WO2021004031A1 - 一种低熔阻高纺性超低粘尼龙6切片聚合装置及操作方法 - Google Patents

一种低熔阻高纺性超低粘尼龙6切片聚合装置及操作方法 Download PDF

Info

Publication number
WO2021004031A1
WO2021004031A1 PCT/CN2019/129032 CN2019129032W WO2021004031A1 WO 2021004031 A1 WO2021004031 A1 WO 2021004031A1 CN 2019129032 W CN2019129032 W CN 2019129032W WO 2021004031 A1 WO2021004031 A1 WO 2021004031A1
Authority
WO
WIPO (PCT)
Prior art keywords
polymerization
box
pipe
fixedly connected
polymerization device
Prior art date
Application number
PCT/CN2019/129032
Other languages
English (en)
French (fr)
Inventor
马驰
沈家广
吉增明
Original Assignee
江苏海阳化纤有限公司
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 江苏海阳化纤有限公司 filed Critical 江苏海阳化纤有限公司
Publication of WO2021004031A1 publication Critical patent/WO2021004031A1/zh

Links

Images

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B01J19/0013—Controlling the temperature of the process
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00—Feed or outlet devices; Feed or outlet control devices
    • B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
    • C08G69/08—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from amino-carboxylic acids
    • C08G69/14—Lactams
    • C08G69/16—Preparatory processes

