WO2021258120A3 - Herstellungsverfahren für polyimide - Google Patents

Herstellungsverfahren für polyimide Download PDF

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Publication number
WO2021258120A3
WO2021258120A3 PCT/AT2021/060206 AT2021060206W WO2021258120A3 WO 2021258120 A3 WO2021258120 A3 WO 2021258120A3 AT 2021060206 W AT2021060206 W AT 2021060206W WO 2021258120 A3 WO2021258120 A3 WO 2021258120A3
Authority
WO
WIPO (PCT)
Prior art keywords
salt
residues
formula
preparing polyimides
polyimides
Prior art date
Application number
PCT/AT2021/060206
Other languages
English (en)
French (fr)
Other versions
WO2021258120A2 (de
Inventor
Miriam Margarethe UNTERLASS
Daniel Alonso CERRON-INFANTES
Original Assignee
Technische Universität Wien
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Technische Universität Wien filed Critical Technische Universität Wien
Priority to KR1020237002467A priority Critical patent/KR20230027258A/ko
Priority to EP21759231.0A priority patent/EP4168473A2/de
Priority to US18/012,465 priority patent/US20230265247A1/en
Priority to CN202180044832.1A priority patent/CN115720583A/zh
Publication of WO2021258120A2 publication Critical patent/WO2021258120A2/de
Publication of WO2021258120A3 publication Critical patent/WO2021258120A3/de

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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C08G73/1003—Preparatory processes
    • C08G73/1007—Preparatory processes from tetracarboxylic acids or derivatives and diamines
    • C08G73/1028—Preparatory processes from tetracarboxylic acids or derivatives and diamines characterised by the process itself, e.g. steps, continuous
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C08G73/1003—Preparatory processes
    • C08G73/1007—Preparatory processes from tetracarboxylic acids or derivatives and diamines
    • C08G73/1028—Preparatory processes from tetracarboxylic acids or derivatives and diamines characterised by the process itself, e.g. steps, continuous
    • C08G73/1032—Preparatory processes from tetracarboxylic acids or derivatives and diamines characterised by the process itself, e.g. steps, continuous characterised by the solvent(s) used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C08G73/1075—Partially aromatic polyimides
    • C08G73/1082—Partially aromatic polyimides wholly aromatic in the tetracarboxylic moiety
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C08G73/1085—Polyimides with diamino moieties or tetracarboxylic segments containing heterocyclic moieties
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D179/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing nitrogen, with or without oxygen, or carbon only, not provided for in groups C09D161/00 - C09D177/00
    • C09D179/04—Polycondensates having nitrogen-containing heterocyclic rings in the main chain; Polyhydrazides; Polyamide acids or similar polyimide precursors
    • C09D179/08—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2203/00—Applications
    • C08L2203/16—Applications used for films

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)

Abstract

Die Erfindung betrifft ein stöchiometrisches Salz einer Tetracarbonsäure und eines Diamins der nachstehenden allgemeinen Formel (I): worin R1 aus vierwertigen Resten von Butan, Cyclobutan, Cyclopentan, Cyclohexan, Tetrahydrofuran und Benzophenon ausgewählt ist und R2 aus zweiwertigen Resten von unverzweigten, verzweigten oder cyclischen aliphatischen Kohlenwasserstoffen mit 3 bis 15 Kohlenstoffatomen ausgewählt ist, mit dem Kennzeichen, dass das Salz der Formel (I) wasserlöslich ist und aus den Verbindungen (1 ) bis (28) ausgewählt ist; sowie die aus diesen Salzen durch Polykondensation hergestellten Polyimide.
PCT/AT2021/060206 2020-06-23 2021-06-17 Herstellungsverfahren für polyimide WO2021258120A2 (de)

Priority Applications (4)

