ATE532811T1 - Verfahren zur reinigung einer polyetherverbindung - Google Patents
Verfahren zur reinigung einer polyetherverbindungInfo
- Publication number
- ATE532811T1 ATE532811T1 AT07806283T AT07806283T ATE532811T1 AT E532811 T1 ATE532811 T1 AT E532811T1 AT 07806283 T AT07806283 T AT 07806283T AT 07806283 T AT07806283 T AT 07806283T AT E532811 T1 ATE532811 T1 AT E532811T1
- Authority
- AT
- Austria
- Prior art keywords
- polyether
- complex catalyst
- cyanide complex
- inorganic adsorbent
- powder
- Prior art date
Links
- 239000004721 Polyphenylene oxide Substances 0.000 title abstract 6
- 229920000570 polyether Polymers 0.000 title abstract 6
- 238000004140 cleaning Methods 0.000 title 1
- 150000001875 compounds Chemical class 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- 239000002184 metal Substances 0.000 abstract 5
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 abstract 3
- 239000003463 adsorbent Substances 0.000 abstract 3
- 239000003054 catalyst Substances 0.000 abstract 3
- 239000000843 powder Substances 0.000 abstract 3
- 239000010419 fine particle Substances 0.000 abstract 2
- 239000002245 particle Substances 0.000 abstract 2
- 125000002947 alkylene group Chemical group 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract 1
- 239000003999 initiator Substances 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
- 238000007151 ring opening polymerisation reaction Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
- C08G65/2606—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups
- C08G65/2609—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups containing aliphatic hydroxyl groups
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/04—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers only
- C08G65/06—Cyclic ethers having no atoms other than carbon and hydrogen outside the ring
- C08G65/08—Saturated oxiranes
- C08G65/10—Saturated oxiranes characterised by the catalysts used
- C08G65/12—Saturated oxiranes characterised by the catalysts used containing organo-metallic compounds or metal hydrides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
- C08G65/2645—Metals or compounds thereof, e.g. salts
- C08G65/2663—Metal cyanide catalysts, i.e. DMC's
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/30—Post-polymerisation treatment, e.g. recovery, purification, drying
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Toxicology (AREA)
- Polyethers (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2006236937 | 2006-08-31 | ||
| PCT/JP2007/066806 WO2008026657A1 (fr) | 2006-08-31 | 2007-08-29 | Procédé de purification d'un composé polyéther |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE532811T1 true ATE532811T1 (de) | 2011-11-15 |
Family
ID=39135939
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT07806283T ATE532811T1 (de) | 2006-08-31 | 2007-08-29 | Verfahren zur reinigung einer polyetherverbindung |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US8354559B2 (de) |
| EP (1) | EP2058352B1 (de) |
| JP (1) | JP5251510B2 (de) |
| CN (1) | CN101506268B (de) |
| AT (1) | ATE532811T1 (de) |
| TW (1) | TW200833735A (de) |
| WO (1) | WO2008026657A1 (de) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2471837B1 (de) * | 2009-09-17 | 2015-01-14 | Asahi Glass Company, Limited | Verfahren zur polyetherherstellung |
| EP2471831A4 (de) * | 2009-09-30 | 2013-08-21 | Asahi Glass Co Ltd | Verfahren zur herstellung eines isocyanat-terminierten präpolymers, in diesem verfahren gewonnenes präpolymer und polyurethanharz |
| CN101962441B (zh) * | 2010-10-09 | 2013-05-08 | 南京理工大学 | 一种低不饱和度聚醚多元醇的提纯方法 |
| JP5716382B2 (ja) * | 2010-12-21 | 2015-05-13 | 東ソー株式会社 | ポリアルキレングリコールの製造方法 |