Definitions

  • the invention relates to the technical field of agricultural machinery, in particular to a low melting resistance and high spinnability ultra-low viscosity nylon 6 chip polymerization device and an operation method.
  • Nylon “6” chip is a polymer compound made by adding caprolactam as a raw material with a certain amount of additives, polymerizing under certain technological conditions, and through the processes of tape injection, pelletizing, extraction and vacuum drying. It is the main original batch for the production of nylon filament, short yarn, brown yarn, fishing nets and nylon cord. Its poly pick extraction and related equipment are the main technical keys of the product.
  • the nylon sheet is for the production of nylon! Lun silk series products provide a guarantee of raw materials.
  • the relative viscosity of ultra-low viscosity nylon 6 chips is generally lower than 2.0. It is used for polyester/polyamide ultra-fine fiber spinning. The melt resistance is low, the crystallinity is low, and the spinnability is better than medium and high viscosity.
  • nylon 6 high-strength nylon filaments For engineering injection molding, it has good fluidity, strong adaptability to fillers, easy demoulding, unique performance in reducing costs, improving flame retardancy and electrical properties, and the current domestic market demand for nylon 6 high-strength nylon filaments is about 5 100,000 tons/year, related companies mainly use imported products. Now technical personnel in some domestic colleges and universities have not seen reports on in-situ polymerization of nylon 6 anti-UV high-strength nylon colored yarns. I believe that in the near future With the localization of nylon 6 UV-resistant high-strength nylon colored yarns, new applications will continue to appear in its downstream, and potential market demand is expected to be released quickly.
  • the purpose of the present invention is to provide a low melting resistance high spinnability ultra-low viscosity nylon 6 chip polymerization device to solve the above-mentioned background art problems.
  • a low melting resistance, high spinnability, ultra-low viscosity nylon 6 slice polymerization device comprising a polymerization device, a polymerization box and a base, and the polymerization device is fixedly connected with a polymerization device by bolts.
  • a box body, the middle of the lower surface of the polymer box body is fixedly connected with a discharge tube by bolts, the bottom end of the discharging tube penetrates the polymerization device and is threadedly connected with a cover plate, and the middle parts on both sides of the polymer box body near the top end are fixed by bolts
  • the transmission pipe is connected with the first transmission pipe on both sides of the transmission pipe.
  • the upper surface of the base near the four corners are all fixedly connected with electric push rods by bolts.
  • the top ends of the four electric push rods are connected with each other through pin shafts.
  • the aggregating device is rotatably connected, the separated ends of the upper surface of the base are respectively fixedly connected with a controller and a power interface through bolts, the output end of the power interface is electrically connected to the input end of the controller, and the output end of the controller is connected to the The input end of the electric push rod is electrically connected.
  • the base further includes a collection box, the middle of the upper surface of the base is fixedly connected with a collection box by bolts, the height of the collection box is not greater than the length of the four electric push rods, and the collection box is used for As a collection device for the materials in the polymerization tank.
  • the polymerization box body further includes a heating device, and heating devices are fixedly connected with bolts on both sides of the polymerization box body near both ends, and one side of the heating device is fixedly connected to the inner wall of the polymerization device by bolts, One end of the heating device penetrates the polymerization box body and is plugged into the polymerization box body.
  • the heating device is used as a heating and warming device for materials inside the polymerization box body, and the heating device is electrically signaled to the controller.
  • the polymerization device further includes a heat exchange device, the middle of both sides of the inner wall of the polymerization device can be fixedly connected with a heat exchange device by bolts, and one end of the heat exchange device penetrates the polymerization box body and is inserted into the polymerization box body. Then, the other end of the heat exchange device penetrates the polymerization device, the heat exchange device is used as a device for adjusting the internal heat of the polymerization box, and the heat exchange device is electrically signaled to the controller.
  • a heat exchange device the middle of both sides of the inner wall of the polymerization device can be fixedly connected with a heat exchange device by bolts, and one end of the heat exchange device penetrates the polymerization box body and is inserted into the polymerization box body. Then, the other end of the heat exchange device penetrates the polymerization device, the heat exchange device is used as a device for adjusting the internal heat of the polymerization box, and the heat exchange device is electrically signaled to the controller.
  • the polymerization device further includes a deaerator, one end of the deaerator is fixedly connected with a dredging pipe through a bolt and a clip, and the deaerator penetrates the polymerization device through the dredging pipe and is connected to the polymerization box. Plug-in connection, the deaerator is located on both sides of the polymerization device, and the deaerator is electrically signaled to the controller.
  • the polymer box body further includes a first filter screen, a second filter screen; and a third filter screen.
  • the inner wall of the polymer box body is fixedly connected with a first filter screen at both ends by bolts.
  • the inner wall of the polymer box adjacent to the first filter screen is fixedly connected with a second filter screen by bolts, and the inner walls of the polymer box adjacent to the two second filter screens are fixedly connected with a third filter screen by bolts.
  • the pore size of the first filter is not larger than the pore size of the second filter, and the pore size of the second filter is not larger than the pore size of the third filter.
  • the polymerization device further includes a second delivery pipe, the second delivery pipes are screwed on the middle of the polymerization device at both ends near the two ends, and a connecting cover is rotatably connected to one end of the second delivery pipe.
  • One end of the second conveying pipe penetrates the polymerization device and is inserted into the conveying pipe.
  • the first conveying pipe further includes a connecting pipe, one end of the first conveying pipe penetrates the polymerization device and is screwed to the polymerization device, and one end of the first conveying pipe outside the polymerization device passes through a flange
  • a telescopic hose is fixedly connected with the bolt, and one end of the telescopic hose is fixedly connected with a connecting pipe through a flange and the bolt, and the telescopic hose is used as a connecting device between the connecting pipe and the first delivery pipe.
  • the polymerization device is cross-shaped, the base is a regular quadrangular ridge plate, the side length of the base is not less than the length of the polymerization device, and the transfer tube is T-shaped.
  • a method for using an ultra-low viscosity nylon chip polymerization device with low melting resistance and high spinnability includes the following steps:
  • the polymerization device drives the relative angle between the polymerization tank and the horizontal plane, so that the materials inside the polymerization tank can fully react At the same time, it is convenient for users to put in materials;
  • the reactants inside the polymerization box can effectively avoid the appearance of oxides caused by the oxidation reaction when the reaction mass production is carried out, so that the gloss of nylon 6 slices
  • the temperature can be greatly improved and the yellowing caused by the oxidation reaction can be effectively avoided, and the heating device and heat exchange device are provided between the inside of the polymerization device and the polymerization box, so that the reactants can be effectively polymerized during the polymerization.
