AU562078B2 - Preparation of 2-hydroxy-4-methyl timobutyric acid - Google Patents

Preparation of 2-hydroxy-4-methyl timobutyric acid

Info

Publication number
AU562078B2
AU562078B2 AU35359/84A AU3535984A AU562078B2 AU 562078 B2 AU562078 B2 AU 562078B2 AU 35359/84 A AU35359/84 A AU 35359/84A AU 3535984 A AU3535984 A AU 3535984A AU 562078 B2 AU562078 B2 AU 562078B2
Authority
AU
Australia
Prior art keywords
hydroxy
acid
weight
preparation
hydrolyzate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
AU35359/84A
Other languages
English (en)
Other versions
AU3535984A (en
Inventor
Dennis Arthur Ruest
Masaharu Takano
Lawrence Russell Wolf
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Novus International Inc
Original Assignee
Monsanto Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Monsanto Co filed Critical Monsanto Co
Publication of AU3535984A publication Critical patent/AU3535984A/en
Application granted granted Critical
Publication of AU562078B2 publication Critical patent/AU562078B2/en
Assigned to NOVUS INTERNATIONAL INC reassignment NOVUS INTERNATIONAL INC Alteration of Name(s) in Register under S187 Assignors: MONSANTO COMPANY
Anticipated expiration legal-status Critical
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/26—Separation; Purification; Stabilisation; Use of additives
    • C07C319/28—Separation; Purification
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23K—FODDER
    • A23K20/00—Accessory food factors for animal feeding-stuffs
    • A23K20/10—Organic substances
    • A23K20/105—Aliphatic or alicyclic compounds
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23K—FODDER
    • A23K20/00—Accessory food factors for animal feeding-stuffs
    • A23K20/10—Organic substances
    • A23K20/142—Amino acids; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23K—FODDER
    • A23K50/00—Feeding-stuffs specially adapted for particular animals
    • A23K50/70—Feeding-stuffs specially adapted for particular animals for birds
    • A23K50/75—Feeding-stuffs specially adapted for particular animals for birds for poultry
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/14—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
    • C07C319/20—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides by reactions not involving the formation of sulfide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
    • C07C323/50—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton
    • C07C323/51—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton
    • C07C323/52—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being acyclic and saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Zoology (AREA)
  • Animal Husbandry (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Birds (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Fodder In General (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
AU35359/84A 1983-11-14 1984-11-13 Preparation of 2-hydroxy-4-methyl timobutyric acid Expired AU562078B2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US550857 1983-11-14
US06/550,857 US4524077A (en) 1983-11-14 1983-11-14 Liquid 2-hydroxy-4-methylthiobutyric acid and process for the preparation thereof

Publications (2)

Publication Number Publication Date
AU3535984A AU3535984A (en) 1985-05-23
AU562078B2 true AU562078B2 (en) 1987-05-28

Family

ID=24198852

Family Applications (1)

Application Number Title Priority Date Filing Date
AU35359/84A Expired AU562078B2 (en) 1983-11-14 1984-11-13 Preparation of 2-hydroxy-4-methyl timobutyric acid

Country Status (13)

Country Link
US (1) US4524077A (cg-RX-API-DMAC7.html)
EP (1) EP0142488B1 (cg-RX-API-DMAC7.html)
JP (2) JPS60156396A (cg-RX-API-DMAC7.html)
KR (1) KR870000657B1 (cg-RX-API-DMAC7.html)
AT (1) ATE29131T1 (cg-RX-API-DMAC7.html)
AU (1) AU562078B2 (cg-RX-API-DMAC7.html)
CA (1) CA1263668A (cg-RX-API-DMAC7.html)
DE (1) DE3465592D1 (cg-RX-API-DMAC7.html)
GB (1) GB2149791B (cg-RX-API-DMAC7.html)
GE (1) GEP19960463B (cg-RX-API-DMAC7.html)
MX (1) MX163989B (cg-RX-API-DMAC7.html)
SU (1) SU1428193A3 (cg-RX-API-DMAC7.html)
ZA (1) ZA848847B (cg-RX-API-DMAC7.html)

