BR112012033761A2 - processo para a fabricação de uma composição de graxa de complexo metálico, e, composição de graxa. - Google Patents

processo para a fabricação de uma composição de graxa de complexo metálico, e, composição de graxa.

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Publication number
BR112012033761A2
BR112012033761A2 BR112012033761A BR112012033761A BR112012033761A2 BR 112012033761 A2 BR112012033761 A2 BR 112012033761A2 BR 112012033761 A BR112012033761 A BR 112012033761A BR 112012033761 A BR112012033761 A BR 112012033761A BR 112012033761 A2 BR112012033761 A2 BR 112012033761A2
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BR
Brazil
Prior art keywords
grease composition
metal complex
water
sym
slurry
Prior art date
Application number
BR112012033761A
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English (en)
Inventor
Jean Luc Pierre André Brossaud
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Shell Int Research
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Publication date
Application filed by Shell Int Research filed Critical Shell Int Research
Publication of BR112012033761A2 publication Critical patent/BR112012033761A2/pt

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    • C10M129/00Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing oxygen
    • C10M129/02Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing oxygen having a carbon chain of less than 30 atoms
    • C10M129/26Carboxylic acids; Salts thereof
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    • C10M117/00Lubricating compositions characterised by the thickener being a non-macromolecular carboxylic acid or salt thereof
    • C10M117/02Lubricating compositions characterised by the thickener being a non-macromolecular carboxylic acid or salt thereof having only one carboxyl group bound to an acyclic carbon atom, cycloaliphatic carbon atom or hydrogen
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  • Chemical Kinetics & Catalysis (AREA)
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  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

processo para a fabricação de uma composição de graxa de complexo metálico,e,composição de graxa. processo para a fabricação de uma composição de graxa de complexo metálico que compreende as etapas de: (i) preparar uma psta fluida que compreende óleo de base, água, base metálica e agente complexador, em que a razão em peso de água: sólido na pasta fluida está na faixa de 0,15:1 a 1,5:1; (ii) aplicar corte a pasta fluida em uma frequência de corte de pelo menos 1.000.000 s<sym>; (iii) adicionar a pasta fluida que emerge da etapa (ii) a um ácido graxo saturado ou insaturado c<sym>c<sym> ou derivados deste para afetar a reação de saponificação, a reação de saponificação sendo realizada em uma temperatura de pelo menos 80ºc; (iv) remover água do prtoduto saponificado que resulta da etapa (iii) e (v) aquecer o produto que emerge da etapa (iv) em uma temperatura na faixa de 190 a 230ºc e (vi) esfriar o produto que emerge da etapa (v) a uma temperatura na faixa de 200 a 150ºc para formar uma composição de graxa de complexo metálico. o processo da presente invenção fornece uma redução no tempo de ventilação requerido para evaporar a água, uma redução no tempo de batelada total, um processo de fabricação mais eficiente em energia e um aumento na produtividade.
BR112012033761A 2010-07-05 2011-07-01 processo para a fabricação de uma composição de graxa de complexo metálico, e, composição de graxa. BR112012033761A2 (pt)

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JP5911857B2 (ja) 2016-04-27
EP2591080A1 (en) 2013-05-15
RU2564020C2 (ru) 2015-09-27
WO2012004198A1 (en) 2012-01-12
EP2591080B1 (en) 2014-11-26
RU2013104568A (ru) 2014-08-10
US9074156B2 (en) 2015-07-07
CN102971405B (zh) 2015-05-06
JP2013530289A (ja) 2013-07-25
CN102971405A (zh) 2013-03-13
US20130157907A1 (en) 2013-06-20

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