  • the first conveying pipe and the second conveying pipe provided inside the polymerization device through the conveying pipe enable the two to effectively achieve the interlocking effect, thereby improving the user's flexibility and convenience when batching materials to implement the polymerization reaction and realizing the effective amount.
  • the purpose of production thus effectively makes up for the deficiencies in the existing technology.
  • Fig. 1 is a schematic diagram of the top half-sectional structure of the present invention
  • Figure 2 is a schematic top view of the structure of the present invention.
  • Figure 3 is a schematic view of the left side structure of the present invention.
  • Figure 4 is a schematic diagram of the structure of the present invention in right view
  • FIG. 5 is a connection diagram of the components of the present invention.
  • a low melting resistance high spinnability ultra-low viscosity nylon 6 slice polymerization device including a polymerization device 1, a polymerization box 2 and a base 6, the polymerization device 1
  • the inside of the polymer box 2 is fixedly connected by bolts
  • the polymer box 2 is in the shape of a triangular prism
  • the polymer device 1 is in the shape of a cross
  • both sides of the polymer box 2 are fixedly connected with heating by bolts.
  • one side of the heating device 3 is fixedly connected to the inner wall of the polymerization device 1 through bolts, one end of the heating device 3 penetrates the polymerization box 2 and is plugged into the polymerization box 2, and the heating device 3 is used as A heating and warming device for the materials inside the polymerization tank 2.
  • the heating device 3 is connected to the controller 63 with electrical signals.
  • the heating device 3 can effectively provide the materials inside the polymerization tank 2 with the required reaction temperature to reach an effective temperature
  • the energy supply effect is convenient for the user to control, and the reaction efficiency is improved to achieve the complete reaction effect.
  • the water content and monomer content of the color chip meet the index requirements.
  • the high-speed spinning screw and spinning equipment must be heated and insulated, and the heating time is basically the same.
  • the middle of both sides of the inner wall of the polymerization device 1 can be fixedly connected with a heat exchange device 4 through bolts.
  • One end of the heat exchange device 4 penetrates the polymerization box 2 and is plugged into the polymerization box 2.
  • the heat exchange device 4 The other end runs through the polymerization device 1.
  • the heat exchange device 4 is used as a device for adjusting the internal heat of the polymerization tank 2, and the heat exchange device 4 is electrically connected to the controller 63.
  • the heat exchange device 4 can effectively The thermal energy inside the polymerization device 1 and the polymerization tank 2 can be replaced in a cycle to achieve the repeated cycle of energy and further improve the utilization rate of energy to avoid unnecessary waste.
  • One end of the deaerator 5 is fixed by a bolt and a clip.
  • a dredging pipe is connected.
  • the deaerator 5 penetrates the polymerization device 1 through the dredging pipe and is plugged into the polymerization tank 2.
  • the deaerator 5 is located on both sides of the polymerization device 1. 5 is connected with the electrical signal of the controller 63, and the deaerator 5 can effectively create an oxygen-free space inside the polymerization box 2, so that the reaction materials, namely caprolactam, pigment additives, and antioxidants can effectively avoid oxidation reactions.
  • the reaction effect is reduced, and the reaction is incomplete, thereby effectively improving the reverse efficiency of the nylon 6 slices during polymerization.
  • the middle of the lower surface of the polymerization box 2 is fixedly connected with a discharge tube 24 through a bolt.
  • the bottom end of the polymerization device 1 is threadedly connected with a cover plate, and the discharging pipe 24 can effectively facilitate the user to effectively transfer the fully reacted materials to achieve the effect of cyclic reaction.
  • the middle of the polymerization box 2 is close to the top.
  • a transfer tube 14 is fixedly connected with bolts.
  • the transfer tube 14 is T-shaped. Both sides of the transfer tube 14 are inserted with a first transfer tube 11.
  • One end of the first transfer tube 11 penetrates the polymerization device 1 and is connected with The polymerization device 1 is threadedly connected, one end of the first delivery pipe 11 outside the polymerization device 1 is fixedly connected with a telescopic hose 12 through a flange and a bolt, and one end of the telescopic hose 12 is fixedly connected with a bolt through a flange There is a connecting pipe 13, so The telescopic hose 12 is used as a connecting device between the connecting pipe 13 and the first conveying pipe 11.
  • the second conveying pipe 15 is screwed to the middle of the polymerization device 1 near the two ends.
  • the second conveying pipe 15 A connecting cover is rotatably connected to one end of the periphery.
  • the conveying pipe 14 can effectively realize the pairing of the first conveying pipe 11 and the second conveying pipe 15
  • the connection effect of the transmission and enables the second conveying pipe 15 to effectively achieve a limited effect through the position of the first conveying pipe 11 in the conveying pipe 14, thereby promoting the closing of the second conveying pipe 15 to achieve an interlocking effect, which is effective
  • the inner wall of the polymer box 2 is fixedly connected to the first filter screen 21 by bolts at both ends near the two ends of the first filter screen 21.
  • the inner wall is fixedly connected with a second filter screen 22 by bolts, and the two inner walls of the polymer box adjacent to the second filter screen 22 are fixedly connected with a third filter screen 23 by bolts.
  • the first filter screen 21 has an aperture The size is not greater than the pore size of the second filter 22, the pore size of the second filter 22 is not greater than the pore size of the third filter 23, and it passes through the first filter 21, the second filter 22 and the third filter
  • the net 23 can effectively realize the separation of the reactants inside the polymerization box 2 to improve the reaction effect and promote the effect of more thorough reaction.
  • the upper surface of the base 6 is fixedly connected with electric push rods 61 by bolts at the four corners.
  • the base 6 is in the shape of a regular quadrangular prism, the side length of the base 6 is not less than the length of the polymerization device 1, and the top ends of the four electric push rods 61 are rotatably connected with the polymerization device 1 through pins.
  • the electric push rod 61 can effectively facilitate the user to control the polymerization device 1 to drive the polymerization box 2 to implement the deviation of various angular positions, to promote the further complete reaction of the reactants, and to facilitate the user to put materials and extract the reacted materials.
  • the separated ends of the upper surface of the base 6 are respectively fixedly connected with a controller 63 and a power interface 64 by bolts.
  • the output of the power interface 64 is electrically connected to the input of the controller 63, and the output of the controller 63 is connected to the electric push rod. 61.
  • the input terminal is electrically connected.
  • the middle of the upper surface of the base 6 is fixedly connected with a collection box 62 by bolts.
  • the height of the collection box 62 is not greater than the length of the four electric push rods 61.
  • the collection box 62 is used for Used as a collection device for materials in the polymerization tank 2.
  • a low melting resistance, high spinnability and ultra-low viscosity nylon 6 chip polymerization device including the following steps:
  • the power interface 64 Connect the power interface 64 to the power source, so that the user can start the heating device 3, the heat exchange device 4, and the deaerator 5 through the controller 63, so that the materials inside the polymerization tank 2 can realize energy recovery during the polymerization reaction. Supply and drain, so that the heat inside the polymerization tank 2 can be recycled and reused.
  • the polymerization device 1 drives the relative angle of the polymerization tank 2 to the horizontal plane. The material inside the polymerization box 2 can be fully reacted, and it is convenient for the user to put the material;
  • the polymerized materials can be collected through the collection box 62 above the base 6, so that the materials can be collected through the collection box 62 for protection.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Polymerisation Methods In General (AREA)
  • Polyamides (AREA)

