BR0014510A - Processo para produção de uma solução de ácido láctico purificada - Google Patents
Processo para produção de uma solução de ácido láctico purificadaInfo
- Publication number
- BR0014510A BR0014510A BR0014510-6A BR0014510A BR0014510A BR 0014510 A BR0014510 A BR 0014510A BR 0014510 A BR0014510 A BR 0014510A BR 0014510 A BR0014510 A BR 0014510A
- Authority
- BR
- Brazil
- Prior art keywords
- lactic acid
- solution
- amine
- extractor
- sulfuric acid
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/41—Preparation of salts of carboxylic acids
- C07C51/412—Preparation of salts of carboxylic acids by conversion of the acids, their salts, esters or anhydrides with the same carboxylic acid part
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Heterocyclic Compounds That Contain Two Or More Ring Oxygen Atoms (AREA)
Abstract
"PROCESSO PARA PRODUçãO DE UMA SOLUçãO DE áCIDO LáCTICO PURIFICADA". A presente revelação providencia um processo para o preparo de uma solução de ácido láctico purificada adequada para uso juntamente com uma fonte de material de lactato com um pH na faixa de 0,8 a 9,0. O processo inclui as etapas de providenciar uma fonte e material de lactato que inclui um sal de cálcio; acidular o caldo concentrado com ácido sulfúrico para formar uma solução acidulada que inclui ácido láctico e sulfato de cálcio; reduzir uma quantidade do sulfato de cálcio da solução acidulada; extrair a solução acidulada com um extrator contendo amina'para formar um solvente carregado; e extrair de volta o solvente carregado com um solvente aquoso para dar uma solução purificada de ácido láctico. opcionalmente, a fonte de material de lactato pode ser concentrada antes da etapa de acidulação. Alternativamente o extrator contendo amina pode incluir ânion sulfato. O ânion sulfúrico no extrator contendo amina pode ser ácido sulfúrico residual da etapa de acidulação. Alternativamente, o ácido sulfúrico no extrator contendo amina pode ser adicionado durante a etapa de extração, como ácido sulfúrico, por exemplo.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US09/412,085 US20020102672A1 (en) | 1999-10-04 | 1999-10-04 | Process for producing a purified lactic acid solution |
PCT/US2000/027200 WO2001025180A1 (en) | 1999-10-04 | 2000-10-03 | Process for producing a purified lactic acid solution |
Publications (1)
Publication Number | Publication Date |
---|---|
BR0014510A true BR0014510A (pt) | 2002-06-11 |
Family
ID=23631553
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR0014510-6A BR0014510A (pt) | 1999-10-04 | 2000-10-03 | Processo para produção de uma solução de ácido láctico purificada |
Country Status (10)
Country | Link |
---|---|
US (2) | US20020102672A1 (pt) |
EP (1) | EP1220828A1 (pt) |
JP (1) | JP2003511360A (pt) |
KR (1) | KR20020040833A (pt) |
CN (1) | CN1174953C (pt) |
AU (1) | AU1190601A (pt) |
BR (1) | BR0014510A (pt) |
HK (1) | HK1048985B (pt) |
WO (1) | WO2001025180A1 (pt) |
ZA (1) | ZA200203508B (pt) |
Families Citing this family (71)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
IT1294728B1 (it) | 1997-09-12 | 1999-04-12 | Biopolo S C A R L | Ceppi di lievito per la riproduzione di acido lattico |
US20020102672A1 (en) * | 1999-10-04 | 2002-08-01 | Joseph Mizrahi | Process for producing a purified lactic acid solution |
CA2414012A1 (en) * | 2000-05-30 | 2001-12-06 | Birgir Norddahl | Method for producing lactic acid |
AU2002211057A1 (en) * | 2000-09-15 | 2002-03-26 | Purac Biochem B.V. | Method for the purification of an alpha-hydroxy acid on an industrial scale |
US7838708B2 (en) | 2001-06-20 | 2010-11-23 | Grt, Inc. | Hydrocarbon conversion process improvements |
US6632966B2 (en) | 2001-08-24 | 2003-10-14 | Purac Biochem B.V. | Method for the preparation of lactic acid and calcium sulphate dihydrate |
