BR112013000758A8 - Processo para preparar- 5 amino -3- ciano-1- (2,6 dicloro-4 triflúor metil fenil)-4- triflúor metil sulfinil-pirazol - Google Patents
Processo para preparar- 5 amino -3- ciano-1- (2,6 dicloro-4 triflúor metil fenil)-4- triflúor metil sulfinil-pirazolInfo
- Publication number
- BR112013000758A8 BR112013000758A8 BR112013000758A BR112013000758A BR112013000758A8 BR 112013000758 A8 BR112013000758 A8 BR 112013000758A8 BR 112013000758 A BR112013000758 A BR 112013000758A BR 112013000758 A BR112013000758 A BR 112013000758A BR 112013000758 A8 BR112013000758 A8 BR 112013000758A8
- Authority
- BR
- Brazil
- Prior art keywords
- amino
- pyrazole
- dichloro
- preparing
- trifluor methyl
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D231/44—Oxygen and nitrogen or sulfur and nitrogen atoms
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
- A01N43/56—1,2-Diazoles; Hydrogenated 1,2-diazoles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P33/00—Antiparasitic agents
- A61P33/14—Ectoparasiticides, e.g. scabicides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- General Chemical & Material Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Pharmacology & Pharmacy (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Animal Behavior & Ethology (AREA)
- Tropical Medicine & Parasitology (AREA)
- Public Health (AREA)
- Agronomy & Crop Science (AREA)
- Medicinal Chemistry (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Plural Heterocyclic Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
PROCESSO PARA PREPARAR 5-AMINO-3-CIANO-1-(2,6-DICLORO-4-TRIFLÚOR METIL FENIL) -4- TRIFLÚOR METIL SULFINIL- PIRAZOL Descreve- se um processo de oxidação melhorado para preparar 5- amino -3 ciano -1- ( 2,6-dicloro-4- triflúor metil fenil ) -4- triflúor sulfinil -pirazol de fórmula (i),o processo inclui misturar 5- amino -3 ciano -1 (2,6 docloro -4- triflúor metil fenil )-4- triflúor netil tiopirazol de fórmula (II) com ácido dicloro acético e peroxido de hidrgênio na presença de um ácido forte.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US36336610P | 2010-07-12 | 2010-07-12 | |
PCT/IL2011/000546 WO2012007938A1 (en) | 2010-07-12 | 2011-07-10 | Fipronil production process |
Publications (2)
Publication Number | Publication Date |
---|---|
BR112013000758A2 BR112013000758A2 (pt) | 2016-05-24 |
BR112013000758A8 true BR112013000758A8 (pt) | 2018-02-14 |
Family
ID=44645163
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR112013000758A BR112013000758A8 (pt) | 2010-07-12 | 2011-07-10 | Processo para preparar- 5 amino -3- ciano-1- (2,6 dicloro-4 triflúor metil fenil)-4- triflúor metil sulfinil-pirazol |
Country Status (13)
Country | Link |
---|---|
US (10) | US20130197238A1 (pt) |
EP (1) | EP2593436A1 (pt) |
JP (1) | JP2013532187A (pt) |
KR (1) | KR20130124473A (pt) |
CN (1) | CN103153961A (pt) |
AU (1) | AU2011277946B2 (pt) |
BR (1) | BR112013000758A8 (pt) |
CA (1) | CA2805227A1 (pt) |
CO (1) | CO6660510A2 (pt) |
MX (1) | MX2013000374A (pt) |
NZ (1) | NZ605535A (pt) |