Abstract

一种低熔阻高纺性超低粘尼龙6切片聚合装置，包括聚合装置(1)、聚合箱体(2)以及底座(6)；通过在聚合装置(1)上通过疏通管设有的除氧器(5)，使得聚合箱体(2)内部的反应物在实施反应量产时能够有效的避免氧化反应而造成氧化物的出现，使得尼龙6切片的光泽度得以极大的提升且有效的避免因氧化反应而出现变黄的情况，且通过在聚合装置(1)内部与聚合箱体(2)间设有的加热装置(3)与换热装置(4)，使得反应物实施聚合时能够有效的保证聚合箱体(2)内温度得以获取有效的的循环供热效果，使得反应时温度达到最佳稳定状态而避免反应不完全降低反应物定量生成的情况，从而有效的提高了尼龙6切片的聚合效果，实现有效的量产目的从而有效的弥补了现有技术中的不足。

Description

一种低熔阻高纺性超低粘尼龙6切片聚合装置及操作方法 技术领域
本发明涉及农用机械技术领域，具体为一种低熔阻高纺性超低粘尼龙6切片聚合装置及操作方法。
背景技术
锦纶“6”切片是以己内酰胺为原料加入一定量的助剂，在一定的工艺条件下进行聚合并经注带，切粒、萃取和真空干燥等过程而制成的高分子化合物。它是生产锦纶长丝、短丝、棕丝，渔网及锦纶帘子线等的主要原批其聚镐萃取和有关设备是该产品的主要技术关键，它的主要质量指标为：注带切片平均分子量为12700(标准为；12700\13lOO)，注带单体含量为：8.98％(标准为<10％)，于燥切片平均分子量为14200(标准为13600～14600)，干燥切片含水量≤0.05％(标准为≤0.05％)。该锦纶片为生产锦！纶丝系列产品提供了原料保证，超低粘尼龙6切片相对粘度一般低于2.0，用于涤锦超细纤维纺丝，熔体阻力小，结晶度低，可纺性好于中、高粘品种。用于工程注塑流动性好，对填充剂适应能力强，易脱模，在降低成本，改善阻燃和电性能等方面性能独特优，目前国内锦纶6抗UV高强锦纶丝的市场需求量大约5-10万吨/年，相关企业主要都是采用进口产品，现在国内一些大专院校技术人员尚没有见到对锦纶6抗UV高强锦纶色丝原位聚合进行研究的报道，相信在不久的未来，随着尼龙6抗UV高强锦纶色丝的国产化，它的下游将会不断出现新的应用领域，潜在的市场需求将有望得到快速释放，目前，国内除了日本家公司建有生产尼龙6抗UV高强锦纶丝生产装置外，国内还没有其他企业能够大规模生产，因此提高国内对尼龙6切片实施有效的聚合量产尤为重要，而现有技术中针对尼龙6切片用的聚合装置在实际应用时仍旧存在一定的不足，例如：
现有技术中在对尼龙6切片实施聚合时极易出现氧化反应而降低反应的完全量，使得光泽度大大降低且极易发生变黄情况，且在加热时无法有效的达到循环供热效果使得反应时温度不够稳定而造成反应不完全降低反应物定量生成的情况故而满足不了现有技术所需。
发明内容
本发明的目的在于提供一种低熔阻高纺性超低粘尼龙6切片聚合装置，以解决上述背景技术中提出的问题。
为实现上述目的，本发明提供如下技术方案：一种低熔阻高纺性超低粘尼龙6切片聚合装置，包括聚合装置、聚合箱体以及底座，所述聚合装置内部通过螺栓固定连接有聚合箱体，所述聚合箱体下表面中部通过螺栓固定连接有出料管，所述出料管底端贯穿聚合装置螺纹连接有盖板，所述聚合箱体两侧中部靠近顶端处通过螺栓固定连接有传输管，所述传输管两侧均插接有第一输送管，所述底座上表面靠近四角处均通过螺栓固定连接有电动推杆，四个所述电动推杆顶端通过销轴与所述聚合装置转动连接，所述底座上表面中部相离端通过螺栓分别固定连接有控制器和电源接口，所述电源接口输出端与控制器输入端电性连接，所述控制器输出端与电动推杆输入端电性连接。
优选的，所述底座还包括采集箱，所述底座上表面中部通过螺栓固定连接有采集箱，所述采集箱高度尺寸不大于四个所述电动推杆的长度尺寸，所述采集箱用于作为聚合箱体中物料的收集装置。
优选的，所述聚合箱体还包括加热装置，所述聚合箱体两侧靠近两端处均通过螺栓固定连接有加热装置，所述加热装置一侧通过螺栓与所述聚合装置内壁固定连接，所述加热装置一端贯穿聚合箱体且与聚合箱体插接，所述加热装置用于作为聚合箱体内部物料的供热保暖装置，所述加热装置与所述控制器电信号连接。
优选的，所述聚合装置还包括换热装置，所述聚合装置内壁两侧中部均能通过螺栓固定连接有换热装置，所述换热装置一端贯穿所述聚合箱体且与聚合箱体插接，所述换热装置另一端贯穿聚合装置，所述换热装置用于作为聚合箱体内部热量的调节装置，所述换热装置与所述控制器电信号连接。
优选的，所述聚合装置还包括除氧器，所述除氧器一端通过螺栓与卡件固定连接有疏通管，所述除氧器通过疏通管贯穿所述聚合装置且与所述聚合箱体插接，所述除氧器位于聚合装置的两侧，所述除氧器与所述控制器电信号连接。
优选的，所述聚合箱体还包括第一过滤网、第二过滤网；以及第三过滤网，所述聚合箱体内壁靠近两端处均通过螺栓固定连接有第一过滤网，两个所述第一过滤网相邻面的聚合箱体内壁通过螺栓固定连接有第二过滤网，两个所述第二过滤网相邻面的聚合箱体内壁通过螺栓固定连接有第三过滤网，所述第一过滤网孔径尺寸不大于所述第二过滤网孔径尺寸，所述第二过滤网孔径尺寸不大于所述第三过滤网孔径尺寸。
