure suspended [chapter 6.21 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 01/12/2011, OBSERVADAS AS CONDICOES LEGAIS.

B21F Lapse acc. art. 78, item iv - on non-payment of the annual fees in time

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B24J Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12)

Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2699 DE 27-09-2022 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013.