| KR101907233B1 (ko) | 2011-06-03 | 2018-10-11 | 스미토모 세이카 가부시키가이샤 | 폴리알킬렌옥시드 입자 및 그의 제조방법 |
| JP5927184B2 (ja) * | 2011-06-03 | 2016-06-01 | 住友精化株式会社 | ポリアルキレンオキシド粒子及びその製造方法 |
| KR101909320B1 (ko) * | 2011-08-25 | 2018-10-17 | 다우 글로벌 테크놀로지스 엘엘씨 | 이중 금속 시아니드 촉매의 존재 하에 에틸렌 카르보네이트의 중합에 의한 옥시에틸렌 단위를 갖는 폴리에테르 알콜의 제조 방법 |
| KR101622274B1 (ko) * | 2013-05-07 | 2016-05-18 | (주)동양유지 | 에틸렌글리콜다이알킬에테르의 정제방법 |
| US9527958B2 (en) | 2014-05-02 | 2016-12-27 | Covestro Llc | Process for purification of polyether carbonate polyols |
| CN105646866B (zh) * | 2016-03-30 | 2017-12-26 | 盐城工学院 | 一种负载型双金属氰化物催化剂、制备方法与应用 |
| CN105885032A (zh) * | 2016-06-30 | 2016-08-24 | 山东凯盛新材料股份有限公司 | 采用乙二胺二邻苯基乙酸对聚醚酮酮粗品进行纯化的工艺 |
| CN106117543A (zh) * | 2016-06-30 | 2016-11-16 | 山东凯盛新材料股份有限公司 | 聚醚酮酮粗品的后处理方法 |
| CN106146826A (zh) * | 2016-06-30 | 2016-11-23 | 山东凯盛新材料股份有限公司 | 聚醚酮酮粗品的纯化工艺 |
| KR101867721B1 (ko) * | 2016-12-16 | 2018-06-14 | 주식회사 포스코 | 폴리에테르 카보네이트 폴리올 제조공정에서의 프로필렌 카보네이트의 분리방법 |
| CN107586383B (zh) * | 2017-10-20 | 2020-05-15 | 江苏钟山化工有限公司 | 一种降低聚醚多元醇中voc含量及气味的精制方法 |
| US20190119444A1 (en) | 2017-10-25 | 2019-04-25 | Covestro Llc | Process to remove dmc catalysts from polyether carbonate polyols |
| ES2988729T3 (es) | 2019-01-31 | 2024-11-21 | Dow Global Technologies Llc | Proceso de purificación de poliéteres de carbonato poliol |
| CN115405701A (zh) * | 2021-10-09 | 2022-11-29 | 南通恒华粘合材料科技有限公司 | 一种机械密封润滑方法及其应用 |
| EP4713380A1 (de) * | 2023-05-18 | 2026-03-25 | Shell Internationale Research Maatschappij B.V. | Verfahren zur behandlung von polyetheralkoholen hergestellt unter verwendung von doppelmetallcyanidkatalysatoren |
| WO2025252602A1 (en) * | 2024-06-07 | 2025-12-11 | Shell Internationale Research Maatschappij B.V. | Polyether alcohol production |
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|---|---|---|---|---|
| US4721818A (en) | 1987-03-20 | 1988-01-26 | Atlantic Richfield Company | Purification of polyols prepared using double metal cyanide complex catalysts |
| US4877906A (en) * | 1988-11-25 | 1989-10-31 | Arco Chemical Technology, Inc. | Purification of polyols prepared using double metal cyanide complex catalysts |
| US4987271A (en) * | 1989-02-17 | 1991-01-22 | Asahi Glass Company, Ltd. | Method for purifying a polyoxyalkylene alcohol |
| JP2870927B2 (ja) | 1989-02-17 | 1999-03-17 | 旭硝子株式会社 | ポリオキシアルキレンアルコールの精製方法 |
| JP2870926B2 (ja) | 1989-02-17 | 1999-03-17 | 旭硝子株式会社 | ポリオキシアルキレンアルコールの精製法 |
| JPH0696635B2 (ja) | 1989-09-01 | 1994-11-30 | 旭硝子株式会社 | ポリエーテル類の精製方法 |
| JP2954604B2 (ja) | 1989-09-01 | 1999-09-27 | 旭硝子株式会社 | ポリエーテル類の精製法 |
| JP2830171B2 (ja) | 1989-09-29 | 1998-12-02 | 旭硝子株式会社 | ポリエーテル類の製造方法 |
| JP2918619B2 (ja) * | 1990-04-06 | 1999-07-12 | 花王株式会社 | 金属磁性粉末の製造方法及び磁気記録媒体用塗膜 |
| JPH04197407A (ja) | 1990-11-29 | 1992-07-17 | Asahi Glass Co Ltd | ポリエーテル類の精製法 |
| JPH04197406A (ja) | 1990-11-29 | 1992-07-17 | Asahi Glass Co Ltd | ポリエーテル類の精製方法 |
| JPH04268329A (ja) | 1991-02-25 | 1992-09-24 | Asahi Glass Co Ltd | ポリエーテル類の製造方法 |
| US5405977A (en) * | 1993-01-04 | 1995-04-11 | Huntsman Corporation | Process for removing organic halides from alkylene carbonates |
| US5470813A (en) * | 1993-11-23 | 1995-11-28 | Arco Chemical Technology, L.P. | Double metal cyanide complex catalysts |
| US5712216A (en) * | 1995-05-15 | 1998-01-27 | Arco Chemical Technology, L.P. | Highly active double metal cyanide complex catalysts |
| US5811566A (en) * | 1994-07-18 | 1998-09-22 | Asahi Glass Company Ltd. | Process for purifying a polyether |
| US5767323A (en) * | 1995-12-22 | 1998-06-16 | Arco Chemical Technology, L.P. | Process for preparing polyoxyalkylene polyether polyols having low levels of transition metals through double metal cyanide complex polyoxyalkylation |
