WO2020235941A1 - Spray composition for improving scalp health containing eoseongcho component - Google Patents

Spray composition for improving scalp health containing eoseongcho component Download PDF

Info

Publication number
WO2020235941A1
WO2020235941A1 PCT/KR2020/006632 KR2020006632W WO2020235941A1 WO 2020235941 A1 WO2020235941 A1 WO 2020235941A1 KR 2020006632 W KR2020006632 W KR 2020006632W WO 2020235941 A1 WO2020235941 A1 WO 2020235941A1
Authority
WO
WIPO (PCT)
Prior art keywords
eoseongcho
weight
parts
extract
spray
Prior art date
Application number
PCT/KR2020/006632
Other languages
French (fr)
Korean (ko)
Inventor
양숙현
Original Assignee
농업회사법인 주식회사 용추
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 농업회사법인 주식회사 용추 filed Critical 농업회사법인 주식회사 용추
Priority to JP2021566333A priority Critical patent/JP7315986B2/en
Publication of WO2020235941A1 publication Critical patent/WO2020235941A1/en

Links

Images

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04Dispersions; Emulsions
    • A61K8/046Aerosols; Foams
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/42Amides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/58Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/82Preparation or application process involves sonication or ultrasonication

Definitions

  • the present invention relates to a spray composition for improving scalp health comprising a component of Eoseongcho, and more specifically, Eoseongcho, which can not only fix hair to express various styles, but also contain natural extracts to have healthy scalp and hair. It relates to a spray composition for improving scalp health comprising an ingredient.
  • hair spray is a liquid spray product for stably setting in a state of temporarily changing the shape of the hair.It is widely used in modern times and contains setting polymers, solvents, plasticizers, moisturizers, and fragrances. It is used to provide sufficient moisturizing effect to the skin and to keep the shape of the trimmed hair for a long time.
  • silicone plasticizers for moisturizing ingredients are added together with a neutralizing agent, but adding a plasticizing ingredient has the effect of softening the hair, but lowering the setting power to maintain the shape of the hair.
  • a cationic surfactant can be used to keep the hair flexible while exhibiting a certain level of setting effect, but the surfactant was difficult to combine due to the problem of compatibility with liquefied petroleum gases such as propane and butane, and spray products with aerosols Since it was not possible to use, the proposal of a spray product with good flexibility and setting power was urgently required.
  • Patent Document 0001 Korean Patent Publication No. 10-2011-0041023 (published on April 21, 2011)
  • Patent Document 0002 Domestic registered patent No. 10-1792747 (registered on October 26, 2017)
  • Patent Document 0003 Korean Patent Publication No. 10-2013-0010746 (published on January 29, 2013)
  • the present invention provides a spray composition for improving scalp health including Eoseongcho ingredients including Eoseongcho ingredients capable of not only fixing hair to express various styles, but also containing natural extracts to have healthy scalp and hair. .
  • the spray composition for improving scalp health comprising the Eoseongcho component according to the present invention contains Eoseongcho extract as a main component.
  • Eoseongcho extract In addition to the Eoseongcho extract, ethanol, Panthenol, Sodium Dehydroacetate, Propylene Glycol, Sulfur (surfur), Zinc Gluconate, Magnesium Gluconate, Camellia Oil, dimethicone, methacryloyl ethyl betaine (Methacryloyl Ethyl Betaine) and flavoring may be included.
  • the composition is Eoseongcho extract 1 to 5 parts by weight, ethanol 60 to 80 parts by weight, Panthenol 05 to 15 parts by weight, Sodium Dehydroacetate 01 to 1 part by weight, Propylene Glycol 03 to 08 Parts by weight, sulfur (surfur) 01 to 05 parts by weight, zinc gluconate 001 to 003 parts by weight, magnesium gluconate 005 to 01 parts by weight, camellia oil 0005 to 003 parts by weight, dimethicone ( Dimethicone) 0025 to 0055 parts by weight, methacryloyl ethyl betaine (Methacryloyl Ethyl Betaine) 005 to 01 parts by weight, and fragrance 0005 to 001 parts by weight may be included in a weight ratio.
  • the Eoseongcho extract is washed after preparing Eoseongcho, and the washed Eoseongcho is pulverized into a certain particle size, and the crushed Eoseongcho is pulverized so that the particle diameter is in the range of 500 to 2500 ⁇ m, and the pulverized Eoseongcho is mixed with a solvent.
  • the mixture was added to an ultrasonic extractor to apply ultrasonic waves to the mixed solution to prepare an Eoseongcho extract mixture, the solvent being mixed in a weight ratio of 1000 to 2000 parts by weight based on 100 parts by weight of the pulverized Eoseongcho, and the solvent
  • any one or more solvents selected from water or alcohols having 1 to 4 carbon atoms are used, and the ultrasonic waves applied to the mixture under a temperature of 20 to 25°C and a pressure of 01 to 05kgf/cm2 are 30 to 50KHz at a vibration frequency of 30 to 50KHz. It is extracted using an output of 100 to 200 watts for 60 minutes, and may be prepared by aging for 1 to 3 hours at a temperature of 10 to 20°C after removing the solids from the Eoseongcho extract mixture.
  • a fermented wild wild ginseng extract may be further included, and the fermented wild wild ginseng extract may be included in a weight ratio of 10 to 30 parts by weight based on 100 parts by weight of the Eoseongcho extract.
  • the present invention provides a spray for improving scalp health comprising the above composition.
  • the scalp health improvement spray composition containing the Eoseongcho component according to the present invention not only fixes the hair to create a variety of styles, but also contains natural extracts to prepare a scalp health improvement spray that can have a healthy scalp and hair. can do.
  • 1A is a photograph showing a subject's scalp.
  • 1B is a photograph showing the scalp of the subject after spraying and shampooing the hair of the subject by spraying and shampooing the spray prepared according to Example 1 at 15 ml a day for 20 days.
  • providing scalp health refers to soothing the scalp and beautifying the hair to increase attractiveness and keep the hair healthy.
  • the spray composition for improving scalp health comprising the Eoseongcho component according to the present invention includes Eoseongcho extract, ethanol, Panthenol, Sodium Dehydroacetate, Propylene Glycol, sulfur (surfur), and zinc gluconate. (Zinc Gluconate), Magnesium Gluconate, Camellia Oil, Dimethicone, Methacryloyl Ethyl Betaine, and Perfume.
  • the spray composition for improving scalp health including the Eoseongcho component according to the present invention is Eoseongcho extract 1 to 5 parts by weight, ethanol 60 to 80 parts by weight, Panthenol 0.5 to 1.5 parts by weight, Sodium Dehydroacetate ) 0.1 to 1 parts by weight, propylene glycol (Propylene Glycol) 0.3 to 0.8 parts by weight, sulfur (surfur) 0.1 to 0.5 parts by weight, zinc gluconate (Zinc Gluconate) 0.01 to 0.03 parts by weight, magnesium gluconate (Magnesium Gluconate) 0.05 To 0.1 parts by weight, camellia oil 0.005 to 0.03 parts by weight, dimethicone 0.025 to 0.055 parts by weight, Methacryloyl Ethyl Betaine 0.05 to 0.1 parts by weight, and 0.005 to 0.01 parts by weight of fragrance It can be included as a percentage.
  • the Eoseongcho extract is prepared by extracting Eoseongcho, and Eoseongcho (Houttuynia cordata thunb) is an outpost of Yakmomil, a plant of the Saururaceae, and lives in Southeast Asia and particularly Japan and Korea.
  • Eoseongcho is also called Sip-Yak because it has ten medicinal effects, and the stem is like a sweet potato leaf, and it is also called Eoseongcho because it originates from the fact that when you touch the raw leaves, fish smells badly.
  • Eoseongcho is also available for medicinal and edible use. It is classified as animals and plants that can only be used in a minimum amount as an auxiliary ingredient in the classification of food raw materials in the food code. Pharmacologically, it is widely known for its strong heart, diuretic, antibacterial, detoxifying and anticancer efficacy Is used as a cosmetic and health functional food that helps detoxification and beauty.
  • Eoseongcho extract prepared by the following manufacturing method may be used as the extract of Eoseongcho.
  • the washed Eoseongcho may be pulverized into a certain particle size.
  • the active ingredient of the Eoseongcho may be sufficiently extracted by pulverizing the Eoseongcho to a certain particle size, and the crushing of the Eoseongcho may be pulverized so that the particle diameter is in the range of 500 to 2500 ⁇ m.
  • the particle diameter of the Eoseongcho is pulverized to less than 500 ⁇ m, it takes a long time to pulverize, and the particles are too small to cause agglomeration between particles in a later process. It may be difficult to effectively extract useful ingredients from Eoseongcho.
  • the pulverized Eoseongcho may be extracted by applying ultrasonic waves in an atmosphere of low temperature and reduced pressure to prepare a mixed solution for extracting Eoseongcho.
  • the solvent is 100 parts by weight of the pulverized Eoseongcho It is mixed at a weight ratio of 1000 to 2000 parts by weight, and any one or more solvents selected from water or an alcohol having 1 to 4 carbon atoms (C1 to C4) may be used as the solvent.
  • the ultrasonic wave applied to the mixed solution under a temperature of 20 to 25°C and a pressure of 0.1 to 0.5kgf/cm 2 outputs 100 to 200 watts for 30 to 60 minutes at a vibration frequency of 30 to 50 KHz. It can be extracted using
  • the Eoseongcho extract can be prepared by removing solids such as pulverized Eoseongcho from the Eoseongcho extract mixture and then aging for 1 to 3 hours at a temperature of 10 to 20°C.
  • the removal of solids such as crushed Eoseongcho from the Eoseongcho extract mixture may be performed by separating and removing the solids using a known sieve such as a sieve.
  • the ethanol acts as a solvent, and as the solvent evaporates, a film is formed on the surface of the hair, and the hair can be fixed by the strength of the film.
  • the panthenol is used as a conditioning agent and may improve the appearance and feel of the hair, increase flexibility, improve style, impart moisture and gloss, and improve the texture of the hair.
  • the sodium dehydroacetate is used as a bactericidal preservative and may serve to improve the storage stability of a spray composition for improving scalp health including the Eoseongcho component.
  • the chemical formula of the propylene glycol is C 3 H 8 O 2 , the specific gravity is 1.036 ⁇ 1.040, the boiling point is 185 ⁇ 189 °C.
  • the propylene glycol is well mixed with water, alcohol, acetone, ethyl acetate, chloroform, ether, and the like, has excellent solubility, and has good hygroscopicity, and can be used as a moisture evaporation barrier.
  • the propylene glycol can give a moisturizing effect to fixed hair, softly set the hair, and give a conditioning effect.
  • the sulfur occupies the eighth largest proportion of biological elements, and is particularly distributed in bones, skin, and hair.
  • the sulfur occupies the eighth largest proportion of biological elements, and is particularly distributed in bones, skin, and hair.
  • sulfur has an excellent detoxification effect against heavy metals and chemicals
  • bones become strong and bone marrow becomes full (Donguibogam)
  • Donguibogam helps yang, warms the body, and It is said that it strengthens bones (new herbal medicine), strengthens bones, strengthens muscles, and prevents hair loss.
  • this sulfur penetrates into the pores to form cystine proteins, and it is known to prevent hair loss by forming a sulfur chain together with it, and has been added as a component to various hair loss prevention products.
  • Sulfur used in the present invention refers to sulfur from which toxic components have been removed, and the sulfur can perform functions such as pain relief, inflammation removal, transport of active substances, cell regeneration, blood circulation promotion, detoxification and sterilization, etc.
  • a commercially known sulfur may be used as the sulfur, and sulfur having a particle diameter of 10 to 80 nm may be used to further improve the physiological activity and penetration into the body.
  • the zinc gluconate is used as a skin conditioning agent and is effective for inflammatory acne due to its antiviral properties.
  • the zinc gluconate is effective in soothing the irritated scalp and relieving skin itching.
  • the magnesium gluconate is a magnesium salt component of gluconic acid, the chemical formula is C 12 H 22 MgO 14 or C 12 H 22 MgO 14 2H 2 O, the molecular weight is 414.61, and the scalp state is It helps to keep it in a healthy and good condition.
  • the camellia oil is an oil containing a large amount of unsaturated fatty acids, and the oil rarely evaporates even if left unattended, and its specific gravity is about 0.916, which is similar to water.
  • the main fatty acid component is oleic acid, which accounts for about 90%. It is a yellow, clear oil with a low freezing point of 25°C, and is mainly used as a substitute for hair oil, precision machine oil, and olive oil in medicine.
  • the camellia oil prepared by the following method may be used as the camellia oil.
  • the washed camellia seeds may be immersed in grape juice and rancidity inhibitors.
  • the camellia oil produced by immersing the camellia seeds in grape juice and rancidity inhibitor can prevent discoloration or rancidity.
  • the washed camellia seeds can be immersed in a mixture of grape juice and rancidity inhibitor in a ratio of 1:1, and the rancidity inhibitor is mixed with vitamin C and salt solution in a weight ratio of 1:1. Can be manufactured.
  • the grape juice is good for preventing blood clots and preventing adult diseases such as high blood pressure, arteriosclerosis and heart disease, and can help improve memory
  • the salt solution used as the rancidity inhibitor may be a salt solution having a concentration of 1 to 2% by weight
  • the washed camellia seeds may be immersed in a weight ratio of 100 to 120 parts by weight of a mixture of grape juice and rancidity inhibitor with respect to 100 parts by weight of the washed camellia seeds, and then maintained for 10 to 40 minutes.