WO (1) | WO2012007938A1 (pt) |
ZA (1) | ZA201300195B (pt) |
Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA2630849C (en) | 2005-12-14 | 2013-05-14 | Makhteshim Chemical Works Ltd. | Polymorphs and amorphous forms of 5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-4-[(trifluoromethyl)sulfinyl]-1h-pyrazole-3-carbonitrile |
IT1400666B1 (it) | 2010-07-07 | 2013-06-28 | Finchimica Srl | Procedimento per la sintesi di 5-amino, 1-fenil, 3-ciano, 4-trifluorometil sulfinil pirazoli. |
CN102690232A (zh) * | 2012-05-30 | 2012-09-26 | 河南中医学院 | 一种氟虫腈中间体的合成方法 |
CN103360316B (zh) * | 2013-04-22 | 2015-02-11 | 浙江海正化工股份有限公司 | 一种氟虫腈的制备方法 |
DE112015002978T5 (de) * | 2014-06-26 | 2017-03-09 | Sumitomo Chemical Company, Limited | Verfahren zur Herstellung einer Phenolverbindung |
EP3412658A1 (en) * | 2017-06-09 | 2018-12-12 | Solvay Sa | Processes for the manufacture of sulfur-substitued pyrazole derivatives |
JP2021502991A (ja) | 2017-11-15 | 2021-02-04 | アダマ・マクテシム・リミテッド | 5−アミノ−1−(2,6−ジクロロ−4−トリフルオロメチル−フェニル)−4−エチルスルファニル−1h−ピラゾール−3−カルボニトリル及び関連化合物の合成 |
CN108318604A (zh) * | 2017-12-19 | 2018-07-24 | 上海市农产品质量安全检测中心 | 一种牛奶中氟虫腈及其代谢物的检测方法 |
KR102083906B1 (ko) | 2018-09-21 | 2020-03-03 | (주)스페이스링크 | 피프로닐 대사산물의 효과적인 제거 물질 생성장치 |
CN111004180A (zh) * | 2019-09-11 | 2020-04-14 | 浙江埃森化学有限公司 | 一种制备氟虫腈的方法 |
WO2021151976A1 (de) * | 2020-01-31 | 2021-08-05 | Bayer Aktiengesellschaft | [(1,4,5-trisubstituierte-1h-pyrazol-3-yl)sulfanyl]essigsäure derivate sowie deren salze und ihre verwendung als herbizide wirkstoffe |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB8713768D0 (en) | 1987-06-12 | 1987-07-15 | May & Baker Ltd | Compositions of matter |
ES2222743T3 (es) | 1999-10-22 | 2005-02-01 | Bayer Cropscience S.A. | Procedimiento para preparar un derivado 4-trifluorometilsulfinilpirazol. |
NZ568025A (en) * | 2006-04-25 | 2011-02-25 | Gharda Chemicals Ltd | Process for the preparation of fipronil, an insecticide, and related pyrazoles |
CN101250158B (zh) * | 2008-04-02 | 2011-12-07 | 湖南化工研究院 | 一种氟虫腈的制备方法 |
WO2010105969A1 (en) * | 2009-03-16 | 2010-09-23 | Basf Se | Process for the preparation of pyrazole derivatives |
EP2493860B1 (en) * | 2009-10-30 | 2014-01-15 | Basf Se | Process for the preparation of 4-sulfinyl-pyrazole derivatives |
IT1400666B1 (it) * | 2010-07-07 | 2013-06-28 | Finchimica Srl | Procedimento per la sintesi di 5-amino, 1-fenil, 3-ciano, 4-trifluorometil sulfinil pirazoli. |
-
2011
- 2011-07-10 EP EP11752348.0A patent/EP2593436A1/en not_active Withdrawn
- 2011-07-10 AU AU2011277946A patent/AU2011277946B2/en not_active Ceased
- 2011-07-10 BR BR112013000758A patent/BR112013000758A8/pt not_active Application Discontinuation
- 2011-07-10 NZ NZ60553511A patent/NZ605535A/en not_active IP Right Cessation
- 2011-07-10 CN CN2011800344333A patent/CN103153961A/zh active Pending
- 2011-07-10 MX MX2013000374A patent/MX2013000374A/es not_active Application Discontinuation
- 2011-07-10 JP JP2013519212A patent/JP2013532187A/ja not_active Ceased
- 2011-07-10 CA CA2805227A patent/CA2805227A1/en not_active Abandoned