Families Citing this family (41)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2005784A6 (es) * 1988-02-22 1989-03-16 Desarrollo Tecnico Ind S A Soc Un procedimiento para preparar soluciones acuosas de acido 2-hidroxi-4-metil-tiobutirico.
MY109603A (en) * 1992-05-21 1997-03-31 Daicel Chem Process for producing 2-hydroxy-4-methylthiobutanoic acid
US5498790A (en) * 1993-06-09 1996-03-12 Novus International, Inc. Regeneration of sulfuric acid from sulfate by-products of 2-hydroxy-4-(methylthio)butyric acid manufacture
RU2130925C1 (ru) * 1994-07-11 1999-05-27 Дегусса Акциенгезельшафт Способ получения 2-гидрокси-4-метилтиомасляной кислоты (гидроксианалогаметионина, гам), гам
DE4428608C1 (de) * 1994-08-12 1996-02-29 Degussa Verfahren zur Gewinnung von 2-Hydroxy-4-methylthiobuttersäure (MHA)
US5856567A (en) * 1995-06-07 1999-01-05 Novus International, Inc. Continuous hydrolysis process for preparing 2-hydroxy-4-methylthiobutanioc acid or salts thereof
CN1094925C (zh) * 1995-06-07 2002-11-27 诺沃斯国际公司 制备2－羟基－4－甲基硫代丁酸或其盐的连续水解法
DE19548538C2 (de) * 1995-12-23 1997-12-18 Degussa Verfahren zur Gewinnung von 2-Hydroxy-4-methylthiobuttersäure (MHA)
DE19654485A1 (de) * 1996-12-27 1998-07-02 Degussa Verfahren zur Gewinnung von lagerstabiler 2-Hydroxy-4-methylthiobuttersäure (MHA)
RU2184111C2 (ru) * 1997-03-04 2002-06-27 Сумитомо Кемикал Компани, Лимитед Способ получения 2-гидрокси-4-метилтиобутановой кислоты
JP3804210B2 (ja) * 1997-03-04 2006-08-02 住友化学株式会社 ２−ヒドロキシ−４−メチルチオブタン酸の製造方法
US6017563A (en) * 1997-07-25 2000-01-25 Novus International, Inc. Process for optimizing milk production
FR2780969B1 (fr) * 1998-07-10 2000-08-18 Rhone Poulenc Nutrition Animal Procede de separation de l'acide hydroxymethylthiobutyrique
FR2780968B1 (fr) * 1998-07-10 2000-08-18 Rhone Poulenc Nutrition Animal Procede de preparation de l'acide hydroxymethylthiobutyrique
FR2791673B1 (fr) 1999-04-02 2001-06-08 Rhone Poulenc Animal Nutrition Procede de preparation des esters de l'acide hydroxymethylthiobutyrique
US6342651B1 (en) 1999-08-05 2002-01-29 Novus International, Inc. Reductive combustion of ammonium salts of sulfuric acid
US6649794B2 (en) * 2000-02-18 2003-11-18 Sumitomo Chemical Company, Limited Method for producing 2-Hydroxy-4-Methylthiobutanoic Acid
TWI296652B (en) * 2000-03-29 2008-05-11 Mitsui Chemicals Inc Production process of amide compound
JP4517474B2 (ja) * 2000-07-25 2010-08-04 住友化学株式会社 ２−ヒドロキシ−４−メチルチオブタン酸の製造方法
JP4517486B2 (ja) * 2000-09-25 2010-08-04 住友化学株式会社 ２−ヒドロキシ−４−メチルチオブタンニトリルの製造方法
