AR058827A1 - Composiciones azeotropicas que comprenden 2,3,3,3-tetra-fluoropropeno y fluoruro de hidrogeno y sus usos - Google Patents
Composiciones azeotropicas que comprenden 2,3,3,3-tetra-fluoropropeno y fluoruro de hidrogeno y sus usosInfo
- Publication number
- AR058827A1 AR058827A1 ARP060104801A ARP060104801A AR058827A1 AR 058827 A1 AR058827 A1 AR 058827A1 AR P060104801 A ARP060104801 A AR P060104801A AR P060104801 A ARP060104801 A AR P060104801A AR 058827 A1 AR058827 A1 AR 058827A1
- Authority
- AR
- Argentina
- Prior art keywords
- fluoropropen
- tetra
- hydrogen fluoride
- azeotropic compositions
- compositions
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C21/00—Acyclic unsaturated compounds containing halogen atoms
- C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
- C07C21/18—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/19—Fluorine; Hydrogen fluoride
- C01B7/191—Hydrogen fluoride
- C01B7/195—Separation; Purification
- C01B7/196—Separation; Purification by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/25—Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
- C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
- C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
- C07C17/386—Separation; Purification; Stabilisation; Use of additives by distillation with auxiliary compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
Abstract
Composiciones azeotropicas o casi azeotropicas que comprenden 2,3,3,3-tetrafluoropropeno (HFC-1234yf) y fluoro de hidrogeno. Estas composiciones son utiles en procesos para producir y purificar HFC-1234yf. Adicionalmente, se divulgan aquí procesos para la fabricacion de HFC-1234yf.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US73232105P | 2005-11-01 | 2005-11-01 |
Publications (1)
Publication Number | Publication Date |
---|---|
AR058827A1 true AR058827A1 (es) | 2008-02-27 |
Family
ID=37907695
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ARP060104801A AR058827A1 (es) | 2005-11-01 | 2006-11-01 | Composiciones azeotropicas que comprenden 2,3,3,3-tetra-fluoropropeno y fluoruro de hidrogeno y sus usos |
Country Status (12)
Country | Link |
---|---|
US (1) | US7476771B2 (es) |
EP (3) | EP2476661A1 (es) |
JP (1) | JP5281407B2 (es) |
KR (1) | KR101474026B1 (es) |
CN (2) | CN101351428B (es) |
AR (1) | AR058827A1 (es) |
BR (1) | BRPI0619721A2 (es) |
CA (1) | CA2627898A1 (es) |
ES (2) | ES2453159T3 (es) |
RU (1) | RU2422427C2 (es) |
UA (1) | UA95259C2 (es) |
WO (1) | WO2007053736A2 (es) |
Families Citing this family (79)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9102579B2 (en) | 2004-04-29 | 2015-08-11 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
US7897823B2 (en) * | 2004-10-29 | 2011-03-01 | E. I. Du Pont De Nemours And Company | Process for production of azeotrope compositions comprising hydrofluoroolefin and hydrogen fluoride and uses of said azeotrope compositions in separation processes |
US8766020B2 (en) * | 2008-07-31 | 2014-07-01 | Honeywell International Inc. | Process for producing 2,3,3,3-tetrafluoropropene |
EP2336102A1 (en) * | 2005-11-03 | 2011-06-22 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
WO2007079435A2 (en) * | 2006-01-03 | 2007-07-12 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
WO2007111313A1 (ja) | 2006-03-24 | 2007-10-04 | Zeon Corporation | 長尺の延伸フィルムおよびその製造方法並びに用途 |