- 2011-07-10 US US13/809,327 patent/US20130197238A1/en not_active Abandoned
- 2011-07-10 WO PCT/IL2011/000546 patent/WO2012007938A1/en active Application Filing
- 2011-07-10 KR KR1020137001662A patent/KR20130124473A/ko not_active Application Discontinuation
-
2012
- 2012-12-27 CO CO12234698A patent/CO6660510A2/es unknown
-
2013
- 2013-01-08 ZA ZA2013/00195A patent/ZA201300195B/en unknown
- 2013-06-25 US US13/926,389 patent/US20130289283A1/en not_active Abandoned
-
2014
- 2014-02-06 US US14/174,406 patent/US20140155620A1/en not_active Abandoned
- 2014-09-12 US US14/485,508 patent/US20150099892A1/en not_active Abandoned
-
2016
- 2016-06-29 US US15/196,633 patent/US20160304467A1/en not_active Abandoned
-
2017
- 2017-01-17 US US15/408,124 patent/US20170121290A1/en not_active Abandoned
- 2017-07-25 US US15/659,440 patent/US20170320832A1/en not_active Abandoned
-
2018
- 2018-02-02 US US15/887,231 patent/US20180155294A1/en not_active Abandoned
- 2018-05-29 US US15/991,776 patent/US20180282286A1/en not_active Abandoned
-
2019
- 2019-01-25 US US16/257,452 patent/US20190152921A1/en not_active Abandoned
Also Published As
Publication number | Publication date |
---|---|
US20150099892A1 (en) | 2015-04-09 |
CO6660510A2 (es) | 2013-04-30 |
US20170121290A1 (en) | 2017-05-04 |
US20190152921A1 (en) | 2019-05-23 |
US20180282286A1 (en) | 2018-10-04 |
US20160304467A1 (en) | 2016-10-20 |
BR112013000758A2 (pt) | 2016-05-24 |
KR20130124473A (ko) | 2013-11-14 |
MX2013000374A (es) | 2013-03-05 |
US20130289283A1 (en) | 2013-10-31 |
WO2012007938A8 (en) | 2012-12-13 |
AU2011277946A1 (en) | 2013-02-07 |
CA2805227A1 (en) | 2012-01-19 |
EP2593436A1 (en) | 2013-05-22 |
ZA201300195B (en) | 2013-09-25 |
US20130197238A1 (en) | 2013-08-01 |
US20180155294A1 (en) | 2018-06-07 |
NZ605535A (en) | 2015-03-27 |
WO2012007938A1 (en) | 2012-01-19 |
JP2013532187A (ja) | 2013-08-15 |
US20170320832A1 (en) | 2017-11-09 |
CN103153961A (zh) | 2013-06-12 |
AU2011277946B2 (en) | 2015-06-11 |
US20140155620A1 (en) | 2014-06-05 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
B25F | Entry of change of name and/or headquarter and transfer of application, patent and certif. of addition of invention: change of name on requirement |
Owner name: IRVITA PLANT PROTECTION, A BRANCH OF CELSIUS PROPE Free format text: A FIM DE ATENDER A ALTERACAO DE NOME E POSTERIOR TRANSFERENCIA DE TITULAR REQUERIDAS ATRAVES DA PETICAO NO 860150226036, DE 01/10/2015, E NECESSARIO APRESENTAR GUIA DE RECOLHIMENTO REFERENTE A ALTERACAO DE NOME OCORRIDA. |
|
B25D | Requested change of name of applicant approved |
Owner name: ADAMA CELSIUS B.V., CURACAO BRANCH (NL) |
|
B25A | Requested transfer of rights approved |
Owner name: ADAMA MAKHTESHIM LTD. (IL) |
|
B06F | Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette] | ||
B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
B06A | Patent application procedure suspended [chapter 6.1 patent gazette] | ||
B11B | Dismissal acc. art. 36, par 1 of ipl - no reply within 90 days to fullfil the necessary requirements |