  • camellia seeds immersed in the mixed solution of the grape juice and rancidity inhibitor may be taken out so that the grape juice and components of the rancidity inhibitor may penetrate into the camellia seeds.
  • a mixture of grape juice and rancidity inhibitor The camellia seeds separated from may be stored at a temperature of 35 to 40° C. for 30 to 60 minutes.
  • camellia seeds into which the components of the grape juice and rancidity inhibitors have penetrated can be steamed.
  • the steaming of the camellia seeds can be performed by steaming the camellia seeds into which the grape juice and rancidity inhibitor components are infiltrated with steam for 30 to 60 minutes. If the steaming of the camellia seeds is performed below the above lower limit, sufficient There is a problem in that steaming is not performed, and when the steaming is performed beyond the upper limit range, the difference in effect according to the increase of the steaming time may be insignificant.
  • the steamed camellia seeds can be dried.
  • Drying of the steamed camellia seeds can be carried out for 10 to 20 hours at a temperature of 30 to 40°C on the steamed camellia seeds, and mechanical drying using a dryer is used to keep the drying temperature of the camellia seeds constant. Can be.
  • the dried camellia seeds may be washed with at least one acid of acetic acid or citric acid.
  • the washing of the dried camellia seeds is effective in improving the flavor and color of camellia oil to be produced through a later fermentation process by washing the surface of the dried camellia seeds with one or more acids of acetic acid or citric acid.
  • the washed camellia seed may be sprayed with a fermentation broth consisting of a culture broth and lactic acid bacteria.
  • lactic acid bacteria any one known lactic acid bacteria selected from the group consisting of lactic acid bacteria ( Lactobacillales ), Streptococcus thermophiles , and Bifidobacterium longum may be used, and the culture medium is peptone , Malt extract, sodium citrate, potassium phosphate dibasic, glucose, and distilled water, and the culture solution is 15 to 25 parts by weight of peptone, malt extract 5 to 15 It may be made by mixing in a weight ratio of 0.5 to 1.5 parts by weight of sodium citrate, 0.1 to 0.3 parts by weight of dibasic potassium phosphate, 1 to 3 parts by weight of glucose, and 100 to 200 parts by weight of distilled water.
  • the peptone is a nitrogen source that supplies protein and supplies proteins necessary for the growth of microorganisms
  • the malt extract contains various minerals, vitamin B groups, and amino acids, so that it can help the growth of microorganisms
  • the sodium citrate Silver is an inorganic substance that maintains a state optimized for the growth of microorganisms by adjusting the pH of the culture medium, and can supply nutrients, and the glucose can function as an important component by which lactic acid bacteria metabolize sugar to produce organic acids.
  • camellia seeds sprayed with the fermentation broth may be fermented.
  • Fermentation of the camellia seeds may be fermented by storing the camellia seeds sprayed with the fermentation broth in a storage container maintaining a temperature of 45 to 50° C. and a humidity of 60 to 65% for 3 to 6 days.
  • the fermented camellia seeds may be dried in cold air.
  • Cold air drying of the fermented camellia seeds may be performed by drying the fermented camellia seeds with cold air at a temperature of 3 to 6° C. for 5 to 10 hours and maintaining the fermented camellia seeds at a temperature of 55 to 60° C. for 1 to 3 days.
  • camellia seed oil (camellia seed oil).
  • the dimethicone is used as an emulsifier, and it can improve the mixing properties of the spray composition for improving scalp health including the Eoseongcho component according to the present invention so as to exhibit homogeneous physical properties.
  • the methacryloyl ethyl betaine (Methacryloyl Ethyl Betaine) may be so as to be well dissolved in an ethanol solvent ( ⁇ ), a transparent aromatic alcohol.
  • the fragrance provides the fragrance of the spray composition, and various kinds of known fragrances can be used.
  • natural fragrances extracted from plants can be used to consider the health of the hair or scalp. have.
  • the spray composition for improving scalp health comprising the Eoseongcho component according to the present invention may further include a fermented wild ginseng extract in addition to the composition, wherein the fermented wild wild ginseng extract is 10 to 30 parts by weight based on 100 parts by weight of the Eoseongcho extract. It can be included as a percentage.
  • the fermented wild wild ginseng extract can be prepared using wild wild ginseng roots and wild wild ginseng leaves.
  • the wild wild ginseng contains 10 times more saponin than ginseng and 4 to 5 times more than red ginseng, which has great efficacy in enhancing immunity. , Diabetes prevention, digestion, stress relief, energy enhancement, etc. are effective.
  • the wild wild ginseng fermented extract may be used wild wild ginseng fermented extract prepared by the following manufacturing method.
  • the wild mountain ginseng root and the fresh mountain mountain leaves can be separated and prepared, and then washed.
  • the wild ginseng root can be heated with steam to increase steam and then fumigate with sulfur.
  • the wild ginseng roots are heated with steam for 30 to 100 minutes at a temperature of 130 to 140°C and a pressure of 1 to 3kgf/cm 2 , and then sulfur fumigation is performed on the wild ginseng roots heated with steam for 1 to 3 minutes. I can.
  • the sulfur fumigated wild ginseng roots may be dried for 1 to 3 days at a temperature of 25 to 30°C.
  • the dried wild ginseng root may be cut in units of a predetermined length, for example, the dried wild ginseng root may be cut in a length unit of 0.1 to 1.0 cm.
  • the aging can be aged by maintaining the wild ginseng root mixed with the lactic acid bacteria for 10 to 30 hours at a temperature of 20 to 25 °C.
  • lactic acid bacteria any one known lactic acid bacteria selected from the group consisting of lactic acid bacteria ( Lactobacillales ), Streptococcus thermophiles , and Bifidobacterium longum may be used.
  • the washed wild wild ginseng leaves may be heated with steam.
  • step it may be carried out by heating the wild wild ginseng leaves at 110 to 120°C and a pressure of 1 to 3kgf/cm 2 with steam for 10 to 30 minutes.
  • the fresh wild wild ginseng leaves heated with the steam may be dried.
  • the wild wild wild ginseng leaves may be dried for 5 to 10 hours at a temperature of 25 to 30°C.
  • the dried wild wild ginseng leaves can be heated to roast.
  • the dried wild wild ginseng leaves are put into a heating container (for example, a cauldron) and then first roasted at a temperature of 90 to 95°C for 3 to 5 minutes, and the first roasted wild wild wild ginseng leaves are 130 to 140 At a temperature of °C 30 to 60 seconds may proceed to the step of the second abrasion.
  • a heating container for example, a cauldron
  • the washed wild wild ginseng leaves may be fermented by spraying the Bacteria leachate into the washed wild wild ginseng leaves.
  • the Bacillus leachate is capable of accelerating the fermentation of the dried wild wild ginseng leaves, sprayed at a weight ratio of 30 to 50 parts by weight of the dried wild wild ginseng leaves, and a temperature of 55 to 60°C and 60 to 65 After allowing the% humidity to be maintained, it can be fermented for 2 to 4 days.
  • the Bacillus Bacillus culture medium is produced by mixing Bacillus bacillus and water, and the Bacillus bacillus is grown twice a day at 25°C after mixing 10 to 12% by weight of brown sugar in godubap, placing eco-friendly rice husks on the prepared medium and covering a cloth. It can be cultured for one week while spraying water on the plant to generate Bacillus bacteria, which are re-inoculated in a medium mixed with rice bran and brown sugar at a weight ratio of 50:50, and cultured at 25°C for one week to be used as the Bacillus bacteria leachate used in the present invention. have.
  • Bacillus subtilis Bacillus subtilis
  • Bacillus subtilis spjijepiyi Bacillus subtilis
  • Bacillus megaterium Bacillus megaterium
  • Bacillus licheniformis Bacillus licheniformis
  • Bacillus fulmis Any one or more selected from the group consisting of ( Bacillus pumilus ) may be used.
  • the fermented wild wild ginseng root and the fermented wild wild ginseng leaves are mixed and fermented to prepare a fermented wild wild ginseng mixture.
  • the fermented wild wild ginseng leaves are mixed at a weight ratio of 200 to 400 parts by weight with respect to 100 parts by weight of the aged wild ginseng roots, and then fermented for 3 to 5 days at a temperature of 60 to 65°C and a humidity of 55 to 60%.
  • a fermented wild ginseng mixture is prepared.
  • the fermented wild wild ginseng fermentation broth may be prepared by mixing a solvent with the fermented wild wild ginseng mixture and applying ultrasonic waves.
  • the fermented wild ginseng mixture may be mixed with a solvent to prepare a mixture, and then added to an ultrasonic extractor to apply ultrasonic waves to the mixture to prepare a wild wild ginseng fermentation broth. It is included in a weight ratio of 300 to 500 parts by weight based on parts, and water may be used as the solvent.
  • the ultrasonic wave applied to the mixed solution to prepare the fermented wild ginseng may be extracted using an output of 100 to 200 watts for 50 to 100 minutes at a vibration frequency of 60 to 80 KHz.
  • solids such as wild wild ginseng roots and fresh wild wild ginseng leaves can be removed from the fermented wild ginseng broth.
  • Separation of solids such as wild wild ginseng roots and fresh wild wild ginseng leaves in the above step may be performed using a known strainer such as a sieve.
  • the fermented wild ginseng broth from which the solid content has been removed may be centrifuged.
  • the fermented wild ginseng broth from which solids have been removed by centrifuging the fermented wild ginseng broth from which solids have been removed, it can be separated into a lower layer in which fine particles of wild ginseng roots and fresh leaves are located, and a middle layer and a supernatant located above the lower layer. .
  • the useful ingredient of sanyangsam may prepare a fermented sanyangsam extract.
  • the fermented wild wild ginseng extract is first extracted with 10 to 15 l of a 70% (v/v) ethanol aqueous solution in 2000 to 3000 g of wild wild ginseng fermentation broth at 85 to 90°C for 3 to 4 hours, and then 70% (v/v) ethanol Completing the secondary extraction for 2 to 3 hours at 85 to 90 °C with 4 to 6 l of aqueous solution, and preparing an extract until it becomes 1000 to 1500 ml in a vacuum rotary evaporator; And ethanol is added to the extract, diluted to 2 to 3 times by weight, centrifuged at 18,000 to 20,000 rpm for 30 to 40 minutes to completely remove polymer fibers and solids that may be included in the fermented wild ginseng, and then the collected supernatant is 1.5 to It can be prepared by extracting twice with 2.0 times the weight of acetic acid.
  • the spray composition for improving scalp health comprising the Eoseongcho component according to the present invention may further include an onion extract in addition to the composition, wherein the onion extract is in a weight ratio of 5 to 15 parts by weight based on 100 parts by weight of the Eoseongcho extract. Can be included.
  • the onion extract is prepared by extracting the useful ingredients of onion, and the onion (Allium cepa) is a perennial plant belonging to the lily family, and is used as food, spices and medicinal materials to which a unique taste and aroma are applied along with a long cultivation history.
  • 100g of onion contains 90g of moisture, about 72g of carbohydrates, 11g of protein, 10 to 20mg of vitamin C, calcium, phosphorus, and iron.
  • the onion skin contains 504% sugar, 2924% fiber, 148% fat, and 499% ash. Contains.
  • onions The efficacy of onions is known for antioxidant, lowering blood lipids, antihypertension, anti-inflammatory, antibacterial, anti-tumor, and lowering blood sugar.
  • the main physiologically active substances contained in onions include organic sulfur compounds and flavonoid compounds.
  • onions contain very high quercetin, which exhibits antioxidant activity, compared to other vegetables and fruits.
  • Quercetin is a plant-derived flavonoid-based phenolic compound that is not only a powerful antioxidant, but also has anti-arteriosclerosis, antibacterial activity, cholesterol lowering, anti-cancer, anti-viral and anti-allergic activities, but little toxicity. It is known. Therefore, eating foods containing a lot of quercetin is effective in improving blood circulation, lowering blood pressure and dieting such as diabetes and weight loss, strengthening immune function, inhibiting DNA damage, and inhibiting lipid peroxidation of red blood cell membranes.
  • the onion extract can be prepared by the following manufacturing method.
  • the onion is collected and 1 to 5 minutes with purified water in which sodium hydrogen carbonate (NaHCO 3 ) having a concentration range of 1 to 3 (w/w)% and a temperature of 33 to 37°C is dissolved During washing to remove foreign substances adhering to the onion, the peel of the onion can be separated and separated into onion flesh and onion peel.
  • NaHCO 3 sodium hydrogen carbonate
  • the onion pulp is dried in a dryer, but drying of the onion pulp is performed in a dryer in which a constant temperature and humidity are maintained in order to prevent the chlorophyll of the onion pulp from being destroyed and the inherent flavor of the onion pulp from disappearing when drying in sunlight.
  • the onion flesh may be dried for 3 to 7 hours in a dryer maintained at a temperature of 20 to 25° C. and a humidity of 33 to 40%.
  • the dried onion pulp is mixed with purified water and heated to prepare the onion pulp extract.
  • the onion pulp extract may be prepared by mixing 500 to 1000 parts by weight of purified water with respect to 100 parts by weight of the dried onion pulp and heating at a temperature of 95 to 105°C for 5 to 15 hours.
  • the onion peel can be dried to remove moisture contained in the onion peel, and the onion peel can be dried for 3 to 7 hours in a dryer maintained at 30 to 35°C and 35 to 45% humidity.
  • the moisture contained in the onion skin is gradually and evenly evaporated, so that the inherent aroma and useful ingredients of the onion skin can be more easily extracted.
