BR0009413A - Processos para a preparação de sais den-alquilamonioacetonitrila granulares, e para apreparação de hidrogeno sulfato dfn-metilmorfolinoacetonitrila granular - Google Patents
Processos para a preparação de sais den-alquilamonioacetonitrila granulares, e para apreparação de hidrogeno sulfato dfn-metilmorfolinoacetonitrila granularInfo
- Publication number
- BR0009413A BR0009413A BR0009413-7A BR0009413A BR0009413A BR 0009413 A BR0009413 A BR 0009413A BR 0009413 A BR0009413 A BR 0009413A BR 0009413 A BR0009413 A BR 0009413A
- Authority
- BR
- Brazil
- Prior art keywords
- preparation
- granular
- den
- salts
- hydrogen sulfate
- Prior art date
Links
- 238000002360 preparation method Methods 0.000 title abstract 5
- QAOWNCQODCNURD-UHFFFAOYSA-M hydrogensulfate Chemical compound OS([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-M 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 3
- 150000003839 salts Chemical class 0.000 title abstract 2
- 239000007864 aqueous solution Substances 0.000 abstract 2
- 230000008020 evaporation Effects 0.000 abstract 2
- 238000001704 evaporation Methods 0.000 abstract 2
- 230000008018 melting Effects 0.000 abstract 2
- 238000002844 melting Methods 0.000 abstract 2
- HTSGKJQDMSTCGS-UHFFFAOYSA-N 1,4-bis(4-chlorophenyl)-2-(4-methylphenyl)sulfonylbutane-1,4-dione Chemical compound C1=CC(C)=CC=C1S(=O)(=O)C(C(=O)C=1C=CC(Cl)=CC=1)CC(=O)C1=CC=C(Cl)C=C1 HTSGKJQDMSTCGS-UHFFFAOYSA-N 0.000 abstract 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 239000012876 carrier material Substances 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C253/00—Preparation of carboxylic acid nitriles
- C07C253/30—Preparation of carboxylic acid nitriles by reactions not involving the formation of cyano groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
- C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
- C07D295/14—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals
- C07D295/145—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals with the ring nitrogen atoms and the carbon atoms with three bonds to hetero atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings
- C07D295/15—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals with the ring nitrogen atoms and the carbon atoms with three bonds to hetero atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings to an acyclic saturated chain
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
"PROCESSOS PARA A PREPARAçãO DE SAIS DEN-ALQUILAMONIOACETONITRILA GRANULARES, E PARA APREPARAçãO DE HIDROGêNO SULFATO DEN-METILMORFOLINOACETONITRILA GRANULAR". A invençãodiz respeito a um processo melhorado para a preparação de saisde N-alquilamónioacetonitrila granulares I R^ 2^R^ 3^N^ +^R^1^-CR^ 4^R^ 5^-CN Y^ -^ (I) em que R^ 1^ a R^ 5^ sãohidrogênio ou radicais orgânicos e Y^ -^ é um ânion de sulfato oude hidrogeno sulfato, de uma solução aquosa do composto II R^2^R^ 3^N^ +^R^ 1^-CR^ 4^R^ 5^-CN R^ 6^O-SO~ 2~-O (II)onde R^ 6^ é alquila C~ 1~ a C~ 4~, que compreendeevaporação dessa solução aquosa a uma temperatura dentre 80 e250<198> C e uma pressão dentre 10 mbar e 2 bar para obter umamassa em fusão e então deixar a massa em fusão solidificar-se,onde durante ou após a evaporação, materiais veículos usuaise/ou auxiliares podem ser adicionados, e o composto solidificadoresultante (I) é convertido para a forma granular desejada.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19913995A DE19913995A1 (de) | 1999-03-29 | 1999-03-29 | Verfahren zur Herstellung von körnigen N-Alkylamoniumacetonitril-Salzen |
| PCT/EP2000/002378 WO2000058273A1 (de) | 1999-03-29 | 2000-03-17 | Verfahren zur herstellung von körnigen n-alkylammoniumacetonitril-salzen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BR0009413A true BR0009413A (pt) | 2001-12-26 |
Family
ID=7902675
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BR0009413-7A BR0009413A (pt) | 1999-03-29 | 2000-03-17 | Processos para a preparação de sais den-alquilamonioacetonitrila granulares, e para apreparação de hidrogeno sulfato dfn-metilmorfolinoacetonitrila granular |
Country Status (17)
| Country | Link |
|---|---|
| US (1) | US6593473B1 (pt) |