ES2256509T3 (es) * | 2001-08-24 | 2006-07-16 | Purac Biochem B.V. | Metodo para la preparacion de acido lactico y dihidrato de sulfato de calcio. |
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US20050171393A1 (en) | 2003-07-15 | 2005-08-04 | Lorkovic Ivan M. | Hydrocarbon synthesis |
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US7507561B2 (en) * | 2004-05-20 | 2009-03-24 | Reliance Life Sciences Pvt. Ltd. | Process for the production of polylactic acid (PLA) from renewable feedstocks |
EP1929009A2 (en) | 2005-09-22 | 2008-06-11 | Tate & Lyle Ingredients Americas, Inc. | Improved strains for the production of organic acids |
CN101817720A (zh) | 2006-02-03 | 2010-09-01 | Grt公司 | 天然气转化为液体烃的连续方法 |
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CN101410526B (zh) * | 2006-03-29 | 2015-08-12 | 生物能源株式会社 | 来自乳酸发酵液的乳酸成分的分离方法和分离部件 |
CN101506371B (zh) * | 2006-07-05 | 2012-12-12 | 詹森药业有限公司 | 制备金属纳米颗粒的方法 |
WO2008071776A2 (en) * | 2006-12-13 | 2008-06-19 | Solvay | Production of cyclic diesters of alpha-hydroxyacids |
US20080254165A1 (en) * | 2007-04-12 | 2008-10-16 | Rashid Patel | Novel manufacturing process for milk acid |
US7998438B2 (en) | 2007-05-24 | 2011-08-16 | Grt, Inc. | Zone reactor incorporating reversible hydrogen halide capture and release |
CN101688224A (zh) | 2007-06-29 | 2010-03-31 | 东丽株式会社 | 乳酸的制造方法 |
DE102007045701B3 (de) * | 2007-09-24 | 2009-05-14 | Uhde Gmbh | Gewinnung von Milchsäure durch Fermentation und Extraktion mit Aminen |
GB0800081D0 (en) * | 2008-01-04 | 2008-02-13 | Univ Gent | Silver nanoparticles with specific surface area and/or isoelectric point and a method for producing them |
AU2009235066A1 (en) * | 2008-04-08 | 2009-10-15 | Hcl Cleantech Ltd. | A process for the recovery of HCl from a dilute solution thereof and extractant composition for use therein |
EP2133346A1 (fr) * | 2008-06-12 | 2009-12-16 | Ktanton Ltd | Procédé pour la fabrication d'un diester cyclique d'un acide alpha-hydroxylé |
US8282810B2 (en) | 2008-06-13 | 2012-10-09 | Marathon Gtf Technology, Ltd. | Bromine-based method and system for converting gaseous alkanes to liquid hydrocarbons using electrolysis for bromine recovery |
WO2010003534A1 (de) * | 2008-07-11 | 2010-01-14 | Uhde Gmbh | Isolierung von organischen säuren aus fermenterbrühe mit hilfe chromatographischer methoden |
AU2009270801B2 (en) | 2008-07-18 | 2014-04-24 | Reaction 35, Llc | Continuous process for converting natural gas to liquid hydrocarbons |
KR102237801B1 (ko) * | 2009-06-04 | 2021-04-07 | 게노마티카 인코포레이티드 | 발효액 성분들의 분리 방법 |
CN101967091A (zh) * | 2009-07-28 | 2011-02-09 | 凯发知识产权资源私人有限公司 | 用于有机酸提纯的方法 |
CA2778818A1 (en) * | 2009-10-26 | 2011-05-05 | University Of Maine System Board Of Trustees | Production of lactic acid from hemicellulose extracts |
US8367884B2 (en) | 2010-03-02 | 2013-02-05 | Marathon Gtf Technology, Ltd. | Processes and systems for the staged synthesis of alkyl bromides |
US8198495B2 (en) | 2010-03-02 | 2012-06-12 | Marathon Gtf Technology, Ltd. | Processes and systems for the staged synthesis of alkyl bromides |
JP5679411B2 (ja) * | 2010-06-17 | 2015-03-04 | 日立造船株式会社 | ポリ乳酸の製造方法 |
IL207329A0 (en) | 2010-08-01 | 2010-12-30 | Robert Jansen | A method for refining a recycle extractant and for processing a lignocellulosic material and for the production of a carbohydrate composition |
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BR112013010169B1 (pt) | 2010-10-28 | 2021-11-16 | Total Raffinage Marketing | Microrganismo monascus ruber, seu uso na produção de ácido láctico e método para produzir uma composição a um rendimento elevado, que compreende um ácido láctico |
JPWO2012081112A1 (ja) * | 2010-12-16 | 2014-05-22 | 株式会社日立製作所 | 精製乳酸溶液の製造方法 |
JP2012162471A (ja) * | 2011-02-04 | 2012-08-30 | Nippon Shokubai Co Ltd | アクリル酸およびその重合体の製造方法 |