  • By destroying the cell tissue of the onion skin it facilitates the penetration of air and promotes the fermentation, so that the useful components of the onion skin can be enriched.
  • the dried onion peel is mixed with purified water and then heated to prepare the onion peel extract.
  • the onion peel extract is mixed with 200 to 400 parts by weight of purified water based on 100 parts by weight of the dried onion peel. After immersing for 1 to 3 hours at a temperature of 60 to 70°C, the purified water immersed in the onion skin is added to a heater, and purified water in which the onion skin is immersed in the heater is added to a temperature of 110 to 120°C and inside a pressure vessel
  • the onion peel extract can be prepared by heating for 3 to 5 hours in a pressure range of 2.5 to 3.5kgf/cm 2 .
  • the onion peel is immersed in purified water and then extracted as described above, thereby weakening the plant wall of the onion peel to increase extraction efficiency.
  • an onion extract can be prepared by mixing the onion flesh extract and the onion peel extract, wherein the onion extract is prepared by mixing the onion flesh extract and the onion peel extract in a weight ratio of 7:3 to 6:4. I can.
  • the onion extract may be aged by storing it for 1 to 5 hours at a temperature of 3 to 7°C.
  • the onion extract may be uniformly mixed and the flavor may be enhanced.
  • a spray was prepared using a spray composition included in a weight ratio of 0.008 parts by weight and a fragrance.
  • a spray was prepared using the same composition as in Example 1, but in Example 2, a spray was prepared by further including 20 parts by weight of the fermented wild ginseng extract with respect to 100 parts by weight of the Eoseongcho extract.
  • Soap was prepared using the same composition as in Example 1, and in Example 3, a spray was prepared by further including 10 parts by weight of onion extract with respect to 100 parts by weight of the Eoseongcho extract.
  • a spray was prepared using the same composition as in Example 1, but in Comparative Example 1, Eoseongcho extract and camellia oil were not included.
  • a commercially available spray (manufactured by W company, using a chemical substance) was prepared, and it was used as a spray according to Comparative Example 2.
  • the experiment was conducted on 20 healthy subjects (7 males and 13 females) between the ages of 10 and 50, and the spray was used 15 ml per day for 20 days, and the result was measured by a 5-point scale method. I did.
  • the spray according to Examples 1 to 3 included natural extracts such as Eoseongcho extract, fermented wild ginseng extract, and onion extract, thereby contributing to the improvement of the user's scalp and hair.
  • the stimulation test for the spray prepared as described above was conducted as follows.
  • the stimulation experiment targeted 20 healthy people (7 men, 13 women) between 10 and 50 years old.After the hair shampoo, spray was sprayed onto the hair of the subject, and after 3 hours the scalp condition (erythema, Edema, papules, etc.) were observed, and a qualitative evaluation was performed through an evaluation table as shown in [Table 2] below.
  • the easy cleaning experiment was targeting 20 healthy people (7 men, 13 women) between the ages of 10 and 50 years, and the hair was set by spraying 10 ml of spray onto the hair, and washing with shampoo And washing without using shampoo, and the results are shown in Table 4 below.
  • The hair gel component has been removed to some extent, and after washing, a refreshing feeling is generated.
  • The hair gel component has been removed to some extent, but after washing, there is no refreshing feeling.
  • the hair gel component is hardly removed, and an unpleasant feeling occurs after washing.
  • the spray prepared according to Example 1 was sprayed onto the hair of the subject (35 years old female) to observe the condition of the subject's scalp.
  • FIG. 1A is a photograph showing the scalp of a subject
  • FIG. 1B is a spray prepared according to Example 1 and spraying and shampooing on the subject's hair at 15 ml per day for 20 days, and after 20 days, the scalp of the subject This is a picture showing.

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dispersion Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Cosmetics (AREA)

Abstract

The present invention relates to a spray composition which is for improving scalp health and includes an Eoseongcho component. A spray composition, which is for improving scalp health and includes an Eoseongcho component according to the present invention, comprises: an Eoseongcho extract; ethanol; panthenol; sodium dehydroacetate; propylene glycol; sulfur; zinc gluconate; magnesium gluconate; camellia oil; dimethicone; methacryloyl ethyl betaine; and a fragrance. Due to the abovementioned configuration, the present invention can produce a spray for improving scalp health, wherein the spray makes it possible to wear a variety of hairstyles by fixing hair, and also makes it possible to achieve a healthy scalp and hair by virtue of containing a natural extract.

Description

어성초 성분을 포함하는 두피 건강 개선용 스프레이 조성물Spray composition for improving scalp health containing Eoseongcho ingredients
본 발명은 어성초 성분을 포함하는 두피 건강 개선용 스프레이 조성물에 관한 것으로서, 더욱 상세하게는 모발을 고정하여 다양한 스타일을 연출할 수 있도록 할 뿐만 아니라 천연 추출물이 포함되어 건강한 두피와 모발을 갖도록 할 수 있는 어성초 성분을 포함하는 두피 건강 개선용 스프레이 조성물에 관한 것이다.The present invention relates to a spray composition for improving scalp health comprising a component of Eoseongcho, and more specifically, Eoseongcho, which can not only fix hair to express various styles, but also contain natural extracts to have healthy scalp and hair. It relates to a spray composition for improving scalp health comprising an ingredient.
일반적으로 헤어 스프레이는 모발(毛髮)의 형태를 일시적으로 변화시킨 상태에서 안정적으로 세팅하기 위한 액상의 스프레이 제품으로 현대에는 널리 사용되는 것으로서 셋팅용 폴리머, 용제, 가소제, 보습제 및 향료 등이 함유되어 모발에 충분한 보습효과를 부여하는 한편 손질된 머리의 형태를 장기간 지속적으로 유지할 수 있도록 하는 용도로 사용된다.In general, hair spray is a liquid spray product for stably setting in a state of temporarily changing the shape of the hair.It is widely used in modern times and contains setting polymers, solvents, plasticizers, moisturizers, and fragrances. It is used to provide sufficient moisturizing effect to the skin and to keep the shape of the trimmed hair for a long time.
그러나 일반적인 스프레이 액제를 모발에 분사하면 세팅용 폴리머 용제가 증발함에 따라 모발이 너무 딱딱해지면서 유연성이 저하되어 모발이 부자연스럽게 느껴지는 문제점과 함께 모발에 고형분말이 생성되는 문제점이 발생되었다.However, when a general spray liquid is sprayed on the hair, the hair becomes too hard and the flexibility decreases as the setting polymer solvent evaporates, resulting in a problem that the hair feels unnatural and a solid powder is generated in the hair.
이러한 현상의 방지를 위하여 중화제와 함께 보습성분을 위한 실리콘류의 가소제가 첨가되나, 가소 성분을 첨가하면 모발을 유연하게 하는 효과는 있으나 머리의 형태를 유지하는 세팅력이 저하된다.In order to prevent such a phenomenon, silicone plasticizers for moisturizing ingredients are added together with a neutralizing agent, but adding a plasticizing ingredient has the effect of softening the hair, but lowering the setting power to maintain the shape of the hair.
따라서, 일정수준의 세팅효과를 나타내면서도 모발을 유연하게 유지하기 위하여 양이온 계면활성제를 사용할 수 있으나, 계면활성제는 프로판, 부탄과 같은 액화석유가스와 상용성의 문제로 결합이 어려웠고 에어졸을 적용한 스프레이 제품에는 사용이 불가능하였으므로 유연성과 세팅력이 좋은 스프레이 제품의 제안이 절실히 요구되었다.Therefore, a cationic surfactant can be used to keep the hair flexible while exhibiting a certain level of setting effect, but the surfactant was difficult to combine due to the problem of compatibility with liquefied petroleum gases such as propane and butane, and spray products with aerosols Since it was not possible to use, the proposal of a spray product with good flexibility and setting power was urgently required.
또한, 종래의 헤어 스프레이 제품에는 단순하게 모발의 보습과 세팅을 위한 화학적인 성분들로만 구성된 것이므로 인체에 유용한 천연 추출물이 포함되어 모발과 두피의 상태를 건강하게 유지하고, 탈모를 예방하는 등의 효과는 기대할 수 없는 문제점이 있었다.In addition, since conventional hair spray products are simply composed of chemical ingredients for moisturizing and setting hair, natural extracts useful for the human body are included to maintain healthy hair and scalp conditions, and effects such as preventing hair loss are expected. There was a problem that could not be.
(특허문헌 0001) 국내공개특허 제10-2011-0041023호(2011년 04월 21일 공개) (Patent Document 0001) Korean Patent Publication No. 10-2011-0041023 (published on April 21, 2011)
(특허문헌 0002) 국내등록특허 제10-1792747호(2017년 10월 26일 등록) (Patent Document 0002) Domestic registered patent No. 10-1792747 (registered on October 26, 2017)
(특허문헌 0003) 국내공개특허 제10-2013-0010746호(2013년 01월 29일 공개) (Patent Document 0003) Korean Patent Publication No. 10-2013-0010746 (published on January 29, 2013)
본 발명은 모발을 고정하여 다양한 스타일을 연출할 수 있도록 할 뿐만 아니라천연 추출물이 포함되어 건강한 두피와 모발을 갖도록 할 수 있는 어성초 성분을 포함하는 어성초 성분을 포함하는 두피 건강 개선용 스프레이 조성물을 제공하는데 있다.The present invention provides a spray composition for improving scalp health including Eoseongcho ingredients including Eoseongcho ingredients capable of not only fixing hair to express various styles, but also containing natural extracts to have healthy scalp and hair. .
본 발명이 해결하고자 하는 다양한 과제들은 이상에서 언급한 과제들에 제한되지 않으며, 언급되지 않은 또 다른 과제들은 아래의 기재로부터 당업자에게 명확하게 이해될 수 있을 것이다.Various problems to be solved by the present invention are not limited to the problems mentioned above, and other problems that are not mentioned will be clearly understood by those skilled in the art from the following description.
본 발명에 따른 어성초 성분을 포함하는 두피 건강 개선용 스프레이 조성물은 어성초 추출액을 주요 성분으로 포함한다.The spray composition for improving scalp health comprising the Eoseongcho component according to the present invention contains Eoseongcho extract as a main component.
상기 어성초 추출액 이외에, 에탄올, 판테놀(Panthenol), 소듐데하이드로아세테이트(Sodium Dehydroacetate), 프로필렌글리콜(Propylene Glycol), 유황(surfur), 징크 글루코네이트(Zinc Gluconate), 마그네슘 글루코네이트(Magnesium Gluconate), 동백 오일, 디메치콘(Dimethicone), 메타크릴로일에칠베타인(Methacryloyl Ethyl Betaine) 및 향료를 포함할 수 있다.In addition to the Eoseongcho extract, ethanol, Panthenol, Sodium Dehydroacetate, Propylene Glycol, Sulfur (surfur), Zinc Gluconate, Magnesium Gluconate, Camellia Oil, dimethicone, methacryloyl ethyl betaine (Methacryloyl Ethyl Betaine) and flavoring may be included.
상기 조성물은 어성초 추출액 1 내지 5 중량부, 에탄올 60 내지 80 중량부, 판테놀(Panthenol) 05 내지 15 중량부, 소듐데하이드로아세테이트(SodiumDehydroacetate) 01 내지 1 중량부, 프로필렌글리콜(Propylene Glycol) 03 내지 08 중량부, 유황(surfur) 01 내지 05 중량부, 징크 글루코네이트(Zinc Gluconate) 001 내지 003 중량부, 마그네슘 글루코네이트(Magnesium Gluconate) 005 내지 01 중량부, 동백 오일 0005 내지 003 중량부, 디메치콘(Dimethicone) 0025 내지 0055 중량부, 메타크릴로일에칠베타인(Methacryloyl Ethyl Betaine) 005 내지 01중량부 및 향료 0005 내지 001 중량부의 중량 비율로 포함될 수 있다.The composition is Eoseongcho extract 1 to 5 parts by weight, ethanol 60 to 80 parts by weight, Panthenol 05 to 15 parts by weight, Sodium Dehydroacetate 01 to 1 part by weight, Propylene Glycol 03 to 08 Parts by weight, sulfur (surfur) 01 to 05 parts by weight, zinc gluconate 001 to 003 parts by weight, magnesium gluconate 005 to 01 parts by weight, camellia oil 0005 to 003 parts by weight, dimethicone ( Dimethicone) 0025 to 0055 parts by weight, methacryloyl ethyl betaine (Methacryloyl Ethyl Betaine) 005 to 01 parts by weight, and fragrance 0005 to 001 parts by weight may be included in a weight ratio.