优选的，所述聚合装置还包括第二输送管，所述聚合装置两侧中部靠近两端处均螺纹连接有第二输送管，所述第二输送管外围一端转动连接有连接罩，所述第二输送管一端贯穿聚合装置与所述传输管插接。
优选的，所述第一输送管还包括连接管，所述第一输送管一端贯穿聚合装置，且与所述聚合装置螺纹连接，所述聚合装置外部的所述第一输送管一端通过法兰与螺栓固定连接有伸缩软管，所述伸缩软管一端通过法兰与螺栓固定连接有连接管，所述伸缩软管用于作为连接管和第一输送管的连接装置。
优选的，所述聚合装置呈十字型，所述底座呈正四棱板型，所述底座边长尺寸不小于所述聚合装置长度尺寸，所述传输管呈T型。
优选的，一种低熔阻高纺性超低粘尼龙切片聚合装置的使用方法，包括以下步骤：
S1、先将底座安装固定在所需使用的方位，通过连接管将第一输送管与外部所需投放的物料管道连接，使得用户得以通过连接管、伸缩软管和第一输送管将物料投放至聚合装置内，并通过传输管输送至聚合箱体中，通过第二输送管将另一类别的物料通过传输管投放至聚合箱体中，通过调节第一输送管在传输管内的位置，使得第二输送管的输送启停得以通过第一输送管在传输管内的位置实施控制即可；
S2、将电源接口接通电源，使得用户得以通过控制器启动加热装置、换热装置以及除氧器，使得聚合箱体内部的物料在进行聚合反应时，能够实现能量的供给与疏导，使得聚合箱体内部的热量得以实现循环再利用即可，通过调节相邻两个电动推杆的伸长量来控制聚合装置带动聚合箱体与水平面的相对角度，使得聚合箱体内部的物料得以充分反应的同时也便于用户投放物料即可；
S3、通过开启出料管底端的盖板使得聚合后的物料得以通过底座上方的采集箱实施集中收集，使得物料得以通过采集箱实施防护采集即可。
与现有技术相比，本发明的有益效果是：
本发明通过在聚合装置上通过疏通管设有的除氧器，使得聚合箱体内部的反应物在实施反应量产时能够有效的避免氧化反应而造成氧化物的出现，使得尼龙6切片的光泽度得以极大的提升且有效的避免因氧化反应而出现变黄的情况，且通过在聚合装置内部与聚合箱体间设有的加热装置与换热装置，使得反应物实施聚合时能够有效的保证聚合箱体内温度得以获取有效的的循环供热效果，使得反应时温度达到最佳稳定状态而避免反应不完全降低反应物定量生成的情况，从而有效的提高了尼龙6切片的聚合效果，同时通过在聚合装置内部通过传输管设有的第一输送管与第二输送管使得二者得以有效的实现互锁效果进而提高用户在批量投放物料实施聚合反应时得以更加灵活便捷进而实现有效的量产目的从而有效的弥补了现有技术中的不足。
附图说明
图1为本发明俯视半剖结构示意图；
图2为本发明俯视结构示意图；
图3为本发明左视结构示意图；
图4为本发明右视结构示意图；
图5为本发明元器件连接图。
图中：1-聚合装置；11-第一输送管；12-伸缩软管；13-连接管；14-传输管；15-第二输送管；2-聚合箱体；21-第一过滤网；22-第二过滤网；23-第三过滤网；24-出料管；3-加热装置；4-换热装置；5-除氧器；6-底座；61-电动拖杆；62-采集箱；63-控制器；64-电源接口。
具体实施方式
下面将结合本发明实施例中的附图，对本发明实施例中的技术方案进行清楚、完整地描述，显然，所描述的实施例仅仅是本发明一部分实施例，而不是全部的实施例。基于本 发明中的实施例，本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例，都属于本发明保护的范围。
请参阅图1-5，本发明提供一种技术方案：一种低熔阻高纺性超低粘尼龙6切片聚合装置，包括聚合装置1、聚合箱体2以及底座6，所述聚合装置1内部通过螺栓固定连接有聚合箱体2，所述聚合箱体2呈三棱柱型，所述聚合装置1呈十字型，所述聚合箱体2两侧靠近两端处均通过螺栓固定连接有加热装置3，所述加热装置3一侧通过螺栓与所述聚合装置1内壁固定连接，所述加热装置3一端贯穿聚合箱体2且与聚合箱体2插接，所述加热装置3用于作为聚合箱体2内部物料的供热保暖装置，所述加热装置3与所述控制器63电信号连接，通过加热装置3能够有效的为聚合箱体2内部提供物料所需反应的温度达到有效的供能效果，且方便用户控制便于提高反应效率达到完全反应的效果，色切片含水、含单体量达到指标要求，高速纺丝螺杆、纺丝设备要进行加热、保温，各加热时间基本相同，所述聚合装置1内壁两侧中部均能通过螺栓固定连接有换热装置4，所述换热装置4一端贯穿所述聚合箱体2且与聚合箱体2插接，所述换热装置4另一端贯穿聚合装置1，所述换热装置4用于作为聚合箱体2内部热量的调节装置，所述换热装置4与所述控制器63电信号连接，通过换热装置4能够有效的将聚合装置1与聚合箱体2内部的热能实现循环更换的效果，达到能量的重复循环进而进一步提高能源的利