WO2008002500A1 (en) | 2006-06-27 | 2008-01-03 | E. I. Du Pont De Nemours And Company | Tetrafluoropropene production processes |
ES2539939T3 (es) * | 2006-06-27 | 2015-07-07 | E.I. Du Pont De Nemours And Company | Procedimientos de producción de 1,2,3,3,3-pentafluoropropeno |
JP2009542650A (ja) | 2006-06-27 | 2009-12-03 | イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー | テトラフルオロプロペン製造方法 |
US8377327B2 (en) | 2006-06-27 | 2013-02-19 | E I Du Pont De Nemours And Company | Tetrafluoropropene production processes |
US7803975B2 (en) * | 2006-07-13 | 2010-09-28 | E.I. Du Pont De Nemours And Company | Process for separating a fluoroolefin from HF by liquid-liquid extraction |
ES2523694T3 (es) * | 2006-07-13 | 2014-11-28 | E.I. Du Pont De Nemours And Company | Procesos de producción catalítica para preparar 1,2,3,3,3-pentafluoropropeno |
GB0614927D0 (en) * | 2006-07-27 | 2006-09-06 | Ineos Fluor Holdings Ltd | Separation process |
PL2433921T3 (pl) | 2006-08-24 | 2014-06-30 | Du Pont | Sposoby oddzielania fluoroolefin od fluorowodoru poprzez destylację azeotropową |
US7420094B2 (en) * | 2006-09-05 | 2008-09-02 | E.I. Du Pont De Nemours And Company | Catalytic isomerization processes of 1,3,3,3-tetrafluoropropene for making 2,3,3,3-tetrafluoropropene |
BRPI0717091A2 (pt) * | 2006-10-03 | 2013-11-26 | Ineos Fluor Holdings Ltd | Processos para preparação de um composto e para isomerização de um composto, uso de um catalisador, fluido, mistura refrigerante, e, automóvel. |
EP4328213A3 (en) * | 2006-10-27 | 2024-04-03 | Honeywell International Inc. | A high purity 2,3,3,3-tetrafluoropropene |
EP2091898A1 (en) * | 2006-10-31 | 2009-08-26 | E.I. Du Pont De Nemours And Company | Processes for producing 2,3,3,3-tetrafluoropropene and/or 1,2,3,3-tetrafluoropropene |
CN103483141B (zh) * | 2006-10-31 | 2015-09-16 | 纳幕尔杜邦公司 | 氟丙烷、卤代丙烯以及2-氯-3,3,3-三氟-1-丙烯与hf的共沸组合物和1,1,1,2,2-五氟丙烷与hf的共沸组合物的制备方法 |
CA3002834C (en) | 2007-05-11 | 2020-04-07 | E. I. Du Pont De Nemours And Company | Vapor compression heat transfer system comprising an intermediate heat exchanger and a dual-row evaporator |
US20100185029A1 (en) * | 2007-06-27 | 2010-07-22 | Arkema Inc. | Two step process for the manufacture of hydrofluoroolefins |
US7884254B2 (en) * | 2007-08-08 | 2011-02-08 | Honeywell International Inc. | Dehydrochlorination of hydrochlorofluorocarbons using pre-treated activated carbon catalysts |
US9035111B2 (en) | 2007-08-22 | 2015-05-19 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
US9079818B2 (en) * | 2007-10-15 | 2015-07-14 | Honeywell International Inc. | Process for synthesis of fluorinated olefins |
JP4849058B2 (ja) * | 2007-11-21 | 2011-12-28 | ダイキン工業株式会社 | 含フッ素オレフィンの製造方法 |
KR101851887B1 (ko) * | 2008-02-21 | 2018-04-24 | 이 아이 듀폰 디 네모아 앤드 캄파니 | 공비 증류에 의한 플루오르화수소로부터의 1,3,3,3-테트라플루오로프로펜의 분리 방법 |
RU2476416C2 (ru) * | 2008-02-21 | 2013-02-27 | Е.И.Дюпон Де Немур Энд Компани | Способы отделения 2,3,3,3-тетрафторпропена от фтористого водорода способом азеотропной дистилляции |
KR101861111B1 (ko) * | 2008-02-21 | 2018-05-28 | 이 아이 듀폰 디 네모아 앤드 캄파니 | 3,3,3-트라이플루오로프로펜 및 플루오르화수소를 포함하는 공비 조성물 및 이의 분리방법 |
EP2098499B2 (en) † | 2008-03-06 | 2017-11-22 | Honeywell International Inc. | Azeotrope-like composition of 2-chloro-3,3,3-trifluoropropene (HCFC-1233xf) and hydrogen fluoride (HF) |