상기 어성초 추출액은, 어성초를 준비한 후 세척하고, 상기 세척된 어성초를 일정한 입도로 분쇄하되, 상기 어성초의 분쇄는 입경이 500 내지 2500㎛의 범위가 되도록 분쇄하며, 상기 분쇄된 어성초를 용매와 혼합하여 혼합액을 제조한 후, 초음파 추출기에 투입하여 상기 혼합액에 초음파를 가함으로써 어성초 추출 혼합액을 제조하되, 상기 용매는 상기 분쇄된 어성초 100 중량부에 대해 1000 내지 2000 중량부의 중량비율로 혼합되고, 상기 용매로는 물 또는 탄소수 1 내지 4의 알코올 중에서 선택된 어느 하나 이상의 용매가 사용되고, 20 내지 25℃의 온도 및 01 내지 05kgf/㎠의 압력하에서 상기 혼합액에 가해지는 초음파는 30 내지 50KHz의 진동주파수에서 30 내지 60분 동안 100 내지 200와트(watt)의 출력을 이용하여 추출하며, 상기 어성초 추출 혼합액에서 고형물을 제거한 후 10 내지 20℃의 온도에서 1 내지 3시간 동안 숙성함으로써 제조될 수 있다.The Eoseongcho extract is washed after preparing Eoseongcho, and the washed Eoseongcho is pulverized into a certain particle size, and the crushed Eoseongcho is pulverized so that the particle diameter is in the range of 500 to 2500㎛, and the pulverized Eoseongcho is mixed with a solvent. After preparing the mixed solution, the mixture was added to an ultrasonic extractor to apply ultrasonic waves to the mixed solution to prepare an Eoseongcho extract mixture, the solvent being mixed in a weight ratio of 1000 to 2000 parts by weight based on 100 parts by weight of the pulverized Eoseongcho, and the solvent As the furnace, any one or more solvents selected from water or alcohols having 1 to 4 carbon atoms are used, and the ultrasonic waves applied to the mixture under a temperature of 20 to 25°C and a pressure of 01 to 05kgf/cm2 are 30 to 50KHz at a vibration frequency of 30 to 50KHz. It is extracted using an output of 100 to 200 watts for 60 minutes, and may be prepared by aging for 1 to 3 hours at a temperature of 10 to 20°C after removing the solids from the Eoseongcho extract mixture.
상기 어성초 추출액 이외에 산양삼 발효 추출액을 더 포함하되, 상기 산양삼 발효 추출액은 상기 어성초 추출액 100 중량부에 대해 10 내지 30 중량부의 중량 비율로 포함될 수 있다.In addition to the Eoseongcho extract, a fermented wild wild ginseng extract may be further included, and the fermented wild wild ginseng extract may be included in a weight ratio of 10 to 30 parts by weight based on 100 parts by weight of the Eoseongcho extract.
또한, 본 발명은 상기한 조성물을 포함하는 두피 건강 개선용 스프레이를 제공한다.In addition, the present invention provides a spray for improving scalp health comprising the above composition.
기타 실시 예들의 구체적인 사항들은 상세한 설명에 포함되어 있다.Details of other embodiments are included in the detailed description.
본 발명에 따른 어성초 성분을 포함하는 두피 건강 개선용 스프레이 조성물은 모발을 고정하여 다양한 스타일을 연출할 수 있도록 할 뿐만 아니라 천연 추출물이 포함되어 건강한 두피와 모발을 갖도록 할 수 있는 두피 건강 개선용 스프레이를 제조할 수 있다.The scalp health improvement spray composition containing the Eoseongcho component according to the present invention not only fixes the hair to create a variety of styles, but also contains natural extracts to prepare a scalp health improvement spray that can have a healthy scalp and hair. can do.
본 발명의 기술적 사상의 실시예는, 구체적으로 언급되지 않은 다양한 효과를 제공할 수 있다는 것이 충분히 이해될 수 있을 것이다.It will be understood that embodiments of the technical idea of the present invention can provide various effects not specifically mentioned.
도 1a는 피험자의 두피를 보여주는 사진이다.1A is a photograph showing a subject's scalp.
도 1b는 실시예 1에 따라 제조된 스프레이를 20일 동안 하루 15㎖씩 피험자의 모발에 분사 및 샴푸를 반복하였고, 20일이 경과한 후 피험자의 두피를 보여주는 사진이다.1B is a photograph showing the scalp of the subject after spraying and shampooing the hair of the subject by spraying and shampooing the spray prepared according to Example 1 at 15 ml a day for 20 days.
본 발명의 이점 및 특징, 그리고 그것들을 달성하는 방법은 상세하게 후술되어 있는 실시예를 참조하면 명확해질 것이다. 그러나 본 발명은 여기서 설명되는 실시예들에 한정되지 않고 다른 형태로 구체화될 수도 있다. 오히려, 여기서 소개되는 실시예들은 개시된 내용이 철저하고 완전해질 수 있도록 그리고 당업자에게 본 발명의 사상이 충분히 전달될 수 있도록 하기 위해 제공되는 것이다.Advantages and features of the present invention, and a method of achieving them will become apparent with reference to the embodiments described below in detail. However, the present invention is not limited to the embodiments described herein and may be embodied in other forms. Rather, the embodiments introduced herein are provided so that the disclosed content may be thorough and complete, and the spirit of the present invention may be sufficiently conveyed to those skilled in the art.
본 출원에서 사용한 용어는 단지 특정한 실시예를 설명하기 위해 사용된 것으로, 본 발명을 한정하려는 의도가 아니다. 단수의 표현은 문맥상 명백하게 다르게 뜻하지 않는 한, 복수의 표현을 포함한다.The terms used in the present application are only used to describe specific embodiments, and are not intended to limit the present invention. Singular expressions include plural expressions unless the context clearly indicates otherwise.
다르게 정의되지 않는 한, 기술적이거나 과학적인 용어를 포함해서 여기서 사용되는 모든 용어들은 본 발명이 속하는 기술 분야에서 통상의 지식을 가진 자에 의해 일반적으로 이해되는 것과 동일한 의미가 있다. 일반적으로 사용되는 사전에 정의되어 있는 것과 같은 용어들은 관련 기술의 문맥상 가지는 의미와 일치하는 의미가 있는 것으로 해석되어야 하며, 본 출원에서 명백하게 정의하지 않는 한, 이상적이거나 과도하게 형식적인 의미로 해석되지 않는다.Unless otherwise defined, all terms including technical or scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which the present invention belongs. Terms such as those defined in a commonly used dictionary should be interpreted as having a meaning consistent with the meaning of the related technology, and should not be interpreted as an ideal or excessively formal meaning unless explicitly defined in this application. Does not.
이하, 본 발명에 따른 어성초 성분을 포함하는 두피 건강 개선용 스프레이 조성물에 대하여 바람직한 실시예를 들어 상세하게 설명한다.Hereinafter, a preferred embodiment will be described in detail with respect to the spray composition for improving scalp health including the Eoseongcho component according to the present invention.
본 발명에서 사용되는 용어인 "두피 건강 개선"은, 두피를 진정시키고 모발을 미화하여 매력을 증가시키며 모발을 건강하게 유지하는 것을 의미한다.The term "improving scalp health" as used herein refers to soothing the scalp and beautifying the hair to increase attractiveness and keep the hair healthy.
본 발명에 따른 어성초 성분을 포함하는 두피 건강 개선용 스프레이 조성물은 어성초 추출액, 에탄올, 판테놀(Panthenol), 소듐데하이드로아세테이트(Sodium Dehydroacetate), 프로필렌글리콜(Propylene Glycol), 유황(surfur), 징크 글루코네이트(Zinc Gluconate), 마그네슘 글루코네이트(Magnesium Gluconate), 동백 오일, 디메치콘(Dimethicone), 메타크릴로일에칠베타인(Methacryloyl Ethyl Betaine) 및 향료를 포함한다.The spray composition for improving scalp health comprising the Eoseongcho component according to the present invention includes Eoseongcho extract, ethanol, Panthenol, Sodium Dehydroacetate, Propylene Glycol, sulfur (surfur), and zinc gluconate. (Zinc Gluconate), Magnesium Gluconate, Camellia Oil, Dimethicone, Methacryloyl Ethyl Betaine, and Perfume.
또한, 본 발명에 따른 어성초 성분을 포함하는 두피 건강 개선용 스프레이 조성물은 어성초 추출액 1 내지 5 중량부, 에탄올 60 내지 80 중량부, 판테놀(Panthenol) 0.5 내지 1.5 중량부, 소듐데하이드로아세테이트(Sodium Dehydroacetate) 0.1 내지 1 중량부, 프로필렌글리콜(Propylene Glycol) 0.3 내지 0.8 중량부, 유황(surfur) 0.1 내지 0.5 중량부, 징크 글루코네이트(Zinc Gluconate) 0.01 내지 0.03 중량부, 마그네슘 글루코네이트(Magnesium Gluconate) 0.05 내지 0.1 중량부, 동백 오일 0.005 내지 0.03 중량부, 디메치콘(Dimethicone) 0.025 내지 0.055 중량부, 메타크릴로일에칠베타인(Methacryloyl Ethyl Betaine) 0.05 내지 0.1 중량부 및 향료 0.005 내지 0.01 중량부의 중량 비율로 포함될 수 있다.In addition, the spray composition for improving scalp health including the Eoseongcho component according to the present invention is Eoseongcho extract 1 to 5 parts by weight, ethanol 60 to 80 parts by weight, Panthenol 0.5 to 1.5 parts by weight, Sodium Dehydroacetate ) 0.1 to 1 parts by weight, propylene glycol (Propylene Glycol) 0.3 to 0.8 parts by weight, sulfur (surfur) 0.1 to 0.5 parts by weight, zinc gluconate (Zinc Gluconate) 0.01 to 0.03 parts by weight, magnesium gluconate (Magnesium Gluconate) 0.05 To 0.1 parts by weight, camellia oil 0.005 to 0.03 parts by weight, dimethicone 0.025 to 0.055 parts by weight, Methacryloyl Ethyl Betaine 0.05 to 0.1 parts by weight, and 0.005 to 0.01 parts by weight of fragrance It can be included as a percentage.
상기 어성초 추출액은 어성초를 추출하여 제조된 것으로, 어성초(Houttuynia cordata thunb)는 삼백초과(Saururaceae)의 식물인 약모밀의 전초로, 아시아 동남부와 특히 일본, 한국 등지에 서식한다. 상기 어성초는 열가지 약효가 있다고 하여 십약이라고도 부르며, 줄기는 고구마 잎과 같고 생잎을 만지면 생선 비린내가 심하게 나는 것에서 유래되어 어성초로 부르기도 한다. 어성초는 약용 및 식용으로도 가능하며 식품공전 식품 원재료 분류에 부원료로 최소량만을 사용할 수 있는 동ㆍ식물로 분류되어 있고 약리적으로는 강심, 이뇨, 항균, 해독, 항암 효능이 있는 것으로 널리 알려져 있으며, 민간에서는 해독과 미용을 돕는 화장품 및 건강기능식품으로 이용하고 있다.The Eoseongcho extract is prepared by extracting Eoseongcho, and Eoseongcho (Houttuynia cordata thunb) is an outpost of Yakmomil, a plant of the Saururaceae, and lives in Southeast Asia and particularly Japan and Korea. Eoseongcho is also called Sip-Yak because it has ten medicinal effects, and the stem is like a sweet potato leaf, and it is also called Eoseongcho because it originates from the fact that when you touch the raw leaves, fish smells badly. Eoseongcho is also available for medicinal and edible use. It is classified as animals and plants that can only be used in a minimum amount as an auxiliary ingredient in the classification of food raw materials in the food code. Pharmacologically, it is widely known for its strong heart, diuretic, antibacterial, detoxifying and anticancer efficacy Is used as a cosmetic and health functional food that helps detoxification and beauty.
상기 어성초 추출액은 하기의 제조방법으로 제조된 어성초 추출액이 사용될 수 있다.Eoseongcho extract prepared by the following manufacturing method may be used as the extract of Eoseongcho.
먼저, 어성초 추출액을 제조하기 위하여, 어성초를 준비한 후 세척할 수 있다.First, in order to prepare an extract of Eoseongcho, it may be washed after preparing Eoseongcho.
다음으로, 상기 세척된 어성초를 일정한 입도로 분쇄할 수 있다.Next, the washed Eoseongcho may be pulverized into a certain particle size.
상기 단계에서는 상기 어성초를 일정한 입도로 분쇄함으로써 상기 어성초의 유효성분이 충분히 추출되도록 할 수 있는데, 상기 단계에서 어성초의 분쇄는 입경이 500 내지 2500㎛의 범위가 되도록 분쇄할 수 있다. 상기 단계에서 상기 어성초의 입경이 500㎛ 미만으로 분쇄되는 경우에는 분쇄 시간이 오래 걸리고, 또한 입자가 너무 작아 추후 공정에서 입자들간의 뭉침 현상이 발생할 수 있고, 2500㎛를 초과하여 분쇄되는 경우에는 상기 어성초로부터 유용성분들을 효과적으로 추출하기 어려운 문제가 발생할 수 있다.In the above step, the active ingredient of the Eoseongcho may be sufficiently extracted by pulverizing the Eoseongcho to a certain particle size, and the crushing of the Eoseongcho may be pulverized so that the particle diameter is in the range of 500 to 2500㎛. In the above step, if the particle diameter of the Eoseongcho is pulverized to less than 500㎛, it takes a long time to pulverize, and the particles are too small to cause agglomeration between particles in a later process. It may be difficult to effectively extract useful ingredients from Eoseongcho.
그 다음으로, 상기 분쇄된 어성초를 저온 감압의 분위기에서 초음파를 가하여 추출함으로써 어성초 추출 혼합액을 제조할 수 있다.Thereafter, the pulverized Eoseongcho may be extracted by applying ultrasonic waves in an atmosphere of low temperature and reduced pressure to prepare a mixed solution for extracting Eoseongcho.