用率避免不必要的浪费情况，所述除氧器5一端通过螺栓与卡件固定连接有疏通管，所述除氧器5通过疏通管贯穿所述聚合装置1且与所述聚合箱体2插接，所述除氧器5位于聚合装置1的两侧，所述除氧器5与所述控制器63电信号连接，通过除氧器5能够有效的为聚合箱体2内部创造无氧空间，使得反应物料即己内酰胺、颜料助剂、抗氧剂得以有效的避免氧化反应而降低反应效果出现反应不完全的情况，进而有效的提高尼龙6切片在聚合时的反向效率，所述聚合箱体2下表面中部通过螺栓固定连接有出料管24，所述出料管24底端贯穿聚合装置1螺纹连接有盖板，通过出料管24能够有效的方便用户将反应完全的物料实施有效的传输从而达到循环反应的效果，所述聚合箱体2两侧中部靠近顶端处通过螺栓固定连接有传输管14，所述传输管14呈T型，所述传输管14两侧均插接有第一输送管11，所述 第一输送管11一端贯穿聚合装置1，且与所述聚合装置1螺纹连接，所述聚合装置1外部的所述第一输送管11一端通过法兰与螺栓固定连接有伸缩软管12，所述伸缩软管12一端通过法兰与螺栓固定连接有连接管13，所述伸缩软管12用于作为连接管13和第一输送管11的连接装置，所述聚合装置1两侧中部靠近两端处均螺纹连接有第二输送管15，所述第二输送管15外围一端转动连接有连接罩，所述第二输送管15一端贯穿聚合装置1与所述传输管14插接，通过传输管14能够有效的实现第一输送管11与第二输送管15对物料传输的连接效果，且使得第二输送管15得以有效的通过第一输送管11在传输管14内的位置实现限定的效果，进而促使对第二传输管15实施闭合达到互锁的效果，有效的提高用户在投放物料时的投放效果，所述聚合箱体2内壁靠近两端处均通过螺栓固定连接有第一过滤网21，两个所述第一过滤网21相邻面的聚合箱体2内壁通过螺栓固定连接有第二过滤网22，两个所述第二过滤网22相邻面的聚合箱体2内壁通过螺栓固定连接有第三过滤网23，所述第一过滤网21孔径尺寸不大于所述第二过滤网22孔径尺寸，所述第二过滤网22孔径尺寸不大于所述第三过滤网23孔径尺寸，通过第一过滤网21、第二过滤网22和第三过滤网23能够有效的实现聚合箱体2内部的反应物得以有效的实现分隔而提高反应效果促使反应更加彻底的效果，所述底座6上表面靠近四角处均通过螺栓固定连接有电动推杆61，所述底座6呈正四棱板型，所述底座6边长尺寸不小于所述聚合装置1长度尺寸，四个所述电动推杆61顶端通过销轴与所述聚合装置1转动连接，通过四个电动推杆61能够有效的方便用户操控聚合装置1带动聚合箱体2实施各角度位置的偏移，促使反应物进一步完全反应的目的，且方便用户投放物料与提取反应后的物料，所述底座6上表面中部相离端通过螺栓分别固定连接有控制器63和电源接口64，所述电源接口64输出端与控制器63输入端电性连接，所述控制器63输出端与电动推杆61输入端电性连接，所述底座6上表面中部通过螺栓固定连接有采集箱62，所述采集箱62高度尺寸不大于四个所述电动推杆61的长度尺寸，所述采集箱62用于作为聚合箱体2中物料的收集装置。
工作原理：一种低熔阻高纺性超低粘尼龙6切片聚合装置，包括以下步骤：
S1、先将底座6安装固定在所需使用的方位，通过连接管13将第一输送管11与外部 所需投放的物料管道连接，使得用户得以通过连接管13、伸缩软管12和第一输送管11将物料投放至聚合装置1内，并通过传输管14输送至聚合箱体2中，通过第二输送管15将另一类别的物料通过传输管14投放至聚合箱体2中，通过调节第一输送管11在传输管14内的位置，使得第二输送管15的输送启停得以通过第一输送管11在传输管14内的位置实施控制即可；
S2、将电源接口64接通电源，使得用户得以通过控制器63启动加热装置3、换热装置4以及除氧器5，使得聚合箱体2内部的物料在进行聚合反应时，能够实现能量的供给与疏导，使得聚合箱体2内部的热量得以实现循环再利用即可，通过调节相邻两个电动推杆61的伸长量来控制聚合装置1带动聚合箱体2与水平面的相对角度，使得聚合箱体2内部的物料得以充分反应的同时也便于用户投放物料即可；
S3、通过开启出料管24底端的盖板使得聚合后的物料得以通过底座6上方的采集箱62实施集中收集，使得物料得以通过采集箱62实施防护采集即可。
需要说明的是，在本文中，诸如第一和第二等之类的关系术语仅仅用来将一个实体或者操作与另一个实体或操作区分开来，而不一定要求或者暗示这些实体或操作之间存在任何这种实际的关系或者顺序。而且，术语“包括”、“包含”或者其任何其他变体意在涵盖非排他性的包含，从而使得包括一系列要素的过程、方法、物品或者设备不仅包括那些要素，而且还包括没有明确列出的其他要素，或者是还包括为这种过程、方法、物品或者设备所固有的要素。
尽管已经示出和描述了本发明的实施例，对于本领域的普通技术人员而言，可以理解在不脱离本发明的原理和精神的情况下可以对这些实施例进行多种变化、修改、替换和变型，本发明的范围由所附权利要求及其等同物限定。

