AU2010280923B2 - Process for the preparation of pyrazole carboxylic acid amides - Google Patents

Process for the preparation of pyrazole carboxylic acid amides Download PDF

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Publication number
AU2010280923B2
AU2010280923B2 AU2010280923A AU2010280923A AU2010280923B2 AU 2010280923 B2 AU2010280923 B2 AU 2010280923B2 AU 2010280923 A AU2010280923 A AU 2010280923A AU 2010280923 A AU2010280923 A AU 2010280923A AU 2010280923 B2 AU2010280923 B2 AU 2010280923B2
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AU
Australia
Prior art keywords
compound
formula
viii
reacting
reaction
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AU2010280923A
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AU2010280923A1 (en
Inventor
Fanny Giordano
Denis Gribkov
Martin Lagger
Adrian Muller
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Syngenta Participations AG
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Syngenta Participations AG
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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D231/00Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C251/00Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C251/32Oximes
    • C07C251/34Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
    • C07C251/44Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with the carbon atom of at least one of the oxyimino groups being part of a ring other than a six-membered aromatic ring
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/62Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by hydrogenation of carbon-to-carbon double or triple bonds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/65Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by splitting-off hydrogen atoms or functional groups; by hydrogenolysis of functional groups
    • C07C45/66Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by splitting-off hydrogen atoms or functional groups; by hydrogenolysis of functional groups by dehydration
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/67Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton
    • C07C45/68Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms
    • C07C45/69Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by addition to carbon-to-carbon double or triple bonds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/587Unsaturated compounds containing a keto groups being part of a ring
    • C07C49/687Unsaturated compounds containing a keto groups being part of a ring containing halogen
    • C07C49/693Unsaturated compounds containing a keto groups being part of a ring containing halogen polycyclic
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/587Unsaturated compounds containing a keto groups being part of a ring
    • C07C49/703Unsaturated compounds containing a keto groups being part of a ring containing hydroxy groups
    • C07C49/743Unsaturated compounds containing a keto groups being part of a ring containing hydroxy groups having unsaturation outside the rings, e.g. humulones, lupulones
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D251/00Heterocyclic compounds containing 1,3,5-triazine rings
    • C07D251/02Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
    • C07D251/12Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
    • C07D251/26Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
    • C07D251/40Nitrogen atoms
    • C07D251/42One nitrogen atom
    • C07D251/44One nitrogen atom with halogen atoms attached to the two other ring carbon atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00Systems containing at least three condensed rings
    • C07C2603/56Ring systems containing bridged rings
    • C07C2603/58Ring systems containing bridged rings containing three rings
    • C07C2603/60Ring systems containing bridged rings containing three rings containing at least one ring with less than six members
    • C07C2603/66Ring systems containing bridged rings containing three rings containing at least one ring with less than six members containing five-membered rings

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
AU2010280923A 2009-08-06 2010-07-07 Process for the preparation of pyrazole carboxylic acid amides Active AU2010280923B2 (en)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
EP09167363 2009-08-06
EP09167363.2 2009-08-06
EP09169501 2009-09-04
EP09169501.5 2009-09-04
PCT/EP2010/059703 WO2011015416A1 (en) 2009-08-06 2010-07-07 Process for the preparation of pyrazole carboxylic acid amides

Publications (2)

Publication Number Publication Date
AU2010280923A1 AU2010280923A1 (en) 2012-02-09
AU2010280923B2 true AU2010280923B2 (en) 2014-08-07

Family

ID=42670451

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2010280923A Active AU2010280923B2 (en) 2009-08-06 2010-07-07 Process for the preparation of pyrazole carboxylic acid amides

Country Status (28)