상기 단계에서는 상기 분쇄된 어성초를 용매와 혼합하여 혼합액을 제조한 후, 초음파 추출기에 투입하여 상기 혼합액에 초음파를 가함으로써 어성초 추출 혼합액을 제조할 수 있는데, 상기 용매는 상기 분쇄된 어성초 100 중량부에 대해 1000 내지 2000 중량부의 중량비율로 혼합되고, 상기 용매로는 물 또는 탄소수 1 내지 4(C1 내지 C4)의 알코올 중에서 선택된 어느 하나 이상의 용매가 사용될 수 있다.In the above step, after preparing a mixed solution by mixing the pulverized Eoseongcho with a solvent, it is added to an ultrasonic extractor to apply ultrasonic waves to the mixed solution to prepare a Eoseongcho extract mixture, wherein the solvent is 100 parts by weight of the pulverized Eoseongcho It is mixed at a weight ratio of 1000 to 2000 parts by weight, and any one or more solvents selected from water or an alcohol having 1 to 4 carbon atoms (C1 to C4) may be used as the solvent.
또한, 상기 단계는 20 내지 25℃의 온도 및 0.1 내지 0.5kgf/cm2의 압력하에서 상기 혼합액에 가해지는 초음파는 30 내지 50KHz의 진동주파수에서 30 내지 60분 동안 100 내지 200와트(watt)의 출력을 이용하여 추출할 수 있다.In addition, in the step, the ultrasonic wave applied to the mixed solution under a temperature of 20 to 25°C and a pressure of 0.1 to 0.5kgf/cm 2 outputs 100 to 200 watts for 30 to 60 minutes at a vibration frequency of 30 to 50 KHz. It can be extracted using
이어서, 상기 어성초 추출 혼합액에서 분쇄된 어성초와 같은 고형물을 제거한 후 10 내지 20℃의 온도에서 1 내지 3시간 동안 숙성함으로써 어성초 추출액을 제조할 수 있다.Subsequently, the Eoseongcho extract can be prepared by removing solids such as pulverized Eoseongcho from the Eoseongcho extract mixture and then aging for 1 to 3 hours at a temperature of 10 to 20°C.
상기 단계에서 상기 어성초 추출 혼합액에서 분쇄된 어성초와 같은 고형물의 제거는 체(sieve)와 같은 공지의 거름망 등을 이용하여 고형물을 분리하여 제거함으로써 수행될 수 있다.In the above step, the removal of solids such as crushed Eoseongcho from the Eoseongcho extract mixture may be performed by separating and removing the solids using a known sieve such as a sieve.
상기 에탄올은 용제로 작용하며, 상기 용제가 증발함에 따라서 모발 표면에 필름을 형성하고, 상기 필름의 강도에 의해서 모발을 고정시킬 수 있도록 한다.The ethanol acts as a solvent, and as the solvent evaporates, a film is formed on the surface of the hair, and the hair can be fixed by the strength of the film.
상기 판테놀은 컨디셔닝제로 사용되며 모발의 외형과 느낌 개선, 유연성 증대, 스타일 증진, 윤택 및 광택 부여, 모발의 질감을 개선하는 역할을 수행할 수 있다.The panthenol is used as a conditioning agent and may improve the appearance and feel of the hair, increase flexibility, improve style, impart moisture and gloss, and improve the texture of the hair.
상기 소듐데하이드로아세테이트(Sodium Dehydroacetate)는 살균 보존제로 사용되며 상기 어성초 성분을 포함하는 두피 건강 개선용 스프레이 조성물의 저장 안정성을 향상시키는 역할을 수행할 수 있다.The sodium dehydroacetate is used as a bactericidal preservative and may serve to improve the storage stability of a spray composition for improving scalp health including the Eoseongcho component.
상기 프로필렌글리콜(Propylene Glycol)의 화학식은 C3H8O2, 비중은 1.036~1.040이고, 끓는점은 185~189℃이다. 상기 프로필렌글리콜은 물, 알코올, 아세톤, 아세트산에틸, 클로로폼, 에테르 등과 잘 혼합되며 용해성이 뛰어나고, 흡습성이 좋아 수분 증발 차단제로 사용될 수 있다. 상기 프로필렌글리콜은 고정된 모발에 보습효과를 부여하고 모발(毛髮)을 유연하게 세팅하며 컨디셔닝 효과를 줄 수 있다.The chemical formula of the propylene glycol (Propylene Glycol) is C 3 H 8 O 2 , the specific gravity is 1.036 ~ 1.040, the boiling point is 185 ~ 189 ℃. The propylene glycol is well mixed with water, alcohol, acetone, ethyl acetate, chloroform, ether, and the like, has excellent solubility, and has good hygroscopicity, and can be used as a moisture evaporation barrier. The propylene glycol can give a moisturizing effect to fixed hair, softly set the hair, and give a conditioning effect.
상기 유황(surfur)은 생체 원소 중 8번째로 많은 비율을 차지하고 있으며, 특히 뼈, 피부, 머리카락에 많이 분포되어 있다. 인체에서 유황이 결핍되면 대머리, 손톱과 발톱의 각질화, 피부의 노화등이 일어나게 된다.The sulfur (surfur) occupies the eighth largest proportion of biological elements, and is particularly distributed in bones, skin, and hair. When the human body is deficient in sulfur, baldness, keratinization of nails and toenails, and aging of the skin occur.
또한, 유황은 중금속 및 화학약품에 대해 우수한 해독작용을 가지고 있으며, 종래 문헌에 따르면 유황이 몸에 작용하게 되면 뼈가 튼튼해지고 골수가 충만해지며(동의보감), 양기를 돕고 몸을 따뜻하게 하며 근육과 뼈를 튼튼하게 하고(신약본초), 뼈를 강하게 하며 근육을 튼튼하게 하며 탈모를 방지한다(신농본초경)고 밝히고 있다.In addition, sulfur has an excellent detoxification effect against heavy metals and chemicals, and according to the conventional literature, when sulfur acts on the body, bones become strong and bone marrow becomes full (Donguibogam), helps yang, warms the body, and It is said that it strengthens bones (new herbal medicine), strengthens bones, strengthens muscles, and prevents hair loss.
*이러한 유황은 피부에 적용시 모공 내로 침투하여 시스틴 단백질을 형성시키키고, 이와 함께 유황 사슬을 형성하여 탈모를 예방한다고 알려져 있어, 다양한 탈모방지용 제품에 일 성분으로 첨가되어 왔다.* When applied to the skin, this sulfur penetrates into the pores to form cystine proteins, and it is known to prevent hair loss by forming a sulfur chain together with it, and has been added as a component to various hair loss prevention products.
본 발명에서 사용되는 유황은 독성 성분이 제거된 유황을 의미하며, 상기 유황은 통증완화, 염증제거, 유효물질의 운반, 세포 재생, 혈액순환 촉진, 해독 및 멸균 등의 작용을 수행할 수 있는데, 예를 들어, 상기 유황으로는 시중에 판매되고 있는 공지의 유황이 사용될 수 있고, 상기 생리활성 작용과 체내 침투력을 더욱 향상시키기 위하여 입경이 10 내지 80nm인 유황이 사용될 수 있다.Sulfur used in the present invention refers to sulfur from which toxic components have been removed, and the sulfur can perform functions such as pain relief, inflammation removal, transport of active substances, cell regeneration, blood circulation promotion, detoxification and sterilization, etc. For example, a commercially known sulfur may be used as the sulfur, and sulfur having a particle diameter of 10 to 80 nm may be used to further improve the physiological activity and penetration into the body.
상기 징크 글루코네이트(Zinc Gluconate)는 피부 컨디셔닝제로 사용되며, 항바이러스 성질로 인해 염증성 여드름 등에 효과적이다. 또한, 상기 징크 글루코네이트는 자극 받은 두피를 진정시키고 피부 가려움증 등을 해소하는데 효과적이다.The zinc gluconate is used as a skin conditioning agent and is effective for inflammatory acne due to its antiviral properties. In addition, the zinc gluconate is effective in soothing the irritated scalp and relieving skin itching.
상기 마그네슘 글루코네이트(Magnesium Gluconate)는 글루코닉애씨드(Gluconic Acid)의 마그네슘염 성분으로, 화학식은 C12H22MgO14 또는 C12H22MgO14·2H2O이며, 분자량은 414.61이고, 두피 상태를 건강하고 좋은 상태로 가꾸는데 도움을 준다.The magnesium gluconate is a magnesium salt component of gluconic acid, the chemical formula is C 12 H 22 MgO 14 or C 12 H 22 MgO 14 2H 2 O, the molecular weight is 414.61, and the scalp state is It helps to keep it in a healthy and good condition.
상기 동백 오일은 불포화지방산이 다량 함유된 기름으로서, 이 기름은 방치해 두어도 증발하는 일이 거의 없고, 비중은 약 0.916으로 물과 비슷하다. 주된 지방산 성분은 올레산으로 약 90%를 차지하고 있으며, 황색의 맑은 기름으로 응고점은 최저 25℃로 낮고 주로 머리기름·정밀기계유, 의약계의 올리브유 대용으로도 쓰이고 있다.The camellia oil is an oil containing a large amount of unsaturated fatty acids, and the oil rarely evaporates even if left unattended, and its specific gravity is about 0.916, which is similar to water. The main fatty acid component is oleic acid, which accounts for about 90%. It is a yellow, clear oil with a low freezing point of 25℃, and is mainly used as a substitute for hair oil, precision machine oil, and olive oil in medicine.
본 발명에서 상기 동백 오일은 하기의 제조방법으로 제조된 동백 오일이 사용될 수 있다.In the present invention, the camellia oil prepared by the following method may be used as the camellia oil.
먼저, 품질이 우수한 동백씨를 준비한 후 물에서 깨끗하게 세척할 수 있다.First, after preparing high-quality camellia seeds, you can wash them thoroughly in water.
다음으로, 상기 세척된 동백씨를 포도즙 및 산패 억제제에 침지시킬 수 있다. 상기와 같이 동백씨를 포도즙 및 산패 억제제에 침지시킴으로써 제조되는 동백 오일이 변색되거나 산패가 일어나는 것을 방지할 수 있다.Next, the washed camellia seeds may be immersed in grape juice and rancidity inhibitors. As described above, the camellia oil produced by immersing the camellia seeds in grape juice and rancidity inhibitor can prevent discoloration or rancidity.
상기 세척된 동백씨의 침지는 상기 동백씨를 포도즙 및 산패 억제제가 1:1의 중량 비율로 혼합된 혼합액에 침지시킬 수 있고, 상기 산패 억제제는 비타민 C 및 소금용액이 1:1의 중량 비율로 혼합되어 제조될 수 있다.The washed camellia seeds can be immersed in a mixture of grape juice and rancidity inhibitor in a ratio of 1:1, and the rancidity inhibitor is mixed with vitamin C and salt solution in a weight ratio of 1:1. Can be manufactured.
상기 포도즙은 혈전 방지 및 고혈압, 동맥경화 및 심장질환 등 성인병 예방에 좋고 기억력 향상에 도움을 줄 수 있고, 상기 산패 억제제로 사용되는 소금용액은 농도가 1 내지 2 중량%인 소금용액일 수 있으며, 상기 세척된 동백씨 100 중량부에 대해 포도즙 및 산패 억제제의 혼합액 100 내지 120 중량부의 중량 비율로 침지시킨 후 10 내지 40분 동안 유지시켜 진행될 수 있다.The grape juice is good for preventing blood clots and preventing adult diseases such as high blood pressure, arteriosclerosis and heart disease, and can help improve memory, and the salt solution used as the rancidity inhibitor may be a salt solution having a concentration of 1 to 2% by weight, The washed camellia seeds may be immersed in a weight ratio of 100 to 120 parts by weight of a mixture of grape juice and rancidity inhibitor with respect to 100 parts by weight of the washed camellia seeds, and then maintained for 10 to 40 minutes.
그 다음으로, 상기 포도즙 및 산패 억제제의 혼합액에 침지된 동백씨를 꺼내어 상기 동백씨 내부로 포도즙 및 산패 억제제의 성분이 침투되도록 할 수 있다.Next, the camellia seeds immersed in the mixed solution of the grape juice and rancidity inhibitor may be taken out so that the grape juice and components of the rancidity inhibitor may penetrate into the camellia seeds.
상기 단계에서는 포도즙 및 산패 억제제의 유효 성분이 상기 동백씨의 표면으로 침투되도록 함으로써 장시간이 경과한 경우에도 제조되는 동백 오일이 변색되거나 산패하는 것을 방지할 수 있는데, 상기 단계에서는 포도즙 및 산패 억제제의 혼합액에서 분리된 동백씨를 35 내지 40℃의 온도에서 30 내지 60분 동안 보관함으로써 진행될 수 있다.In the above step, by allowing the active ingredient of grape juice and rancidity inhibitor to penetrate to the surface of the camellia seed, it is possible to prevent discoloration or rancidity of the camellia oil produced even after a long period of time. In this step, a mixture of grape juice and rancidity inhibitor The camellia seeds separated from may be stored at a temperature of 35 to 40° C. for 30 to 60 minutes.
이어서, 상기 포도즙 및 산패 억제제의 성분이 침투된 동백씨를 증숙할 수 있다.Subsequently, the camellia seeds into which the components of the grape juice and rancidity inhibitors have penetrated can be steamed.
상기 동백씨의 증숙은 상기 포도즙 및 산패 억제제의 성분이 침투된 동백씨를 수증기로 30분 내지 60분 동안 찜으로써 수행될 수 있는데, 상기 동백씨의 증숙이 상기한 하한 범위 미만으로 수행되는 경우에는 충분한 증숙이 이루어지지 않는 문제점이 있고, 상기한 상한 범위를 초과하여 수행되는 경우에는 증숙 시간의 증가에 따른 효과의 차이가 미미할 수 있다.The steaming of the camellia seeds can be performed by steaming the camellia seeds into which the grape juice and rancidity inhibitor components are infiltrated with steam for 30 to 60 minutes.If the steaming of the camellia seeds is performed below the above lower limit, sufficient There is a problem in that steaming is not performed, and when the steaming is performed beyond the upper limit range, the difference in effect according to the increase of the steaming time may be insignificant.