Claims (10)

  1. 一种低熔阻高纺性超低粘尼龙6切片聚合装置，其特征在于，包括：
    聚合装置(1)；
    聚合箱体(2)；以及底座(6)，所述聚合装置(1)内部通过螺栓固定连接有聚合箱体(2)，所述聚合箱体(2)下表面中部通过螺栓固定连接有出料管(24)，所述出料管(24)底端贯穿聚合装置(1)螺纹连接有盖板，所述聚合箱体(2)两侧中部靠近顶端处通过螺栓固定连接有传输管(14)，所述传输管(14)两侧均插接有第一输送管(11)；
    所述底座(6)上表面靠近四角处均通过螺栓固定连接有电动推杆(61)，四个所述电动推杆(61)顶端通过销轴与所述聚合装置(1)转动连接，所述底座(6)上表面中部相离端通过螺栓分别固定连接有控制器(63)和电源接口(64)，所述电源接口(64)输出端与控制器(63)输入端电性连接，所述控制器(63)输出端与电动推杆(61)输入端电性连接。
  2. 根据权利要求1所述的一种低熔阻高纺性超低粘尼龙6切片聚合装置，其特征在于：所述底座(6)还包括：
    采集箱(62)；
    其中，所述底座(6)上表面中部通过螺栓固定连接有采集箱(62)，所述采集箱(62)高度尺寸不大于四个所述电动推杆(61)的长度尺寸，所述采集箱(62)用于作为聚合箱体(2)中物料的收集装置。
  3. 根据权利要求1所述的一种低熔阻高纺性超低粘尼龙6切片聚合装置，其特征在于：所述聚合箱体(2)还包括：
    加热装置(3)；
    其中，所述聚合箱体(2)两侧靠近两端处均通过螺栓固定连接有加热装置(3)，所述加热装置(3)一侧通过螺栓与所述聚合装置(1)内壁固定连接，所述加热装置(3)一端贯穿聚合箱体(2)且与聚合箱体(2)插接，所述加热装置(3)用于作为聚合箱体(2)内部物料的供热保暖装置；
    其中，所述加热装置(3)与所述控制器(63)电信号连接。
  4. 根据权利要求1所述的一种低熔阻高纺性超低粘尼龙6切片聚合装置，其特征在于：所述聚合装置(1)还包括：
    换热装置(4)；
    其中，所述聚合装置(1)内壁两侧中部均能通过螺栓固定连接有换热装置(4)，所述换热装置(4)一端贯穿所述聚合箱体(2)且与聚合箱体(2)插接，所述换热装置(4)另一端贯穿聚合装置(1)，所述换热装置(4)用于作为聚合箱体(2)内部热量的调节装置；
    其中，所述换热装置(4)与所述控制器(63)电信号连接。
  5. 根据权利要求1所述的一种低熔阻高纺性超低粘尼龙6切片聚合装置，其特征在于：所述聚合装置(1)还包括：
    除氧器(5)；
    其中，所述除氧器(5)一端通过螺栓与卡件固定连接有疏通管，所述除氧器(5)通过疏通管贯穿所述聚合装置(1)且与所述聚合箱体(2)插接，所述除氧器(5)位于聚合装置(1)的两侧；
    其中，所述除氧器(5)与所述控制器(63)电信号连接。
  6. 根据权利要求1所述的一种低熔阻高纺性超低粘尼龙6切片聚合装置，其特征在于：所述聚合箱体(2)还包括：
    第一过滤网(21)；
    第二过滤网(22)；以及第三过滤网(23)；
    其中，所述聚合箱体(2)内壁靠近两端处均通过螺栓固定连接有第一过滤网(21)，两个所述第一过滤网(21)相邻面的聚合箱体(2)内壁通过螺栓固定连接有第二过滤网(22)，两个所述第二过滤网(22)相邻面的聚合箱体(2)内壁通过螺栓固定连接有第三过滤网(23)；
    其中，所述第一过滤网(21)孔径尺寸不大于所述第二过滤网(22)孔径尺寸，所述第二过滤网(22)孔径尺寸不大于所述第三过滤网(23)孔径尺寸。
  7. 根据权利要求1所述的一种低熔阻高纺性超低粘尼龙6切片聚合装置，其特征在于：所述聚合装置(1)还包括：
    第二输送管(15)；
    其中，所述聚合装置(1)两侧中部靠近两端处均螺纹连接有第二输送管(15)，所述第二输送管(15)外围一端转动连接有连接罩，所述第二输送管(15)一端贯穿聚合装置(1)与所述传输管(14)插接。
  8. 根据权利要求1所述的一种低熔阻高纺性超低粘尼龙6切片聚合装置，其特征在于：所述第一输送管(11)还包括：
    连接管(13)；
    其中，所述第一输送管(11)一端贯穿聚合装置(1)，且与所述聚合装置(1)螺纹连接，所述聚合装置(1)外部的所述第一输送管(11)一端通过法兰与螺栓固定连接有伸缩软管(12)，所述伸缩软管(12)一端通过法兰与螺栓固定连接有连接管(13)，所述伸缩软管(12)用于作为连接管(13)和第一输送管(11)的连接装置。
  9. 根据权利要求1所述的一种低熔阻高纺性超低粘尼龙6切片聚合装置，其特征在于：所述聚合装置(1)呈十字型，所述底座(6)呈正四棱板型，所述底座(6)边长尺寸不小于所述聚合装置(1)长度尺寸，所述传输管(14)呈T型。
  10. 根据权利要求1所述的一种低熔阻高纺性超低粘尼龙6切片聚合装置的使用方法，其特征在于：包括以下步骤：
    S1、先将底座(6)安装固定在所需使用的方位，通过连接管(13)将第一输送管(11)与外部所需投放的物料管道连接，使得用户得以通过连接管(13)、伸缩软管(12)和第一输送管(11)将物料投放至聚合装置(1)内，并通过传输管(14)输送至聚合箱体(2)中，通过第二输送管(15)将另一类别的物料通过传输管(14)投放至聚合箱体(2)中，通过调节第一输送管(11)在传输管(14)内的位置，使得第二输送管(15)的输送启停得以通过第一输送管(11)在传输管(14)内的位置实施控制即可；
    S2、将电源接口(64)接通电源，使得用户得以通过控制器(63)启动加热装置(3)、换热装置(4)以及除氧器(5)，使得聚合箱体(2)内部的物料在进行聚合反应时，能够实现能量的供给与疏导，使得聚合箱体(2)内部的热量得以实现循环再利用即可，通过调节相邻两个电动推杆(61)的伸长量来控制聚合装置(1)带动聚合箱体(2)与水平面的相对角度，使得聚合箱体(2)内部的物料得以充分反应的同时也便于用户投放物料即可；
    S3、通过开启出料管(24)底端的盖板使得聚合后的物料得以通过底座(6)上方的采集箱(62)实施集中收集，使得物料得以通过采集箱(62)实施防护采集即可。
PCT/CN2019/129032 2019-07-05 2019-12-27 一种低熔阻高纺性超低粘尼龙6切片聚合装置及操作方法 WO2021004031A1 (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CN201910601394.9 2019-07-05
CN201910601394.9A CN110385093A (zh) 2019-07-05 2019-07-05 一种低熔阻高纺性超低粘尼龙6切片聚合装置及操作方法

Publications (1)

Publication Number Publication Date
WO2021004031A1 true WO2021004031A1 (zh) 2021-01-14

Family

ID=68286232

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/CN2019/129032 WO2021004031A1 (zh) 2019-07-05 2019-12-27 一种低熔阻高纺性超低粘尼龙6切片聚合装置及操作方法

Country Status (2)

Country Link
CN (1) CN110385093A (zh)
WO (1) WO2021004031A1 (zh)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113771370A (zh) * 2021-09-02 2021-12-10 刁海强 一种用于口罩无纺布的切片熔融一体式加工系统

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110385093A (zh) * 2019-07-05 2019-10-29 江苏海阳化纤有限公司 一种低熔阻高纺性超低粘尼龙6切片聚合装置及操作方法

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH1160730A (ja) * 1997-08-20 1999-03-05 Toray Ind Inc ナイロン６の製造方法および重合装置
JP2000327774A (ja) * 1999-05-19 2000-11-28 Toray Ind Inc ナイロン樹脂の製造方法
CN207907674U (zh) * 2018-02-11 2018-09-25 长乐力恒锦纶科技有限公司 一种切片处理的换热节能装置
CN108570148A (zh) * 2018-06-07 2018-09-25 聊城市鲁西化工工程设计有限责任公司 一种防氧化的尼龙6切片聚合生产装置及方法
CN109400872A (zh) * 2017-08-15 2019-03-01 展颂股份有限公司 固态聚合尼龙66的方法及其系统
CN208843975U (zh) * 2018-10-09 2019-05-10 青岛康威化纤有限公司 一种新型pa66固相聚合系统
CN110385093A (zh) * 2019-07-05 2019-10-29 江苏海阳化纤有限公司 一种低熔阻高纺性超低粘尼龙6切片聚合装置及操作方法