Application Number Priority Date Filing Date Title
KR1020237002467A KR20230027258A (ko) 2020-06-23 2021-06-17 폴리이미드 제조 공정
EP21759231.0A EP4168473A2 (de) 2020-06-23 2021-06-17 Herstellungsverfahren für polyimide
US18/012,465 US20230265247A1 (en) 2020-06-23 2021-06-17 Process for preparing polyimides
CN202180044832.1A CN115720583A (zh) 2020-06-23 2021-06-17 用于制备聚酰亚胺的方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
ATA50531/2020A AT523968A2 (de) 2020-06-23 2020-06-23 Herstellungsverfahren für Polyimide
ATA50531/2020 2020-06-23

Publications (2)

Publication Number Publication Date
WO2021258120A2 WO2021258120A2 (de) 2021-12-30
WO2021258120A3 true WO2021258120A3 (de) 2022-03-03

Family

ID=77499569

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/AT2021/060206 WO2021258120A2 (de) 2020-06-23 2021-06-17 Herstellungsverfahren für polyimide

Country Status (6)

Country Link
US (1) US20230265247A1 (de)
EP (1) EP4168473A2 (de)
KR (1) KR20230027258A (de)
CN (1) CN115720583A (de)
AT (1) AT523968A2 (de)
WO (1) WO2021258120A2 (de)

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1917274C3 (de) * 1969-04-03 1981-04-30 Chemische Werke Hüls AG, 4370 Marl Verfahren zur Herstellung von imidgruppenhaltigen Polymeren
JP2000319389A (ja) * 1999-05-07 2000-11-21 Unitika Ltd ポリイミド前駆体水溶液及びその製造方法、それから得られるポリイミド塗膜及びその製造方法
US20140228513A1 (en) * 2011-09-20 2014-08-14 Rhodia Operations Thermoplastic polyimides
US20140342628A1 (en) * 2011-09-20 2014-11-20 Rhodia Operations Thermoplastic (co)polyimides and synthesis methods
WO2018032023A1 (de) * 2016-08-19 2018-02-22 Technische Universität Wien Verfahren zur herstellung von polyimiden

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4484349B2 (ja) 2000-10-18 2010-06-16 ユニチカ株式会社 フッ素樹脂水分散液並びにそれから得られる塗膜及びその製造方法
JP5982320B2 (ja) 2012-05-17 2016-08-31 Ｊｆｅケミカル株式会社 コーティング剤組成物及びコーティング膜形成方法
WO2016032299A1 (ko) 2014-08-29 2016-03-03 연세대학교 원주산학협력단 단량체 염을 이용한 폴리이미드 제조방법

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1917274C3 (de) * 1969-04-03 1981-04-30 Chemische Werke Hüls AG, 4370 Marl Verfahren zur Herstellung von imidgruppenhaltigen Polymeren
JP2000319389A (ja) * 1999-05-07 2000-11-21 Unitika Ltd ポリイミド前駆体水溶液及びその製造方法、それから得られるポリイミド塗膜及びその製造方法
US20140228513A1 (en) * 2011-09-20 2014-08-14 Rhodia Operations Thermoplastic polyimides
US20140342628A1 (en) * 2011-09-20 2014-11-20 Rhodia Operations Thermoplastic (co)polyimides and synthesis methods
WO2018032023A1 (de) * 2016-08-19 2018-02-22 Technische Universität Wien Verfahren zur herstellung von polyimiden

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
MI HIE YI ET AL: "Soluble and Colorless Polyimides from Alicyclic Diamines", PART A: PURE AND APPLIED CHEMISTRY, vol. 35, no. 12, 1 December 1998 (1998-12-01), US, pages 2009 - 2022, XP055532243, ISSN: 1060-1325, DOI: 10.1080/10601329808000993 *

Also Published As

Publication number Publication date
KR20230027258A (ko) 2023-02-27
US20230265247A1 (en) 2023-08-24
AT523968A2 (de) 2022-01-15
WO2021258120A2 (de) 2021-12-30
CN115720583A (zh) 2023-02-28
EP4168473A2 (de) 2023-04-26

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