다음으로, 상기 증숙된 동백씨를 건조할 수 있다.Next, the steamed camellia seeds can be dried.
상기 증숙된 동백씨의 건조는 상기 증숙된 동백씨를 30 내지 40℃의 온도에서 10 내지 20시간 동안 수행될 수 있는데, 상기 동백씨의 건조 온도가 일정하게 유지되도록 하기 위하여 건조기를 이용한 기계식 건조가 이용될 수 있다.Drying of the steamed camellia seeds can be carried out for 10 to 20 hours at a temperature of 30 to 40°C on the steamed camellia seeds, and mechanical drying using a dryer is used to keep the drying temperature of the camellia seeds constant. Can be.
그 다음으로, 상기 건조된 동백씨를 초산 또는 구연산 중 어느 하나 이상의 산으로 세척할 수 있다.Next, the dried camellia seeds may be washed with at least one acid of acetic acid or citric acid.
상기 건조된 동백씨의 세척은 상기 건조된 동백씨의 표면을 초산 또는 구연산 중 어느 하나 이상의 산으로 세척함으로써, 추후 발효 공정을 거쳐 제조될 동백 오일의 향미, 색택 등의 개선 효과가 있다.The washing of the dried camellia seeds is effective in improving the flavor and color of camellia oil to be produced through a later fermentation process by washing the surface of the dried camellia seeds with one or more acids of acetic acid or citric acid.
이어서, 상기 세척된 동백씨에 배양액 및 유산균으로 이루어진 발효액을 분무할 수 있다.Subsequently, the washed camellia seed may be sprayed with a fermentation broth consisting of a culture broth and lactic acid bacteria.
상기 유산균으로는 젖산균(Lactobacillales), 스트렙토코쿠스 테르모필루스(Streptococcus thermophiles) 및 비피도박테리움 롱굼(Bifidobacterium longum)으로 이루어진 군에서 선택된 어느 하나의 공지된 유산균이 이용될 수 있고, 상기 배양액은 펩톤, 맥아추출물(Malt extract), 시트르산나트륨(Sodium citrate), 제2인산칼륨(Potassium phosphate dibasic), 글루코스(Glucose) 및 증류수로 이루어지고, 상기 배양액은 펩톤 15 내지 25 중량부, 맥아추출물 5 내지 15 중량부, 시트르산나트륨 0.5 내지 1.5 중량부, 제2인산칼륨 0.1 내지 0.3 중량부, 글루코스 1 내지 3 중량부 및 증류수 100 내지 200 중량부의 중량 비율로 혼합되어 이루어질 수 있다.As the lactic acid bacteria, any one known lactic acid bacteria selected from the group consisting of lactic acid bacteria ( Lactobacillales ), Streptococcus thermophiles , and Bifidobacterium longum may be used, and the culture medium is peptone , Malt extract, sodium citrate, potassium phosphate dibasic, glucose, and distilled water, and the culture solution is 15 to 25 parts by weight of peptone, malt extract 5 to 15 It may be made by mixing in a weight ratio of 0.5 to 1.5 parts by weight of sodium citrate, 0.1 to 0.3 parts by weight of dibasic potassium phosphate, 1 to 3 parts by weight of glucose, and 100 to 200 parts by weight of distilled water.
상기 배양액에서 상기 펩톤은 단백질을 공급해주는 질소원으로서 미생물의 성장에 필요한 단백질을 공급해 주며, 상기 맥아추출물은 각종 미네랄, 비타민 B군, 아미노산이 포함되어 있어 미생물 성장에 도움을 줄 수 있으며, 상기 시트르산나트륨은 배양액의 pH를 조절하여 미생물의 성장에 최적화된 상태를 유지해 주는 무기질로, 영양을 공급해 줄 수 있고, 상기 글루코스는 유산균이 당을 대사하여 유기산을 만들어내는 중요한 성분으로 기능할 수 있다.In the culture medium, the peptone is a nitrogen source that supplies protein and supplies proteins necessary for the growth of microorganisms, and the malt extract contains various minerals, vitamin B groups, and amino acids, so that it can help the growth of microorganisms, and the sodium citrate Silver is an inorganic substance that maintains a state optimized for the growth of microorganisms by adjusting the pH of the culture medium, and can supply nutrients, and the glucose can function as an important component by which lactic acid bacteria metabolize sugar to produce organic acids.
다음으로, 상기 발효액이 분무된 동백씨를 발효시킬 수 있다.Next, the camellia seeds sprayed with the fermentation broth may be fermented.
상기 동백씨의 발효는 상기 발효액이 분무된 동백씨를 45 내지 50℃의 온도 및 60 내지 65%의 습도를 유지하는 보관용기에서 3 내지 6일 동안 보관하여 발효시킬 수 있다.Fermentation of the camellia seeds may be fermented by storing the camellia seeds sprayed with the fermentation broth in a storage container maintaining a temperature of 45 to 50° C. and a humidity of 60 to 65% for 3 to 6 days.
그 다음으로, 상기 발효된 동백씨를 냉풍 건조할 수 있다.Next, the fermented camellia seeds may be dried in cold air.
상기 발효된 동백씨의 냉풍 건조는 상기 발효된 동백씨를 3 내지 6℃의 온도의 냉풍으로 5 내지 10시간 동안 건조하고, 55 내지 60℃의 온도로 1 내지 3일 동안 유지함으로써 진행될 수 있다.Cold air drying of the fermented camellia seeds may be performed by drying the fermented camellia seeds with cold air at a temperature of 3 to 6° C. for 5 to 10 hours and maintaining the fermented camellia seeds at a temperature of 55 to 60° C. for 1 to 3 days.
이어서, 상기 냉풍 건조된 동백씨를 습도 70 내지 80%, 120 내지 150℃의 온도 및 2 내지 4kgf/cm2으로 압착한 후 오일을 분리함으로써, 동백 오일(동백씨 오일)을 제조할 수 있다.Subsequently, the cold-air dried camellia seeds are compressed at a humidity of 70 to 80%, a temperature of 120 to 150°C, and 2 to 4 kgf/cm 2 , and then the oil is separated to prepare camellia oil (camellia seed oil).
상기 디메치콘(Dimethicone)은 유화제로 사용되는데, 본 발명에 따른 어성초 성분을 포함하는 두피 건강 개선용 스프레이 조성물의 혼합성을 향상시켜 균질한 물성을 나타내도록 할 수 있다.The dimethicone is used as an emulsifier, and it can improve the mixing properties of the spray composition for improving scalp health including the Eoseongcho component according to the present invention so as to exhibit homogeneous physical properties.
상기 메타크릴로일에칠베타인(Methacryloyl Ethyl Betaine)은 투명한 방향성 알코올인 에탄올 용제(溶劑)에 잘 융해될 수 있도록 할 수 있다.The methacryloyl ethyl betaine (Methacryloyl Ethyl Betaine) may be so as to be well dissolved in an ethanol solvent (溶劑), a transparent aromatic alcohol.
상기 향료(香料)는 스프레이 조성물의 방향성을 제공하는 것으로, 공지된 다양한 종류의 향료가 사용될 수 있고, 예를 들어, 식물에서 추출하는 천연향료를 사용하여 두발(頭髮)이나 두피의 건강을 고려할 수 있다.The fragrance provides the fragrance of the spray composition, and various kinds of known fragrances can be used.For example, natural fragrances extracted from plants can be used to consider the health of the hair or scalp. have.
한편, 본 발명에 따른 어성초 성분을 포함하는 두피 건강 개선용 스프레이 조성물은 상기 조성물 이외에 산양삼 발효 추출액을 더 포함할 수도 있는데, 상기 산양삼 발효 추출액은 상기 어성초 추출액 100 중량부에 대해 10 내지 30 중량부의 중량 비율로 포함될 수 있다.On the other hand, the spray composition for improving scalp health comprising the Eoseongcho component according to the present invention may further include a fermented wild ginseng extract in addition to the composition, wherein the fermented wild wild ginseng extract is 10 to 30 parts by weight based on 100 parts by weight of the Eoseongcho extract. It can be included as a percentage.
상기 산양삼 발효 추출물은 산양삼 뿌리 및 산양삼 잎을 이용하여 제조될 수 있는데, 상기 산양삼에는 인삼보다 10배, 홍삼보다는 4~5배 많은 사포닌이 들어있어 면역력을 높이는 데 큰 효능이 있으며, 이와 더불어 혈액순환, 당뇨 예방, 소화력 증진, 스트레스 완화, 기력 증진 등의 효능이 있다.The fermented wild wild ginseng extract can be prepared using wild wild ginseng roots and wild wild ginseng leaves.The wild wild ginseng contains 10 times more saponin than ginseng and 4 to 5 times more than red ginseng, which has great efficacy in enhancing immunity. , Diabetes prevention, digestion, stress relief, energy enhancement, etc. are effective.
상기 산양삼 발효 추출액은 하기의 제조방법으로 제조된 산양삼 발효 추출액이 사용될 수 있다.The wild wild ginseng fermented extract may be used wild wild ginseng fermented extract prepared by the following manufacturing method.
먼저, 산양삼 뿌리 및 산양산 생잎을 분리하여 준비한 후 세척할 수 있다.First, the wild mountain ginseng root and the fresh mountain mountain leaves can be separated and prepared, and then washed.
다음으로, 상기 산양삼 뿌리를 수증기로 가열하여 증삼한 후 유황 훈증할 수 있다.Next, the wild ginseng root can be heated with steam to increase steam and then fumigate with sulfur.
상기 단계에서는 상기 산양삼 뿌리를 130 내지 140℃ 온도 및 1 내지 3kgf/cm2의 압력에서 30 내지 100분 동안 수증기로 가열한 후, 상기 수증기로 가열된 산양삼 뿌리에 1 내지 3분 동안 유황 훈증을 할 수 있다.In the step, the wild ginseng roots are heated with steam for 30 to 100 minutes at a temperature of 130 to 140°C and a pressure of 1 to 3kgf/cm 2 , and then sulfur fumigation is performed on the wild ginseng roots heated with steam for 1 to 3 minutes. I can.
상기 단계에서 상기 유황을 사용하면, 상기 산양삼에 포함되어 있는 탄닌 물질 등의 폴리페놀이 건조 중에 산화되어 흑변되는 것을 방지할 수 있고, 추후 공정에서 미생물이 번식하는 것을 방지할 수 있다.When the sulfur is used in the above step, it is possible to prevent the polyphenols such as tannins contained in the wild ginseng from being oxidized and blackened during drying, and it is possible to prevent the growth of microorganisms in a later process.
그 다음으로, 상기 유황 훈증된 산양삼 뿌리를 건조할 수 있다.Then, the sulfur fumigated wild ginseng roots can be dried.
상기 단계에서는 유황 훈증된 산양삼 뿌리를 25 내지 30℃의 온도에서 1 내지 3일 동안 건조할 수 있다.In the above step, the sulfur fumigated wild ginseng roots may be dried for 1 to 3 days at a temperature of 25 to 30°C.
이어서, 상기 건조된 산양삼 뿌리를 일정 길이 단위로 절단할 수 있는데, 예를 들어, 상기 건조된 산양삼 뿌리를 0.1 내지 1.0cm의 길이 단위로 절단할 수 있다.Subsequently, the dried wild ginseng root may be cut in units of a predetermined length, for example, the dried wild ginseng root may be cut in a length unit of 0.1 to 1.0 cm.
다음으로, 상기 절단된 산양삼 뿌리에 유산균과 혼합한 후 숙성시킬 수 있다.Next, it can be aged after mixing with lactic acid bacteria in the cut wild ginseng root.
상기 단계에서 상기 숙성은 상기 유산균과 혼합된 산양삼 뿌리를 20 내지 25℃의 온도에서 10 내지 30시간 동안 유지하여 숙성시킬 수 있다.In the above step, the aging can be aged by maintaining the wild ginseng root mixed with the lactic acid bacteria for 10 to 30 hours at a temperature of 20 to 25 ℃.
예를 들어, 상기 유산균으로는 젖산균(Lactobacillales), 스트렙토코쿠스 테르모필루스(Streptococcus thermophiles) 및 비피도박테리움 롱굼(Bifidobacterium longum)으로 이루어진 군에서 선택된 어느 하나의 공지된 유산균이 이용될 수 있다.For example, as the lactic acid bacteria, any one known lactic acid bacteria selected from the group consisting of lactic acid bacteria ( Lactobacillales ), Streptococcus thermophiles , and Bifidobacterium longum may be used.
그 다음으로, 상기 세척된 산양삼 생잎을 수증기로 가열할 수 있다.Next, the washed wild wild ginseng leaves may be heated with steam.
상기 단계에서는 상기 산양삼 생잎을 110 내지 120℃ 온도 및 1 내지 3kgf/cm2의 압력에서 10 내지 30분 동안 수증기로 가열함으로써 수행될 수 있다.In the above step, it may be carried out by heating the wild wild ginseng leaves at 110 to 120°C and a pressure of 1 to 3kgf/cm 2 with steam for 10 to 30 minutes.
이어서, 상기 수증기로 가열된 산양삼 생잎을 건조할 수 있다.Subsequently, the fresh wild wild ginseng leaves heated with the steam may be dried.