JP4517520B2 (ja) * 2001-02-27 2010-08-04 住友化学株式会社 ２−ヒドロキシ−４−メチルチオブタン酸の製造方法
DE10316110A1 (de) * 2003-04-09 2004-10-28 Degussa Ag Verfahren zur Herstellung von 2-Hydroxy-4-methylthio-buttersäure Ammoniumsalz
FR2871028B1 (fr) * 2004-06-08 2006-12-29 Adisseo Ireland Ltd Complement alimentaire pour animaux, comprenant un additif olfactif
JP4696496B2 (ja) 2004-08-18 2011-06-08 住友化学株式会社 ２−ヒドロキシ−４−メチルチオ酪酸の製造方法
EP1801227B1 (en) * 2004-10-14 2009-04-15 Sumitomo Chemical Company, Limited Method for producing 2-hydroxy-4-(methylthio)butanoic acid
DE102005050106B4 (de) * 2005-10-18 2008-04-30 Josef Meissner Gmbh & Co. Kg Rückgewinnung von Nitriersäuregemischen aus Nitrienprozessen
ES2279719B1 (es) * 2006-01-26 2008-07-16 Timac Agro España, S.A. Nuevo activador metabolico y nutricional para las plantas.
WO2008010609A1 (en) 2006-07-21 2008-01-24 Sumitomo Chemical Company, Limited Process for producing 2-hydroxy-4-(methylthio)butyrate compounds and intermediates thereof
DE102007062199A1 (de) * 2007-12-21 2009-06-25 Evonik Degussa Gmbh 2-Methylthioethyl-substituierte Heterocyclen als Futtermitteladditive
JP2009161499A (ja) * 2008-01-10 2009-07-23 Sumitomo Chemical Co Ltd ２−ヒドロキシ−４−メチルチオブタンアミドの製造方法
FR2938535B1 (fr) 2008-11-20 2012-08-17 Arkema France Procede de fabrication de methylmercaptopropionaldehyde et de methionine a partir de matieres renouvelables
FR2939791B1 (fr) * 2008-12-16 2011-01-14 Adisseo France Sas Procede de preparation d'acroleine a partir de glycerol ou de glycerine brute
CN103429748B (zh) 2010-12-30 2016-01-06 代谢探索者公司 甲硫氨酸羟基类似物(mha)的发酵产生
WO2013119959A1 (en) 2012-02-09 2013-08-15 Novus International Inc. Heteroatom containing cyclic dimers
KR101419118B1 (ko) * 2012-07-11 2014-07-11 김건희 사료용 향료 조성물
EP3388056A1 (en) 2012-07-12 2018-10-17 Novus International Inc. Matrix and layer compositions for protection of bioactives
WO2015126779A1 (en) * 2014-02-20 2015-08-27 Flsmidth A/S Column settler for high performance liquid/liquid phase separations in hydromellurcial processes and methods thereof
CN104860855B (zh) * 2014-12-08 2017-06-16 宁夏紫光天化蛋氨酸有限责任公司 一种高纯度的d,l‑2‑羟基‑4‑甲硫基丁酸酯的制备方法
MY198309A (en) * 2016-06-24 2023-08-22 Novus Int Inc Hydroxy methionine analog formulations suibtable for specialty chemical applications
FR3064006B1 (fr) 2017-03-16 2019-03-29 Adisseo France S.A.S. Procede de fabrication de l'acide-2-hydroxy-4-methylthio-butyrique
US10584306B2 (en) 2017-08-11 2020-03-10 Board Of Regents Of The University Of Oklahoma Surfactant microemulsions