| JP3145022B2 (ja) * | 1996-01-17 | 2001-03-12 | 旭硝子株式会社 | 硬化性組成物 |
| US5639705A (en) | 1996-01-19 | 1997-06-17 | Arco Chemical Technology, L.P. | Double metal cyanide catalysts and methods for making them |
| JP4201233B2 (ja) * | 1998-10-20 | 2008-12-24 | 三井化学株式会社 | ポリオキシアルキレンポリオール及びその誘導体の製造方法 |
| US6410676B1 (en) * | 1998-10-20 | 2002-06-25 | Mitsui Chemicals, Inc. | Method for producing polyoxyalkylene polyol and derivatives thereof |
| CA2301313A1 (en) * | 1999-03-18 | 2000-09-18 | Yuka Kanamori | Curable composition |
| DE19919267A1 (de) * | 1999-04-28 | 2000-11-02 | Bayer Ag | Kristallisierende Polyetherpolyole, ein Verfahren zu deren Herstellung sowie deren Verwendung |
| JP2002201263A (ja) | 2000-12-28 | 2002-07-19 | Dai Ichi Kogyo Seiyaku Co Ltd | ポリエーテルの製造方法 |
| JP2002212280A (ja) | 2001-01-24 | 2002-07-31 | Dai Ichi Kogyo Seiyaku Co Ltd | ポリエーテルの製造方法 |
| US6762325B2 (en) * | 2001-05-16 | 2004-07-13 | Nippon Shokubai Co., Ltd. | Method for production of alkoxylated compound |
| JP4251820B2 (ja) | 2001-05-16 | 2009-04-08 | 株式会社日本触媒 | アルコキシレート化合物の製造方法 |
| DE10138216A1 (de) * | 2001-08-03 | 2003-02-20 | Bayer Ag | Aliphatische Polycarbonathomo- und -copolymere durch DMC-Katalyse |
| EP1288244A1 (de) * | 2001-08-31 | 2003-03-05 | Asahi Glass Company, Limited | Doppelmetallcyanidkatalysator für ringöffende Polymerisation von Alkylenoxiden und Verfahren zu seiner Herstellung |
| JP2003165836A (ja) | 2001-11-29 | 2003-06-10 | Asahi Glass Co Ltd | スラリー状複合金属シアン化物錯体触媒およびその製造方法、ならびにこれを用いたポリエーテルポリオールまたはポリエーテルモノオールの製造方法 |
| ES2199666B1 (es) * | 2002-02-25 | 2005-06-01 | Repsol Quimica, S.A. | Procedimiento de produccion de polioleteres. |
| JP2004182970A (ja) * | 2002-10-09 | 2004-07-02 | Sanyo Chem Ind Ltd | 共重合ポリエーテル及びその製造法 |
| KR100990062B1 (ko) | 2003-01-28 | 2010-10-29 | 아사히 가라스 가부시키가이샤 | 폴리에테르폴리올 조성물 및 그 용도 |
| KR101231506B1 (ko) * | 2003-06-04 | 2013-02-07 | 아사히 가라스 가부시키가이샤 | 복합 금속 시안화물 착물 촉매, 그 제조방법 및 그 이용 |
| JP4556496B2 (ja) | 2003-06-04 | 2010-10-06 | 旭硝子株式会社 | 複合金属シアン化物錯体触媒、その製造方法およびその利用 |
| DE60317652T2 (de) * | 2003-06-30 | 2008-10-30 | Repsol Quimica S.A. | Verfahren zur Reinigung von Polyetherpolyolen |
| JP2005132990A (ja) * | 2003-10-31 | 2005-05-26 | Asahi Glass Co Ltd | ポリエーテル類の製造法 |
| RU2007119396A (ru) * | 2004-10-26 | 2008-12-10 | Дау Глобал Текнолоджиз Инк. (Us) | Улучшенный способ алкоксилирования соединений, содержащих активный водород, и алкоксилированные соединения, получаемые таким способом |
| JP2006236937A (ja) | 2005-02-28 | 2006-09-07 | Nec Tokin Corp | 蓄電装置 |
| JP4674896B2 (ja) * | 2005-03-16 | 2011-04-20 | 協和化学工業株式会社 | 珪酸アルミニウム、その製造方法およびそれを用いたポリオキシアルキレンポリオールの精製方法 |
-
2007
- 2007-08-29 CN CN2007800311831A patent/CN101506268B/zh not_active Expired - Fee Related
- 2007-08-29 EP EP07806283A patent/EP2058352B1/de not_active Not-in-force
- 2007-08-29 AT AT07806283T patent/ATE532811T1/de active
- 2007-08-29 JP JP2008532097A patent/JP5251510B2/ja active Active
- 2007-08-29 WO PCT/JP2007/066806 patent/WO2008026657A1/ja not_active Ceased
- 2007-08-30 TW TW096132276A patent/TW200833735A/zh unknown
-
2009
- 2009-03-02 US US12/396,175 patent/US8354559B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| US8354559B2 (en) | 2013-01-15 |
| CN101506268B (zh) | 2012-09-05 |
| JPWO2008026657A1 (ja) | 2010-01-21 |
| WO2008026657A1 (fr) | 2008-03-06 |
| TW200833735A (en) | 2008-08-16 |
| EP2058352A4 (de) | 2010-07-07 |
| EP2058352A1 (de) | 2009-05-13 |
| CN101506268A (zh) | 2009-08-12 |
| JP5251510B2 (ja) | 2013-07-31 |
| EP2058352B1 (de) | 2011-11-09 |
| US20090203875A1 (en) | 2009-08-13 |
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