상기 단계에서는 햇빛 건조시 상기 산양삼 생잎의 엽록소가 파괴되고 유용 성분이 휘발되는 것을 방지하기 위하여, 상기 산양삼 생잎을 온도 25 내지 30℃에서 5 내지 10시간 동안 건조할 수 있다.In the above step, in order to prevent the chlorophyll of the wild wild ginseng leaves from being destroyed and the useful components volatilized during sunlight drying, the wild wild wild ginseng leaves may be dried for 5 to 10 hours at a temperature of 25 to 30°C.
다음으로, 상기 건조된 산양삼 생잎을 가열하여 덖음할 수 있다.Next, the dried wild wild ginseng leaves can be heated to roast.
상기 단계는 상기 건조된 산양삼 생잎을 가열 용기(예를 들어, 가마솥)에 투입한 후 90 내지 95℃의 온도에서 3 내지 5분 동안 1차 덖음하고, 상기 1차 덖음된 산양삼 생잎을 130 내지 140℃의 온도에서 30 내지 60초 동안 2차 덖음하는 단계로 진행될 수 있다.In the step, the dried wild wild ginseng leaves are put into a heating container (for example, a cauldron) and then first roasted at a temperature of 90 to 95°C for 3 to 5 minutes, and the first roasted wild wild wild ginseng leaves are 130 to 140 At a temperature of ℃ 30 to 60 seconds may proceed to the step of the second abrasion.
그 다음으로, 상기 세척된 산양삼 생잎에 고초균 침출수를 분무하여 상기 산양삼 생잎을 발효시킬 수 있다.Then, the washed wild wild ginseng leaves may be fermented by spraying the Bacteria leachate into the washed wild wild ginseng leaves.
상기 고초균 침출수는 상기 건조된 산양삼 생잎의 발효를 촉진할 수 있는 것으로, 상기 건조된 산양삼 생잎 100 중량부에 대해 고초균 배양액 30 내지 50 중량부의 중량 비율로 분무하고 55 내지 60℃의 온도 및 60 내지 65%의 습도가 유지되도록 한 후 2 내지 4일 동안 발효시킬 수 있다.The Bacillus leachate is capable of accelerating the fermentation of the dried wild wild ginseng leaves, sprayed at a weight ratio of 30 to 50 parts by weight of the dried wild wild ginseng leaves, and a temperature of 55 to 60°C and 60 to 65 After allowing the% humidity to be maintained, it can be fermented for 2 to 4 days.
상기 고초균 배양액은 고초균과 물을 혼합하여 생성되는 것으로, 상기 고초균은 고두밥에 흑설탕을 10 내지 12중량% 혼합하고, 준비된 배지 위에 친환경 왕겨를 놓고 헝겊을 덮은 후, 25℃ 온도에서 1일 2회 생육에 수분을 분무하면서 1주일 동안 배양시켜 고초균을 생성시키고, 이를 쌀겨와 흑설탕이 50:50 중량비로 혼합된 배지에 다시 접종하여 25℃에서 1주일 동안 배양하여 본 발명에 이용되는 고초균 침출수로 사용할 수 있다.The Bacillus Bacillus culture medium is produced by mixing Bacillus bacillus and water, and the Bacillus bacillus is grown twice a day at 25°C after mixing 10 to 12% by weight of brown sugar in godubap, placing eco-friendly rice husks on the prepared medium and covering a cloth. It can be cultured for one week while spraying water on the plant to generate Bacillus bacteria, which are re-inoculated in a medium mixed with rice bran and brown sugar at a weight ratio of 50:50, and cultured at 25°C for one week to be used as the Bacillus bacteria leachate used in the present invention. have.
본 발명에서 상기 고초균은 바실러스 서브틸리스(Bacillus subtilis), 바실러스 서브틸리스 스피지제피아이(Bacillus subtilis), 바실러스 메가테리움(Bacillus megaterium), 바실러스 리체니포르미스(Bacillus licheniformis) 및 바실러스 풀미스(Bacillus pumilus)로 이루어진 군에서 선택된 어느 하나 이상이 사용될 수 있다.In the present invention, the Bacillus subtilis ( Bacillus subtilis ), Bacillus subtilis spjijepiyi ( Bacillus subtilis ), Bacillus megaterium ( Bacillus megaterium ), Bacillus licheniformis ( Bacillus licheniformis ) and Bacillus fulmis Any one or more selected from the group consisting of ( Bacillus pumilus ) may be used.
다음으로, 상기 숙성된 산양삼 뿌리와, 상기 발효된 산양삼 생잎을 혼합한 후 발효시켜 발효 산양삼 혼합물을 제조할 수 있다.Next, the fermented wild wild ginseng root and the fermented wild wild ginseng leaves are mixed and fermented to prepare a fermented wild wild ginseng mixture.
상기 단계에서는 상기 숙성된 산양삼 뿌리 100 중량부에 대해 상기 발효된 산양삼 생잎 200 내지 400 중량부의 중량 비율로 혼합한 후, 60 내지 65℃의 온도 및 55 내지 60%의 습도에서 3 내지 5일 동안 발효시켜 발효 산양삼 혼합물을 제조할 수 있다.In the step, the fermented wild wild ginseng leaves are mixed at a weight ratio of 200 to 400 parts by weight with respect to 100 parts by weight of the aged wild ginseng roots, and then fermented for 3 to 5 days at a temperature of 60 to 65°C and a humidity of 55 to 60%. To prepare a fermented wild ginseng mixture.
그 다음으로, 상기 발효 산양삼 혼합물에 용매를 혼합하고 초음파를 가함으로써 산양삼 발효액을 제조할 수 있다.Next, the fermented wild wild ginseng fermentation broth may be prepared by mixing a solvent with the fermented wild wild ginseng mixture and applying ultrasonic waves.
상기 산양삼 발효액을 제조하기 위하여 상기 발효 산양삼 혼합물을 용매와 혼합하여 혼합액을 제조한 후, 초음파 추출기에 투입하여 상기 혼합액에 초음파를 가함으로써 산양삼 발효액을 제조할 수 있는데, 상기 용매는 상기 산양삼 혼합액 100 중량부에 대해 300 내지 500 중량부의 중량 비율로 포함되고, 상기 용매로는 물이 사용될 수 있다.In order to prepare the wild wild ginseng fermentation broth, the fermented wild ginseng mixture may be mixed with a solvent to prepare a mixture, and then added to an ultrasonic extractor to apply ultrasonic waves to the mixture to prepare a wild wild ginseng fermentation broth. It is included in a weight ratio of 300 to 500 parts by weight based on parts, and water may be used as the solvent.
또한, 상기 산양삼 발효액을 제조하기 위하여 상기 혼합액에 가해지는 초음파는 60 내지 80KHz의 진동주파수에서 50 내지 100분 동안 100 내지 200와트(watt)의 출력을 이용하여 추출할 수 있다.In addition, the ultrasonic wave applied to the mixed solution to prepare the fermented wild ginseng may be extracted using an output of 100 to 200 watts for 50 to 100 minutes at a vibration frequency of 60 to 80 KHz.
*이어서, 상기 산양삼 발효액에서 산양삼 뿌리, 산양삼 생잎과 같은 고형분을 제거할 수 있다.* Subsequently, solids such as wild wild ginseng roots and fresh wild wild ginseng leaves can be removed from the fermented wild ginseng broth.
상기 단계에서 산양삼 뿌리, 산양삼 생잎과 같은 고형분의 분리는 체(sieve) 등과 같은 공지의 거름망을 이용할 수 있다.Separation of solids such as wild wild ginseng roots and fresh wild wild ginseng leaves in the above step may be performed using a known strainer such as a sieve.
다음으로, 상기 고형분이 제거된 산양삼 발효액을 원심분리할 수 있다.Next, the fermented wild ginseng broth from which the solid content has been removed may be centrifuged.
상기 단계에서는 고형분이 제거된 산양삼 발효액을 원심분리함으로써, 산양삼 뿌리와 생잎의 미세입자들이 위치하는 하층액과, 상기 하층액 상부에 위치하는 중층액 및 상층액으로 위치적으로 구분하여 분리할 수 있다.In the above step, by centrifuging the fermented wild ginseng broth from which solids have been removed, it can be separated into a lower layer in which fine particles of wild ginseng roots and fresh leaves are located, and a middle layer and a supernatant located above the lower layer. .
다음으로, 상기 중층액 및 상층액에 위치하는 산양삼 발효액을 추출하여 산양삼의 유용성분이 산양삼 발효 추출액을 제조할 수 있다.Next, by extracting the fermented sanyangsam broth located in the intermediate and supernatant liquid, the useful ingredient of sanyangsam may prepare a fermented sanyangsam extract.
상기 단계에서 상기 산양삼 발효 추출액은 산양삼 발효액 2000 내지 3000g에 70%(v/v) 에탄올수용액 10~15ℓ로 85 내지 90℃에서 3~4시간 동안 1차 추출한 다음, 70%(v/v) 에탄올수용액 4~6ℓ로 85 내지 90℃에서 2~3시간 동안 2차 추출을 완료하고, 진공회전증발기에서 1000 내지 1500㎖이 될 때까지 추출액을 제조하는 단계; 및 상기 추출액에 에탄올을 가하여 2 내지 3배 중량으로 희석하고, 18,000~20,000rpm에서 30 내지 40분 동안 원심분리하여 상기 산양삼 발효액에 포함될 수 있는 고분자 섬유소 및 고형분을 완전히 제거한 다음, 모아진 상등액을 1.5~2.0배 중량의 아세트산으로 2회 추출하는 단계에 의해 제조될 수 있다.In the above step, the fermented wild wild ginseng extract is first extracted with 10 to 15 ℓ of a 70% (v/v) ethanol aqueous solution in 2000 to 3000 g of wild wild ginseng fermentation broth at 85 to 90°C for 3 to 4 hours, and then 70% (v/v) ethanol Completing the secondary extraction for 2 to 3 hours at 85 to 90 °C with 4 to 6 ℓ of aqueous solution, and preparing an extract until it becomes 1000 to 1500 ㎖ in a vacuum rotary evaporator; And ethanol is added to the extract, diluted to 2 to 3 times by weight, centrifuged at 18,000 to 20,000 rpm for 30 to 40 minutes to completely remove polymer fibers and solids that may be included in the fermented wild ginseng, and then the collected supernatant is 1.5 to It can be prepared by extracting twice with 2.0 times the weight of acetic acid.
한편, 본 발명에 따른 어성초 성분을 포함하는 두피 건강 개선용 스프레이 조성물은 상기 조성물 이외에 양파 추출물을 더 포함할 수도 있는데, 상기 양파 추출물은 상기 어성초 추출액 100 중량부에 대해 5 내지 15 중량부의 중량 비율로 포함될 수 있다.Meanwhile, the spray composition for improving scalp health comprising the Eoseongcho component according to the present invention may further include an onion extract in addition to the composition, wherein the onion extract is in a weight ratio of 5 to 15 parts by weight based on 100 parts by weight of the Eoseongcho extract. Can be included.
상기 양파 추출물은 양파의 유용성분을 추출하여 제조되는데, 상기 양파(Allium cepa)는 백합과에 속하는 다년생 식물로, 오랜 재배역사와 더불어 특유의 맛과 향을 적용한 식품, 향신료 및 약재 등으로 이용되고 있다. 양파 100g에는 수분 90g, 탄수화물 약 72g, 단백질 11g, 비타민 C 10 내지 20mg, 칼슘, 인, 철 등이 함유되어 있으며, 양파껍질에는 당질 504%, 섬유질 2924%, 지방 148%, 회분 499% 등이 함유되어 있다.The onion extract is prepared by extracting the useful ingredients of onion, and the onion (Allium cepa) is a perennial plant belonging to the lily family, and is used as food, spices and medicinal materials to which a unique taste and aroma are applied along with a long cultivation history. have. 100g of onion contains 90g of moisture, about 72g of carbohydrates, 11g of protein, 10 to 20mg of vitamin C, calcium, phosphorus, and iron.The onion skin contains 504% sugar, 2924% fiber, 148% fat, and 499% ash. Contains.
양파의 효능으로는 항산화, 혈액 지질 저하, 항고혈압, 항염증, 항균, 항종양, 혈당 저하 등이 알려져 있다. 양파 내에 함유된 주요 생리활성물질로는 유기 황화합물과 플라보노이드 화합물을 들 수 있으며, 특히 양파에는 항산화 작용을 나타내는 케르세틴(quercetin)이 다른 야채나 과일에 비해 매우 높게 함유되어 있다. 케르세틴은 식물유래 플라보노이드계(flavonoid)계의 페놀화합물로서, 강력한 항산화제(antioxidant)일 뿐만 아니라 항동맥 경화, 항균작용, 콜레스테롤 저하, 항암, 항바이러스 및 항알러지 활성을 지니고 있으면서 독성은 거의 나타나지 않는 것으로 알려져 있다. 따라서 케르세틴이 많이 함유되어 있는 식품을 섭취하면 혈액순환 개선, 혈압 강하와 당뇨, 체중감소 등의 다이어트, 면역기능 강화, DNA 손상억제효과 및 적혈구 막의 지질과산화 저해효과 등에 효과가 있다.The efficacy of onions is known for antioxidant, lowering blood lipids, antihypertension, anti-inflammatory, antibacterial, anti-tumor, and lowering blood sugar. The main physiologically active substances contained in onions include organic sulfur compounds and flavonoid compounds. In particular, onions contain very high quercetin, which exhibits antioxidant activity, compared to other vegetables and fruits. Quercetin is a plant-derived flavonoid-based phenolic compound that is not only a powerful antioxidant, but also has anti-arteriosclerosis, antibacterial activity, cholesterol lowering, anti-cancer, anti-viral and anti-allergic activities, but little toxicity. It is known. Therefore, eating foods containing a lot of quercetin is effective in improving blood circulation, lowering blood pressure and dieting such as diabetes and weight loss, strengthening immune function, inhibiting DNA damage, and inhibiting lipid peroxidation of red blood cell membranes.