SG193153A1 (en) | 2008-05-07 | 2013-09-30 | Du Pont | Compositions comprising 1,1,1,2,3-pentafluoropropane or 2,3,3,3- tetrafluoropropene |
LT2634232T (lt) * | 2008-05-07 | 2022-06-10 | The Chemours Company Fc, Llc | Kompozicijos |
US8168837B2 (en) * | 2008-05-15 | 2012-05-01 | Honeywell International Inc. | Process for separating hydrogen fluoride from organic feedstocks |
GB0808836D0 (en) | 2008-05-15 | 2008-06-18 | Ineos Fluor Ltd | Process |
JP2011525925A (ja) * | 2008-06-26 | 2011-09-29 | アーケマ・インコーポレイテッド | 1230xaから1234yfへの触媒的気相フッ素化 |
JP5119060B2 (ja) * | 2008-06-27 | 2013-01-16 | サンデン株式会社 | 冷凍サイクル |
CN102131754B (zh) * | 2008-08-26 | 2015-02-25 | 大金工业株式会社 | 共沸或类共沸组合物和制备2,3,3,3-四氟丙烯的方法 |
FR2937328B1 (fr) | 2008-10-16 | 2010-11-12 | Arkema France | Procede de transfert de chaleur |
US8008243B2 (en) * | 2008-10-31 | 2011-08-30 | Honeywell International Inc. | Azeotrope-like compositions of 1,1,2,3-tetrachloropropene and hydrogen fluoride |
US20100119460A1 (en) * | 2008-11-11 | 2010-05-13 | Honeywell International Inc. | Azeotrope-Like Compositions Of 2,3,3,3-Tetrafluoropropene And 3,3,3-Trifluoropropene |
JP2012519736A (ja) * | 2009-02-11 | 2012-08-30 | アルケマ フランス | クロロトリフルオロプロペンとペンタンの共沸組成物および共沸様組成物 |
CN102405202B (zh) | 2009-04-23 | 2015-02-11 | 大金工业株式会社 | 制备2-氯-3,3,3-三氟丙烯的方法 |
JP5620478B2 (ja) | 2009-06-03 | 2014-11-05 | イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニーE.I.Du Pont De Nemours And Company | 2,3,3,3−テトラフルオロプロペンを製造するための触媒および方法 |
US8487145B2 (en) | 2009-06-03 | 2013-07-16 | E I De Pont De Nemours And Company | Catalysts and process to manufacture 2,3,3,3-tetrafluoropropene |
FR2948362B1 (fr) | 2009-07-23 | 2012-03-23 | Arkema France | Procede de preparation de composes fluores |
FR2950066B1 (fr) * | 2009-09-11 | 2011-10-28 | Arkema France | Refrigeration basse et moyenne temperature |
US8486293B2 (en) | 2009-10-30 | 2013-07-16 | E I Du Pont De Nemours And Company | Hydrogen fluoride-HFC-254eb azeotrope and its uses |
IN2012DN03407A (es) * | 2009-11-03 | 2015-10-23 | Du Pont | |
MX359434B (es) | 2009-12-22 | 2018-09-27 | Du Pont | Composiciones que comprenden 2,3,3,3-tetrafluoropropeno, 1,1,2,3-tetracloropropeno, 2-cloro-3,3,3-trifluoropropeno, o 2-cloro-1,1,1,2-tetrafluoropropano. |
WO2011099604A2 (en) * | 2010-02-12 | 2011-08-18 | Daikin Industries, Ltd. | Process for producing fluorine-containing alkene |
US8114308B2 (en) | 2010-03-30 | 2012-02-14 | Honeywell International Inc. | Azeotrope-like composition of 2,3-dichloro-3,3-difluoropropene (HCFO-1232xf) and hydrogen fluoride (HF) |
US8927791B2 (en) | 2010-04-29 | 2015-01-06 | Honeywell International Inc. | Method for producing tetrafluoropropenes |
CN102884031B (zh) * | 2010-05-03 | 2016-04-06 | 阿科玛股份有限公司 | 用于形成四氟烯烃的五氟烷的脱氟化氢作用 |
CN101913988B (zh) * | 2010-09-07 | 2013-09-25 | 西安近代化学研究所 | 2,3,3,3-四氟丙烯的制备方法 |
US8741828B2 (en) * | 2011-02-23 | 2014-06-03 | Honeywell International Inc. | Azeotrope and azeotrope-like compositions useful for the production of haloolefins |
CN102295522B (zh) * | 2011-05-27 | 2014-01-01 | 山东东岳高分子材料有限公司 | 2,3,3,3-四氟丙烯的制备方法 |
FR2977584B1 (fr) * | 2011-07-08 | 2014-12-05 | Arkema France | Procede de separation et recuperation du 2,3,3,3-tetrafluoropropene et de l'acide fluorhydrique |
EP2799415B2 (en) | 2011-12-28 | 2019-06-12 | AGC Inc. | Method for purifying 2,3,3,3-tetrafluoropropene and process for producing same |