US8815050B2 (en) | 2011-03-22 | 2014-08-26 | Marathon Gtf Technology, Ltd. | Processes and systems for drying liquid bromine |
US8436220B2 (en) | 2011-06-10 | 2013-05-07 | Marathon Gtf Technology, Ltd. | Processes and systems for demethanization of brominated hydrocarbons |
US8829256B2 (en) | 2011-06-30 | 2014-09-09 | Gtc Technology Us, Llc | Processes and systems for fractionation of brominated hydrocarbons in the conversion of natural gas to liquid hydrocarbons |
JP2013043860A (ja) | 2011-08-24 | 2013-03-04 | Hitachi Plant Technologies Ltd | 精製乳酸の製造方法 |
US9228243B2 (en) | 2011-08-24 | 2016-01-05 | Red Shield Acquistion, LLC | System and method for conditioning a hardwood pulp liquid hydrolysate |
US8802908B2 (en) | 2011-10-21 | 2014-08-12 | Marathon Gtf Technology, Ltd. | Processes and systems for separate, parallel methane and higher alkanes' bromination |
US9193641B2 (en) | 2011-12-16 | 2015-11-24 | Gtc Technology Us, Llc | Processes and systems for conversion of alkyl bromides to higher molecular weight hydrocarbons in circulating catalyst reactor-regenerator systems |
WO2013109143A1 (en) * | 2012-01-18 | 2013-07-25 | Stichting Public Private Partnership Institute For Sustainable Process Technology | Extraction of carboxylic acids from a dilute aqueous stream |
WO2013192451A1 (en) * | 2012-06-20 | 2013-12-27 | Opx Biotechnologies, Inc. | Dehydration of 3-hydroxypropionic acid to acrylic acid |
SG11201501013PA (en) | 2012-08-10 | 2015-04-29 | Opx Biotechnologies Inc | Microorganisms and methods for the production of fatty acids and fatty acid derived products |
NZ706072A (en) | 2013-03-08 | 2018-12-21 | Xyleco Inc | Equipment protecting enclosures |
WO2014146026A1 (en) | 2013-03-15 | 2014-09-18 | Opx Biotechnologies, Inc. | Bioproduction of chemicals |
BR112016001026A2 (pt) | 2013-07-19 | 2017-10-24 | Cargill Inc | organismo geneticamente modificado |
US11408013B2 (en) | 2013-07-19 | 2022-08-09 | Cargill, Incorporated | Microorganisms and methods for the production of fatty acids and fatty acid derived products |
GB201315929D0 (en) * | 2013-09-06 | 2013-10-23 | Plaxica Ltd | Lactate production process |
EP2993228B1 (en) | 2014-09-02 | 2019-10-09 | Cargill, Incorporated | Production of fatty acid esters |
CN105693503A (zh) * | 2016-03-15 | 2016-06-22 | 滨州市华康梦之缘生物科技有限公司 | 一种提取高光学纯度d-乳酸的方法 |
CN106244638B (zh) * | 2016-07-29 | 2020-01-07 | 河南金丹乳酸科技股份有限公司 | 一种生物质循环发酵生产乳酸的综合利用工艺 |
WO2018089971A1 (en) * | 2016-11-14 | 2018-05-17 | Lygos, Inc. | Process for purification of malonic acid from fermentation broth |
JP2020506702A (ja) | 2017-02-02 | 2020-03-05 | カーギル インコーポレイテッド | C6−c10脂肪酸誘導体を生成する遺伝子組み換え細胞 |
CN107857700B (zh) * | 2017-12-11 | 2022-04-12 | 南京大学扬州化学化工研究院 | 一种1,2-丙二醇氧化制乳酸的产物分离工艺 |
CN109503352A (zh) * | 2018-12-04 | 2019-03-22 | 桂林理工大学 | 一种从乙酸盐溶液中回收乙酸和分离其他元素的方法 |
JP2023524744A (ja) * | 2020-05-04 | 2023-06-13 | 大塚製薬株式会社 | 無水乳酸を合成する方法 |
CN114014836B (zh) * | 2021-12-16 | 2022-12-02 | 内蒙古久泰新材料有限公司 | 环状交酯的纯化方法 |
CN114380683A (zh) * | 2021-12-21 | 2022-04-22 | 安徽丰原发酵技术工程研究有限公司 | 一种从含乳酸钙的发酵液中提取乳酸的方法 |
CN114591164B (zh) * | 2022-01-29 | 2023-11-24 | 安徽丰原发酵技术工程研究有限公司 | 一种乳酸的纯化方法 |
CN114409529A (zh) * | 2022-01-30 | 2022-04-29 | 安徽丰原发酵技术工程研究有限公司 | 一种从乳酸聚合物中回收乳酸的方法 |
Family Cites Families (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US1906068A (en) * | 1931-03-02 | 1933-04-25 | Grasselli Chemical Co | Lactic acid |
US2712516A (en) * | 1950-06-17 | 1955-07-05 | Corn Prod Refining Co | Method of treating steep liquor |
IL39710A (en) * | 1972-06-19 | 1975-04-25 | Imi Inst For Res & Dev | Recovery of acids from aqueous solutions by solvent extraction |
IL57024A (en) * | 1979-04-09 | 1982-03-31 | Yissum Appl Eng Syst | Process for the separation of a strong mineral acid from an aqueous solution |