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB722024A (en) * 1950-10-31 1955-01-19 Monsanto Chemicals Production of alpha-hydroxy-gamma-mercapto-carboxylic acids and salts thereof and compositions containing the same
US2745745A (en) * 1952-10-30 1956-05-15 Monsanto Chemicals Poultry feed
US2938053A (en) * 1955-12-29 1960-05-24 Monsanto Chemicals Amino acid analogues
CH385823A (de) * 1959-09-01 1964-12-31 Inventa Ag Verfahren zur Herstellung des Calciumsalzes der a-Oxy-y-methylthio-buttersäure
BE611435A (fr) * 1960-12-14 1962-06-12 Stamicarbon Procédé de préparation de sels métalliques d'acide alpha-hydroxy- gamma -méthylmercaptobutyrique
US3773927A (en) * 1971-12-20 1973-11-20 Du Pont Preparation of an aqueous slurry of ammonium chloride and methylmercapto-hydroxybutyric acid
US4310690A (en) * 1980-10-08 1982-01-12 E. I. Du Pont De Nemours And Company Preparation of the calcium salt of α-hydroxy-gamma-methylmercaptobutyric acid

Also Published As

Publication number Publication date
EP0142488B1 (en) 1987-08-26
KR850004108A (ko) 1985-07-01
JPH05211846A (ja) 1993-08-24
EP0142488A2 (en) 1985-05-22
JPH0797970B2 (ja) 1995-10-25
US4524077A (en) 1985-06-18
GB2149791A (en) 1985-06-19
CA1263668C (en) 1989-12-05
KR870000657B1 (ko) 1987-04-04
SU1428193A3 (ru) 1988-09-30
MX163989B (es) 1992-07-07
AU3535984A (en) 1985-05-23
CA1263668A (en) 1989-12-05
EP0142488A3 (en) 1985-06-26
JPH051787B2 (cg-RX-API-DMAC7.html) 1993-01-11
GB2149791B (en) 1988-04-20
ATE29131T1 (de) 1987-09-15
JPS60156396A (ja) 1985-08-16
GB8428657D0 (en) 1984-12-19
DE3465592D1 (en) 1987-10-01
ZA848847B (en) 1985-09-25
GEP19960463B (en) 1996-07-15

Similar Documents

Publication Publication Date Title
AU562078B2 (en) Preparation of 2-hydroxy-4-methyl timobutyric acid
AU6414386A (en) Method of separation of sugars and concentrated sulfuric acid
GB1458705A (en) Process for separating acrylic acid from aqueous solutions
GB1477860A (en) Separation of wool fatty acid from wool alcohol or wool wax
ATE108441T1 (de) Verfahren zur herstellung von chinolin-3- karbonsäure als bakterienfeindliche wirkstoffe.
DE3684434D1 (de) Verfahren zur herstellung von 2-keto-d-glukarsaeure.
KR890008031A (ko) 이산화티탄 분말의 제조방법
IE821414L (en) Preparation of blood cell protein and haem
CA2115229A1 (en) Process for preparing a low fat, transparent, stable oat protein containing aqueous solution and product thereof
ES479759A1 (es) Un procedimiento para la preparacion de acido 7-metoxi-5-oxo-5h-tiazolo 2,3,-d quinazolin-2-carboxilico.
JPS5571701A (en) Hydrolyzate polysaccharide, its preparation, and immunoregulator containing hydrolyzate polysaccharide as active ingredient
CA2031165A1 (en) Recovery of cobalt catalyst values
ATE73858T1 (de) Verfahren zur herstellung von xylose.
GB1527557A (en) Process for preparing solid sodium amoxycillin
FR2321451A1 (fr) Procede de preparation d'hydrate d'hydrazine
IE40576B1 (en) Purified phosphoric acid and its production
GB1167274A (en) Process for the Production of Cyclic Carboxylic Acids
JPS5247988A (en) Method of producing l-tartaric acid
EP0216696A3 (en) Process for preparing cotarnine
JPS5738312A (en) Manufacture of hydrazine
GB1381418A (en) Recovery of ammonium salts of organic acids
ATE38378T1 (de) Verfahren zur herstellung von n-acetyl-paminophenol.
JPS5534207A (en) Preparation of carboxymethyl starch and its alkali salt
JPS542398A (en) Preparation of d-alpha-amino acid
JPS6416593A (en) Production of castor oil fatty acid