MX359553B (es) | 2012-06-06 | 2018-10-02 | Chemours Co Fc Llc | Proceso para reduccion de impurezas de rfccx en fluoroolefinas. |
FR3000095B1 (fr) * | 2012-12-26 | 2015-02-20 | Arkema France | Composition comprenant du 2,3,3,3-tetrafluoropropene et du 1,2-difluoroethylene |
EP2939994B1 (en) * | 2012-12-27 | 2018-07-18 | Asahi Glass Company, Limited | Method for purifying tetrafluoropropene |
MX370100B (es) | 2013-03-15 | 2019-12-02 | Chemours Co Fc Llc | Proceso para la reduccion de impurezas de alquino en fluoroolefinas. |
FR3003569B1 (fr) * | 2013-03-20 | 2015-12-25 | Arkema France | Composition comprenant hf et 1,3,3,3-tetrafluoropropene |
FR3003566B1 (fr) * | 2013-03-20 | 2018-07-06 | Arkema France | Composition comprenant hf et e-3,3,3-trifluoro-1-chloropropene |
FR3003565B1 (fr) | 2013-03-20 | 2018-06-29 | Arkema France | Composition comprenant hf et 2,3,3,3-tetrafluoropropene |
FR3003567B1 (fr) * | 2013-03-20 | 2015-03-06 | Arkema France | Composition comprenant hf et 3,3,3-trifluoropropene |
FR3015478B1 (fr) | 2013-12-19 | 2015-12-25 | Arkema France | Compositions azeotropiques a base de fluorure d'hydrogene et de z-3,3,3-trifluoro-1-chloropropene |
JP6328589B2 (ja) | 2015-05-29 | 2018-05-23 | ダイキン工業株式会社 | 含フッ素オレフィンの製造方法 |
GB2540427B (en) | 2015-07-17 | 2017-07-19 | Mexichem Fluor Sa De Cv | Process for the preparation of 2,3,3,3-tetrafluoropropene (1234yf) |
KR20160017661A (ko) | 2016-01-29 | 2016-02-16 | 한국과학기술연구원 | 헥사플루오로프로필렌으로부터 2,3,3,3-테트라플루오로프로펜과 1,3,3,3-테트라플루오로프로펜의 제조방법 |
CN105622331A (zh) * | 2016-02-23 | 2016-06-01 | 常熟三爱富中昊化工新材料有限公司 | 一种含氟烯烃的制备方法 |
CN105669363A (zh) * | 2016-02-23 | 2016-06-15 | 常熟三爱富中昊化工新材料有限公司 | 一种含氟烯烃的纯化方法 |
GB201615197D0 (en) | 2016-09-07 | 2016-10-19 | Mexichem Fluor Sa De Cv | Catalyst and process using the catalyst |
GB201615209D0 (en) | 2016-09-07 | 2016-10-19 | Mexichem Fluor Sa De Cv | Catalyst and process using the catalyst |
FR3056222B1 (fr) | 2016-09-19 | 2020-01-10 | Arkema France | Composition a base de 1-chloro-3,3,3-trifluoropropene |
FR3065726B1 (fr) * | 2017-04-28 | 2019-04-19 | Arkema France | Procede de production et de purification du 2,3,3,3-tetrafluoropropene. |
US10487031B2 (en) * | 2017-09-11 | 2019-11-26 | The Chemours Company Fc, Llc | Azeotropic compositions comprising hydrogen fluoride and fluorocarbons |
FR3077572B1 (fr) * | 2018-02-05 | 2021-10-08 | Arkema France | Composition azeotropique ou quasi-azeotropique ternaire comprenant hf, 2,3,3,3-tetrafluoropropene et 1,1,1,2,2,-pentafluoropropane. |
EP3823948A1 (en) | 2018-07-18 | 2021-05-26 | The Chemours Company FC, LLC | Production of haloolefins in an adiabatic reaction zone |
CN113624570B (zh) * | 2021-08-06 | 2023-04-28 | 清华大学 | 汽液相平衡装置及氟代烃中的hf的分析方法 |
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US2931840A (en) * | 1958-11-25 | 1960-04-05 | Du Pont | Process for preparing 2, 3, 3, 3-tetrafluoropropene |
US2996555A (en) * | 1959-06-25 | 1961-08-15 | Dow Chemical Co | Preparation of 2, 3, 3, 3-tetrafluoropropene |
US4799260A (en) * | 1985-03-07 | 1989-01-17 | Dolby Laboratories Licensing Corporation | Variable matrix decoder |
US4766260A (en) | 1987-07-07 | 1988-08-23 | E. I. Du Pont De Nemours And Company | Gas-phase fluorination process |
JPH01207250A (ja) | 1988-02-12 | 1989-08-21 | Daikin Ind Ltd | 含フツ素オレフインの製造方法 |
SU1706690A1 (ru) | 1988-04-19 | 1992-01-23 | Всесоюзный Научно-Исследовательский Институт Технического Углерода | Пористый углеродный материал |