US4334095A (en) * | 1980-10-06 | 1982-06-08 | Miles Laboratories, Inc. | Extraction of organic acids from aqueous solutions |
US4771001A (en) * | 1986-03-27 | 1988-09-13 | Neurex Corp. | Production of lactic acid by continuous fermentation using an inexpensive raw material and a simplified method of lactic acid purification |
AT398982B (de) * | 1993-02-18 | 1995-02-27 | Vogelbusch Gmbh | Verfahren zur abtrennung und reinigung von milchsäure |
US5510526A (en) * | 1993-06-29 | 1996-04-23 | Cargill, Incorporated | Lactic acid production, separation and/or recovery process |
US5426219A (en) * | 1993-07-26 | 1995-06-20 | A.E. Staley Manufacturing Co. | Process for recovering organic acids |
IL109003A (en) | 1994-03-16 | 1999-09-22 | Yissum Res Dev Co | Process and extractant composition for extracting water-soluble carboxylic and mineral acids |
IL109724A (en) * | 1994-05-23 | 1999-11-30 | Innova Sa | Recovery of carboxylic acid from organic solution that contains an amine and an extraction enhancer |
IL110206A (en) * | 1994-07-04 | 1996-10-16 | Innova Sa | Recovery of carboxylic acid from organic solution that contains an amine and an extraction enhancer |
US5814498A (en) * | 1996-04-29 | 1998-09-29 | Archer Daniels Midland Company | Process for the recovery of organic acids and ammonia from their salts |
IL119387A (en) * | 1996-10-09 | 2001-06-14 | Cargill Inc | Process for the recovery of lactic acid by liquid-liquid extraction with a basic extractant |
US5766439A (en) * | 1996-10-10 | 1998-06-16 | A. E. Staley Manufacturing Co. | Production and recovery of organic acids |
BE1011197A3 (fr) | 1997-06-06 | 1999-06-01 | Brussels Biotech En Abrege Bb | Procede de purification d'acide lactique. |
US6229046B1 (en) * | 1997-10-14 | 2001-05-08 | Cargill, Incorported | Lactic acid processing methods arrangements and products |
US20020102672A1 (en) * | 1999-10-04 | 2002-08-01 | Joseph Mizrahi | Process for producing a purified lactic acid solution |
-
1999
- 1999-10-04 US US09/412,085 patent/US20020102672A1/en not_active Abandoned
-
2000
- 2000-10-03 BR BR0014510-6A patent/BR0014510A/pt not_active IP Right Cessation
- 2000-10-03 AU AU11906/01A patent/AU1190601A/en not_active Abandoned
- 2000-10-03 JP JP2001528130A patent/JP2003511360A/ja active Pending
- 2000-10-03 EP EP00973399A patent/EP1220828A1/en not_active Withdrawn
- 2000-10-03 WO PCT/US2000/027200 patent/WO2001025180A1/en active Application Filing
- 2000-10-03 CN CNB008137102A patent/CN1174953C/zh not_active Expired - Fee Related
- 2000-10-03 KR KR1020027004319A patent/KR20020040833A/ko not_active Application Discontinuation
-
2002
- 2002-05-03 ZA ZA200203508A patent/ZA200203508B/xx unknown
- 2002-06-04 US US10/162,935 patent/US7026145B2/en not_active Expired - Fee Related
-
2003
- 2003-02-18 HK HK03101166.3A patent/HK1048985B/zh not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
US20030004375A1 (en) | 2003-01-02 |
US7026145B2 (en) | 2006-04-11 |
AU1190601A (en) | 2001-05-10 |
US20020102672A1 (en) | 2002-08-01 |
ZA200203508B (en) | 2003-07-30 |
HK1048985B (zh) | 2005-09-02 |
CN1174953C (zh) | 2004-11-10 |
KR20020040833A (ko) | 2002-05-30 |
EP1220828A1 (en) | 2002-07-10 |
CN1377335A (zh) | 2002-10-30 |
WO2001025180A1 (en) | 2001-04-12 |
HK1048985A1 (en) | 2003-04-25 |
JP2003511360A (ja) | 2003-03-25 |
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Legal Events
Date | Code | Title | Description |
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B25G | Requested change of headquarter approved | ||
B08F | Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette] |
Free format text: REFERENTE A 9A ANUIDA DE. |
|
B08K | Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette] |
Free format text: REFERENTE AO DESPACHO 8.6 PUBLICADO NA RPI 2051 DE 27/04/2010. |