| EP (1) | EP1165497B1 (pt) |
| JP (1) | JP2002540187A (pt) |
| KR (1) | KR20010104728A (pt) |
| CN (1) | CN1157369C (pt) |
| AT (1) | ATE260244T1 (pt) |
| AU (1) | AU770647B2 (pt) |
| BR (1) | BR0009413A (pt) |
| CA (1) | CA2368481A1 (pt) |
| CZ (1) | CZ20013452A3 (pt) |
| DE (2) | DE19913995A1 (pt) |
| ES (1) | ES2215620T3 (pt) |
| HU (1) | HUP0200282A3 (pt) |
| ID (1) | ID30453A (pt) |
| PL (1) | PL350827A1 (pt) |
| TR (1) | TR200102806T2 (pt) |
| WO (1) | WO2000058273A1 (pt) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10121051A1 (de) | 2001-04-28 | 2002-10-31 | Clariant Gmbh | Builder-Zusammensetzung |
| DE10161766A1 (de) * | 2001-12-15 | 2003-06-26 | Clariant Gmbh | Bleichaktivator-Co-Granulate |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4213924A (en) * | 1978-06-19 | 1980-07-22 | Tennessee Valley Authority | Granulation and coating by improved method of heat removal |
| GB8329880D0 (en) | 1983-11-09 | 1983-12-14 | Unilever Plc | Particulate adjuncts |
| DE3835918A1 (de) * | 1988-10-21 | 1990-04-26 | Henkel Kgaa | Verfahren zur herstellung von tensidhaltigen granulaten |
| US5888419A (en) * | 1995-06-07 | 1999-03-30 | The Clorox Company | Granular N-alkyl ammonium acetontrile compositions |
| CA2264297A1 (en) | 1996-08-30 | 1998-03-05 | Chuan Shih | Pharmaceutical compounds |
| ATE259791T1 (de) * | 1996-11-29 | 2004-03-15 | Clorox Co | N-alkyl-ammonium-acetonitril-salze, methoden dazu und zusammensetzungen die diese enthalten |
| DE19740669A1 (de) * | 1997-09-16 | 1999-03-18 | Clariant Gmbh | Gecoatete Ammoniumnitril-Bleichaktivatorgranulate |
| DE19740671A1 (de) * | 1997-09-16 | 1999-03-18 | Clariant Gmbh | Bleichaktivator-Granulate |
-
1999
- 1999-03-29 DE DE19913995A patent/DE19913995A1/de not_active Withdrawn
-
2000
- 2000-03-17 KR KR1020017012176A patent/KR20010104728A/ko not_active Application Discontinuation
- 2000-03-17 TR TR2001/02806T patent/TR200102806T2/xx unknown
- 2000-03-17 DE DE50005416T patent/DE50005416D1/de not_active Expired - Fee Related
- 2000-03-17 CZ CZ20013452A patent/CZ20013452A3/cs unknown
- 2000-03-17 CA CA002368481A patent/CA2368481A1/en not_active Abandoned
- 2000-03-17 ID IDW00200102349A patent/ID30453A/id unknown
- 2000-03-17 AU AU34300/00A patent/AU770647B2/en not_active Ceased
- 2000-03-17 EP EP00912618A patent/EP1165497B1/de not_active Expired - Lifetime
- 2000-03-17 JP JP2000607976A patent/JP2002540187A/ja not_active Withdrawn
- 2000-03-17 WO PCT/EP2000/002378 patent/WO2000058273A1/de not_active Application Discontinuation
- 2000-03-17 PL PL00350827A patent/PL350827A1/xx not_active Application Discontinuation
- 2000-03-17 ES ES00912618T patent/ES2215620T3/es not_active Expired - Lifetime
- 2000-03-17 AT AT00912618T patent/ATE260244T1/de not_active IP Right Cessation
- 2000-03-17 BR BR0009413-7A patent/BR0009413A/pt not_active IP Right Cessation
- 2000-03-17 CN CNB008055963A patent/CN1157369C/zh not_active Expired - Fee Related
- 2000-03-17 HU HU0200282A patent/HUP0200282A3/hu unknown
- 2000-03-17 US US09/926,216 patent/US6593473B1/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| EP1165497B1 (de) | 2004-02-25 |
| DE50005416D1 (de) | 2004-04-01 |
| TR200102806T2 (tr) | 2002-04-22 |
| AU3430000A (en) | 2000-10-16 |
| ATE260244T1 (de) | 2004-03-15 |
| AU770647B2 (en) | 2004-02-26 |
| DE19913995A1 (de) | 2000-10-05 |
| JP2002540187A (ja) | 2002-11-26 |
| KR20010104728A (ko) | 2001-11-26 |
| ID30453A (id) | 2001-12-06 |
| CN1345305A (zh) | 2002-04-17 |
| PL350827A1 (en) | 2003-02-10 |
| CN1157369C (zh) | 2004-07-14 |
| HUP0200282A3 (en) | 2003-03-28 |
| CZ20013452A3 (cs) | 2002-01-16 |
| CA2368481A1 (en) | 2000-10-05 |
| US6593473B1 (en) | 2003-07-15 |
| HUP0200282A2 (hu) | 2002-07-29 |
| EP1165497A1 (de) | 2002-01-02 |
| WO2000058273A1 (de) | 2000-10-05 |
| ES2215620T3 (es) | 2004-10-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B08F | Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette] |
Free format text: REFERENTE A 3A, 6A E 7A ANUIDADES. |
|
| B08K | Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette] |
Free format text: REFERENTE AO DESPACHO 8.6 PUBLICADO NA RPI 1925 DE 27/11/2007. |