US4902838A (en) | 1988-12-28 | 1990-02-20 | E. I. Du Pont De Nemours And Company | Isomerization of saturated fluorohydrocarbons |
US5136113A (en) | 1991-07-23 | 1992-08-04 | E. I. Du Pont De Nemours And Company | Catalytic hydrogenolysis |
US5268122A (en) | 1991-08-28 | 1993-12-07 | E. I. Du Pont De Nemours And Company | Gem-dihydropolyfluoroalkanes and monohydropolyfluoroalkenes, processes for their production, and use of gem-dihydropolyfluoroalkanes in cleaning compositions |
US5396000A (en) | 1993-05-24 | 1995-03-07 | E. I. Du Pont De Nemours And Company | Process for the manufacture of 1,1,1,2,3,-pentafluoropropane |
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EP0958265B1 (en) | 1997-01-31 | 2003-04-02 | E.I. Du Pont De Nemours And Company | The catalytic manufacture of pentafluoropropenes |
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JP2001524460A (ja) * | 1997-11-25 | 2001-12-04 | インペリアル・ケミカル・インダストリーズ・ピーエルシー | 弗素含有有機化合物の製造 |
CA2333470C (en) | 1998-06-02 | 2008-08-26 | E.I. Du Pont De Nemours And Company | Process for the production of hexafluoropropylene from cc1f2cc1fcf3 and azeotropes of cclf2cc1fcf3 with hf |
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-
2006
- 2006-10-31 US US11/590,454 patent/US7476771B2/en active Active
- 2006-11-01 CA CA002627898A patent/CA2627898A1/en not_active Abandoned
- 2006-11-01 CN CN200680050042XA patent/CN101351428B/zh active Active
- 2006-11-01 EP EP12161039A patent/EP2476661A1/en not_active Withdrawn
- 2006-11-01 BR BRPI0619721-3A patent/BRPI0619721A2/pt not_active IP Right Cessation
- 2006-11-01 CN CN201210021126.8A patent/CN102603462B/zh active Active
- 2006-11-01 UA UAA200806186A patent/UA95259C2/ru unknown
- 2006-11-01 EP EP06836796.0A patent/EP1954662B1/en active Active
- 2006-11-01 AR ARP060104801A patent/AR058827A1/es not_active Application Discontinuation
- 2006-11-01 EP EP12160936.6A patent/EP2508499B1/en active Active
- 2006-11-01 RU RU2008121963/04A patent/RU2422427C2/ru not_active IP Right Cessation
- 2006-11-01 ES ES12160936.6T patent/ES2453159T3/es active Active
- 2006-11-01 JP JP2008539017A patent/JP5281407B2/ja active Active
- 2006-11-01 ES ES06836796T patent/ES2427099T3/es active Active
- 2006-11-01 WO PCT/US2006/042771 patent/WO2007053736A2/en active Application Filing
-
2008
- 2008-05-30 KR KR1020087013105A patent/KR101474026B1/ko active IP Right Grant
Also Published As
Publication number | Publication date |
---|---|
ES2453159T3 (es) | 2014-04-04 |
KR20080066837A (ko) | 2008-07-16 |
WO2007053736A3 (en) | 2007-08-02 |
EP2476661A1 (en) | 2012-07-18 |
CN102603462A (zh) | 2012-07-25 |
US20070100175A1 (en) | 2007-05-03 |
EP1954662A2 (en) | 2008-08-13 |
JP2009513719A (ja) | 2009-04-02 |
CN102603462B (zh) | 2014-11-26 |
CN101351428A (zh) | 2009-01-21 |
UA95259C2 (ru) | 2011-07-25 |
EP2508499B1 (en) | 2014-01-08 |
US7476771B2 (en) | 2009-01-13 |
EP1954662B1 (en) | 2013-07-24 |
KR101474026B1 (ko) | 2014-12-17 |
CN101351428B (zh) | 2012-06-27 |
JP5281407B2 (ja) | 2013-09-04 |
RU2422427C2 (ru) | 2011-06-27 |
CA2627898A1 (en) | 2007-05-10 |
BRPI0619721A2 (pt) | 2011-10-11 |
RU2008121963A (ru) | 2009-12-10 |
EP2508499A1 (en) | 2012-10-10 |
ES2427099T3 (es) | 2013-10-28 |
WO2007053736A2 (en) | 2007-05-10 |
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