Country Link
US (1) US8507694B2 (forum.php)
EP (1) EP2462108B1 (forum.php)
JP (1) JP5667186B2 (forum.php)
KR (1) KR101712083B1 (forum.php)
CN (1) CN102574779B (forum.php)
AR (1) AR077707A1 (forum.php)
AU (1) AU2010280923B2 (forum.php)
BR (1) BR112012002641B1 (forum.php)
CA (1) CA2770144C (forum.php)
CL (1) CL2012000272A1 (forum.php)
CO (1) CO6430457A2 (forum.php)
CR (1) CR20120056A (forum.php)
DK (1) DK2462108T3 (forum.php)
EA (1) EA019475B1 (forum.php)
EC (1) ECSP12011647A (forum.php)
EG (1) EG26957A (forum.php)
ES (1) ES2417315T3 (forum.php)
GE (1) GEP20146010B (forum.php)
IL (1) IL217692A (forum.php)
IN (1) IN2012DN00289A (forum.php)
MX (1) MX2012001480A (forum.php)
MY (1) MY161666A (forum.php)
NZ (1) NZ597576A (forum.php)
PL (1) PL2462108T3 (forum.php)
TW (1) TWI441812B (forum.php)
UY (1) UY32835A (forum.php)
WO (1) WO2011015416A1 (forum.php)
ZA (1) ZA201200413B (forum.php)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI534126B (zh) 2011-01-25 2016-05-21 先正達合夥公司 用於製備吡唑羧酸醯胺之方法
TWI510472B (zh) * 2012-02-15 2015-12-01 Syngenta Participations Ag 立體選擇性製備吡唑羧醯胺之方法
GB201403438D0 (en) * 2014-02-27 2014-04-16 Syngenta Participations Ag Polymorphs
AR099795A1 (es) 2014-03-20 2016-08-17 Mitsui Chemicals Agro Inc Composición de control de enfermedades de plantas y método para controlar enfermedades de plantas mediante su aplicación
KR20250036910A (ko) 2022-07-22 2025-03-14 신젠타 크롭 프로텍션 아게 이종환식 아미드 유도체의 고체 형태
WO2024077487A1 (en) * 2022-10-11 2024-04-18 Syngenta Crop Protection Ag Process for the preparation of pyrazole carboxylic acid amides
CN117362179B (zh) * 2023-09-22 2025-07-08 浙江工业大学 一种苯并烯氟菌唑中间体9-二氯亚甲基-1,4-二氢-5-硝基-1,4-甲桥萘的制备方法
WO2025157998A1 (en) 2024-01-26 2025-07-31 Syngenta Crop Protection Ag Chemical process

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2004035589A1 (en) * 2002-10-18 2004-04-29 Syngenta Participations Ag Heterocyclocarboxamide derivatives
WO2007048556A1 (en) * 2005-10-25 2007-05-03 Syngenta Participations Ag Heterocyclic amide derivatives useful as microbiocides

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4370341A (en) * 1980-12-11 1983-01-25 Ayerst, Mckenna & Harrison, Ltd. 6,7,8,9-Tetrahydro-3H-benz[E]indol-8-amine derivatives
JPS58194853A (ja) * 1982-05-11 1983-11-12 Showa Denko Kk シクロヘキセン−アセチルオキシム誘導体
US5093347A (en) * 1991-01-28 1992-03-03 Monsanto Company 3-difluoromethylpyrazolecarboxamide fungicides, compositions and use
US5932752A (en) * 1995-12-29 1999-08-03 Council Of Scientific And Industrial Research Process for the C-C bond forming reaction using solid acid catalysts
CN1618783A (zh) * 2004-04-22 2005-05-25 复旦大学 一种多取代苯醌的制备方法

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2004035589A1 (en) * 2002-10-18 2004-04-29 Syngenta Participations Ag Heterocyclocarboxamide derivatives
WO2007048556A1 (en) * 2005-10-25 2007-05-03 Syngenta Participations Ag Heterocyclic amide derivatives useful as microbiocides

Also Published As

Publication number Publication date
EG26957A (en) 2015-02-01
EA201200246A1 (ru) 2012-08-30
EA019475B1 (ru) 2014-03-31
ECSP12011647A (es) 2012-03-30
BR112012002641A2 (pt) 2016-03-22
EP2462108B1 (en) 2013-04-17
MX2012001480A (es) 2012-02-22
BR112012002641B1 (pt) 2018-05-22
JP2013501016A (ja) 2013-01-10
MY161666A (en) 2017-04-28
AR077707A1 (es) 2011-09-14
CO6430457A2 (es) 2012-04-30
TW201107297A (en) 2011-03-01
ES2417315T3 (es) 2013-08-07
WO2011015416A1 (en) 2011-02-10
KR101712083B1 (ko) 2017-03-03
IN2012DN00289A (forum.php) 2015-05-08
CR20120056A (es) 2012-03-06
CN102574779B (zh) 2014-10-15
US20120136162A1 (en) 2012-05-31
CL2012000272A1 (es) 2012-09-28
CA2770144A1 (en) 2011-02-10
AU2010280923A1 (en) 2012-02-09
ZA201200413B (en) 2012-10-31
JP5667186B2 (ja) 2015-02-12
GEP20146010B (en) 2014-01-10
KR20120043059A (ko) 2012-05-03
IL217692A (en) 2015-07-30
CN102574779A (zh) 2012-07-11
NZ597576A (en) 2013-01-25
UY32835A (es) 2011-03-31
PL2462108T3 (pl) 2013-09-30
EP2462108A1 (en) 2012-06-13
DK2462108T3 (da) 2013-07-08
CA2770144C (en) 2017-03-21
TWI441812B (zh) 2014-06-21
US8507694B2 (en) 2013-08-13

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