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101195681B (zh) * 2007-12-29 2010-05-19 中蓝晨光化工研究院有限公司 一种用于芳纶ⅱ聚合的混合器
CN201140046Y (zh) * 2007-12-29 2008-10-29 中蓝晨光化工研究院有限公司 用于高温差快速反应的物料混合器
CN102391452B (zh) * 2011-10-18 2012-12-05 江阴中绿化纤工艺技术有限公司 氨纶连续聚合生产的反应器进料管
CN205340768U (zh) * 2015-12-18 2016-06-29 上海上萃精细化工有限公司 一种反应余热利用装置
CN107262003B (zh) * 2017-07-27 2019-03-15 惠州大亚湾海科发实业有限公司 一种自动倾倒式反应釜
CN207159126U (zh) * 2017-08-29 2018-03-30 扬州瑞邦化工技术有限公司 一种尼龙聚合反应试验装置
CN208340697U (zh) * 2018-05-24 2019-01-08 汶川县湘宁氯酸盐有限责任公司 一种化工反应罐多功能支架
CN108579649A (zh) * 2018-06-28 2018-09-28 钦州学院 抽入搅拌混合式反应装置
CN108607493A (zh) * 2018-07-19 2018-10-02 郑州大学 一种化工生产用便于调节温度的反应装置
CN109012528B (zh) * 2018-08-14 2024-03-08 无锡创彩光学材料有限公司 一种管式反应器及用其制备单分散聚酰胺酸溶液的方法
CN109482105A (zh) * 2018-10-26 2019-03-19 惠州市强茂化工科技有限公司 具有切换进料管道功能的丙烯酸反应釜
CN210545043U (zh) * 2019-07-05 2020-05-19 江苏海阳化纤有限公司 一种低熔阻高纺性超低粘尼龙6切片聚合装置

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH1160730A (ja) * 1997-08-20 1999-03-05 Toray Ind Inc ナイロン６の製造方法および重合装置
JP2000327774A (ja) * 1999-05-19 2000-11-28 Toray Ind Inc ナイロン樹脂の製造方法
CN109400872A (zh) * 2017-08-15 2019-03-01 展颂股份有限公司 固态聚合尼龙66的方法及其系统
CN207907674U (zh) * 2018-02-11 2018-09-25 长乐力恒锦纶科技有限公司 一种切片处理的换热节能装置
CN108570148A (zh) * 2018-06-07 2018-09-25 聊城市鲁西化工工程设计有限责任公司 一种防氧化的尼龙6切片聚合生产装置及方法
CN208843975U (zh) * 2018-10-09 2019-05-10 青岛康威化纤有限公司 一种新型pa66固相聚合系统
CN110385093A (zh) * 2019-07-05 2019-10-29 江苏海阳化纤有限公司 一种低熔阻高纺性超低粘尼龙6切片聚合装置及操作方法

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113771370A (zh) * 2021-09-02 2021-12-10 刁海强 一种用于口罩无纺布的切片熔融一体式加工系统
CN113771370B (zh) * 2021-09-02 2023-11-03 徐州市康农消毒技术研究院有限公司 一种用于口罩无纺布的切片熔融一体式加工系统

Also Published As

Publication number Publication date
CN110385093A (zh) 2019-10-29

Similar Documents

Publication Publication Date Title
WO2021004031A1 (zh) 一种低熔阻高纺性超低粘尼龙6切片聚合装置及操作方法
CN204289633U (zh) 一种用于铅酸蓄电池内化成的冷却水循环系统
CN201165050Y (zh) 瓶胚加温热风抽送系统
CN106903855B (zh) 一种高效双螺杆化纤挤压机
CN104451949B (zh) 纳米纤维素晶须增强聚氧亚甲基纤维的制备方法
CN206320995U (zh) 用于药物生产的微波真空干燥柜冷却水循环系统
CN205965747U (zh) 高效造粒机
CN201099711Y (zh) 高模高强聚乙烯纤维双风道牵伸热箱
CN210545043U (zh) 一种低熔阻高纺性超低粘尼龙6切片聚合装置
CN213570319U (zh) 一种防水卷材改性沥青生产设备
CN109162058B (zh) 一种燃气红外线定型机
CN209395211U (zh) 一种塑胶成型冷却装置
CN209126124U (zh) 一种塑料模具冷却降温装置
CN210419269U (zh) 一种制备长晶级初级氧化硼的系统
CN104213210A (zh) 高强高模聚乙烯纤维牵伸热箱中的加热结构
CN206748862U (zh) 一种钢塑管高效注气装置
CN207019437U (zh) 一种仲钨酸铵干燥设备
CN104213219A (zh) 用于高强高模聚乙烯纤维牵伸热箱的甬道结构
CN206201342U (zh) 绿色环保塑料日用品注塑机智能进料仓
CN204625554U (zh) 一种滞留塔具有电伴持温加热的改质沥青生产系统
CN220269844U (zh) 一种纺织品高效烘干装置
CN206011693U (zh) 挤压机平移式降温台
CN203999940U (zh) 日晒牢度1000h涤纶丝的生产设备
CN206631592U (zh) 一种聚羧酸减水剂粉剂生产设备
CN104213221A (zh) 一种聚乙烯纤维牵伸热箱

Legal Events

Date Code Title Description
121 Ep: the epo has been informed by wipo that ep was designated in this application

Ref document number: 19937206

Country of ref document: EP

Kind code of ref document: A1

122 Ep: pct application non-entry in european phase

Ref document number: 19937206

Country of ref document: EP

Kind code of ref document: A1