본 발명에서 상기 양파 추출물은 하기의 제조방법으로 제조될 수 있다.In the present invention, the onion extract can be prepared by the following manufacturing method.
상기 양파 추출물을 제조하기 위하여, 먼저, 양파를 채취하여 1 내지 3(w/w)% 농도 범위 및 33 내지 37℃의 온도를 가지는 탄산수소나트륨(NaHCO3)이 용해된 정제수로 1 내지 5분 동안 세척하여 양파에 부착되어 있는 이물질을 제거하고, 상기 양파의 껍질을 분리하여 양파 과육 및 양파 껍질로 분리할 수 있다.In order to prepare the onion extract, first, the onion is collected and 1 to 5 minutes with purified water in which sodium hydrogen carbonate (NaHCO 3 ) having a concentration range of 1 to 3 (w/w)% and a temperature of 33 to 37°C is dissolved During washing to remove foreign substances adhering to the onion, the peel of the onion can be separated and separated into onion flesh and onion peel.
다음으로, 상기 양파 과육을 건조기에서 건조하되, 상기 양파 과육의 건조는 햇빛 건조시 상기 양파 과육의 엽록소가 파괴되고 양파 과육 고유의 향이 사라지는 것을 방지하기 위하여 일정한 온도 및 습도가 유지되는 건조기에서 수행될 수 있는데, 예를 들어, 상기 양파 과육의 건조는 온도 20 내지 25℃ 및 습도 33 내지 40%로 유지되는 건조기에서 3 내지 7시간 동안 건조할 수 있다.Next, the onion pulp is dried in a dryer, but drying of the onion pulp is performed in a dryer in which a constant temperature and humidity are maintained in order to prevent the chlorophyll of the onion pulp from being destroyed and the inherent flavor of the onion pulp from disappearing when drying in sunlight. For example, the onion flesh may be dried for 3 to 7 hours in a dryer maintained at a temperature of 20 to 25° C. and a humidity of 33 to 40%.
그 다음으로, 상기 건조된 양파 과육을 정제수와 혼합한 후 가열하여 상기 양파 과육 추출물을 제조할 수 있다.Thereafter, the dried onion pulp is mixed with purified water and heated to prepare the onion pulp extract.
상기 양파 과육 추출물은 상기 건조된 양파 과육 100 중량부에 대하여 정제수 500 내지 1000 중량부를 혼합한 후 95 내지 105℃의 온도에서 5 내지 15시간 동안 가열함으로써 상기 양파 과육 추출물을 제조할 수 있다.The onion pulp extract may be prepared by mixing 500 to 1000 parts by weight of purified water with respect to 100 parts by weight of the dried onion pulp and heating at a temperature of 95 to 105°C for 5 to 15 hours.
이어서, 양파 껍질을 건조하여 상기 양파 껍질에 함유되어 있는 수분을 제거할 수 있고, 상기 양파 껍질의 건조는 30 내지 35℃ 및 습도 35 내지 45%로 유지되는 건조기에서 3 내지 7시간 동안 건조할 수 있는데, 본 발명은 상기와 같은 조건으로 양파 껍질을 건조함으로써, 상기 양파 껍질에 포함되어 있는 수분이 점진적으로 고르게 증발되도록 함으로써, 양파 껍질의 고유의 향과 유용성분을 보다 용이하게 추출시킬 수 있고, 양파 껍질의 세포조직의 파괴로 공기의 침투를 용이하게 하여 발효작용을 촉진함으로써 양파 껍질의 유용성분이 진하게 우러나도록 할 수 있다.Subsequently, the onion peel can be dried to remove moisture contained in the onion peel, and the onion peel can be dried for 3 to 7 hours in a dryer maintained at 30 to 35°C and 35 to 45% humidity. In the present invention, by drying the onion skin under the same conditions as described above, the moisture contained in the onion skin is gradually and evenly evaporated, so that the inherent aroma and useful ingredients of the onion skin can be more easily extracted, By destroying the cell tissue of the onion skin, it facilitates the penetration of air and promotes the fermentation, so that the useful components of the onion skin can be enriched.
다음으로, 상기 건조된 양파 껍질을 정제수와 혼합한 후 가열하여 상기 양파 껍질 추출물을 제조할 수 있는데, 상기 양파 껍질 추출물은 상기 건조된 양파 껍질 100 중량부에 대하여 정제수 200 내지 400 중량부를 혼합한 후 60 내지 70℃의 온도에서 1 내지 3시간 동안 침지시킨 후, 상기 양파 껍질이 침지된 정제수를 가열기에 투입하고, 상기 가열기에 투입된 양파 껍질이 침지된 정제수를 110 내지 120℃의 온도 및 압력용기 내부 압력 2.5 내지 3.5kgf/cm2의 범위에서 3 내지 5시간 동안 가열함으로써 상기 양파 껍질 추출물을 제조할 수 있다.Next, the dried onion peel is mixed with purified water and then heated to prepare the onion peel extract. The onion peel extract is mixed with 200 to 400 parts by weight of purified water based on 100 parts by weight of the dried onion peel. After immersing for 1 to 3 hours at a temperature of 60 to 70°C, the purified water immersed in the onion skin is added to a heater, and purified water in which the onion skin is immersed in the heater is added to a temperature of 110 to 120°C and inside a pressure vessel The onion peel extract can be prepared by heating for 3 to 5 hours in a pressure range of 2.5 to 3.5kgf/cm 2 .
본 발명은 상기와 같이 양파 껍질을 정제수에 침지시킨 후 추출함으로써, 양파 껍질의 식물벽을 약화시켜 추출 효율을 증대시킬 수 있다.According to the present invention, the onion peel is immersed in purified water and then extracted as described above, thereby weakening the plant wall of the onion peel to increase extraction efficiency.
그 다음으로, 상기 양파 과육 추출물 및 양파 껍질 추출물을 혼합함으로써 양파 추출물을 제조할 수 있는데, 상기 양파 추출물은 양파 과육 추출물 및 양파 껍질 추출물을 7:3 내지 6:4의 중량 비율로 혼합하여 제조될 수 있다.Next, an onion extract can be prepared by mixing the onion flesh extract and the onion peel extract, wherein the onion extract is prepared by mixing the onion flesh extract and the onion peel extract in a weight ratio of 7:3 to 6:4. I can.
이어서, 상기 양파 추출물을 3 내지 7℃의 온도에서 1 내지 5시간 보관함으로써 숙성시킬 수 있는데, 상기 양파 추출물을 상기와 같은 조건에서 숙성시킴으로써 상기 양파 추출물이 균일하게 혼합되고 향이 증진되게 할 수 있다.Subsequently, the onion extract may be aged by storing it for 1 to 5 hours at a temperature of 3 to 7°C. By aging the onion extract under the same conditions as described above, the onion extract may be uniformly mixed and the flavor may be enhanced.
이하, 본 발명에 따른 어성초 성분을 포함하는 두피 건강 개선용 스프레이 조성물에 대한 바람직한 실시예 및 비교예를 들어 더욱 상세하게 설명하기로 한다.Hereinafter, preferred examples and comparative examples for the spray composition for improving scalp health comprising the Eoseongcho component according to the present invention will be described in more detail.
< 실시예 1 ><Example 1>
어성초 추출액 3 중량부, 에탄올 70 중량부, 판테놀(Panthenol) 1 중량부, 소듐데하이드로아세테이트(Sodium Dehydroacetate) 0.5 중량부, 프로필렌글리콜(Propylene Glycol) 0.6 중량부, 유황(surfur) 0.3 중량부, 징크 글루코네이트(Zinc Gluconate) 0.02 중량부, 마그네슘 글루코네이트(Magnesium Gluconate) 0.08 중량부, 동백 오일 0.02 중량부, 디메치콘(Dimethicone) 0.03 중량부, 메타크릴로일에칠베타인(Methacryloyl Ethyl Betaine) 0.08 중량부 및 향료 0.008 중량부의 중량 비율로 포함된 스프레이 조성물을 이용하여 스프레이를 제조하였다.Eoseongcho extract 3 parts by weight, ethanol 70 parts by weight, Panthenol 1 part by weight, Sodium Dehydroacetate 0.5 parts by weight, Propylene Glycol 0.6 parts by weight, Sulfur (surfur) 0.3 parts by weight, Zinc Gluconate 0.02 parts by weight, Magnesium Gluconate 0.08 parts by weight, Camellia oil 0.02 parts by weight, Dimethicone 0.03 parts by weight, Methacryloyl Ethyl Betaine 0.08 A spray was prepared using a spray composition included in a weight ratio of 0.008 parts by weight and a fragrance.
< 실시예 2 ><Example 2>
상기 실시예 1과 동일한 조성물을 이용하여 스프레이를 제조하였는데, 실시예 2에서는 상기 어성초 추출액 100 중량부에 대해 산양삼 발효 추출액 20 중량부의 중량 비율로 더 포함되도록 하여 스프레이를 제조하였다.A spray was prepared using the same composition as in Example 1, but in Example 2, a spray was prepared by further including 20 parts by weight of the fermented wild ginseng extract with respect to 100 parts by weight of the Eoseongcho extract.
< 실시예 3 ><Example 3>
상기 실시예 1과 동일한 조성물을 이용하여 비누를 제조하였는데, 실시예 3에서는 상기 어성초 추출액 100 중량부에 대해 양파 추출물 10 중량부의 중량 비율로 더 포함되도록 하여 스프레이를 제조하였다.Soap was prepared using the same composition as in Example 1, and in Example 3, a spray was prepared by further including 10 parts by weight of onion extract with respect to 100 parts by weight of the Eoseongcho extract.
< 비교예 1 ><Comparative Example 1>
실시예 1과 동일한 조성물을 이용하여 스프레이를 제조하였는데, 비교예 1에서는 어성초 추출액 및 동백 오일이 포함되지 않도록 하였다.A spray was prepared using the same composition as in Example 1, but in Comparative Example 1, Eoseongcho extract and camellia oil were not included.
< 비교예 2 ><Comparative Example 2>
시중에 판매되고 있는 스프레이(W사 제조, 화학물질 사용)를 준비하였고, 이를 비교예 2에 따른 스프레이로 사용하였다.A commercially available spray (manufactured by W company, using a chemical substance) was prepared, and it was used as a spray according to Comparative Example 2.
1. 관능 평가1. Sensory evaluation
상기 실시예 1 내지 3과, 비교예 1 및 2에 따른 스프레이의 모발 지속 효과, 두피 자극, 두피 개선 및 모발 개선 효과를 측정하여 하기의 [표 1]에 나타내었다.The hair lasting effect, scalp irritation, scalp improvement and hair improvement effect of the sprays according to Examples 1 to 3 and Comparative Examples 1 and 2 were measured and shown in Table 1 below.
상기 실험은 10세에서 50세 사이의 건강한 20명(남자 7명, 여자 13명)을 대상으로 하였는데, 상기 스프레이를 하루에 15ml씩 20일 동안 사용하도록 한 후, 그 결과를 5점 척도법으로 측정하였다.The experiment was conducted on 20 healthy subjects (7 males and 13 females) between the ages of 10 and 50, and the spray was used 15 ml per day for 20 days, and the result was measured by a 5-point scale method. I did.
여기서, 5; 매우 우수, 4; 우수, 3; 보통, 2; 나쁨, 1;매우 나쁨을 나타낸다.Where, 5; Very good, 4; Excellent, 3; Usually, 2; Bad, 1; indicates very bad.
구분division 실시예 1Example 1 실시예 2Example 2 실시예 3Example 3 비교예 1Comparative Example 1 비교예 2Comparative Example 2
모발고정 지속효과Hair fixation lasting effect 4.34.3 4.24.2 4.34.3 3.23.2 4.04.0
두피 개선Scalp improvement 4.44.4 4.54.5 4.54.5 2.22.2 2.12.1
모발 개선Hair improvement 4.34.3 4.54.5 4.54.5 2.02.0 2.02.0
상기 [표 1]을 검토하면, 실시예 1 내지 3에 따른 스프레이는 모발 고정 효과가 우수함과 동시에 두피 및 모발 개선 효과가 우수한 것을 확인할 수 있었다.Examining the [Table 1], it was confirmed that the sprays according to Examples 1 to 3 had excellent hair fixing effects and excellent scalp and hair improvement effects.
이는, 실시예 1 내지 3에 따른 스프레이는 어성초 추출물, 산양삼 발효 추출액, 양파 추출물과 같은 천연 추출물이 포함됨으로써 사용자의 두피 및 모발의 개선에 기여함을 알 수 있었다.It was found that the spray according to Examples 1 to 3 included natural extracts such as Eoseongcho extract, fermented wild ginseng extract, and onion extract, thereby contributing to the improvement of the user's scalp and hair.
2. 스프레이의 자극 실험2. Spray stimulation test
상기와 같이 제조된 스프레이에 대한 자극 실험을 다음과 같이 실시하였다.The stimulation test for the spray prepared as described above was conducted as follows.
먼저, 자극 실험은 10세에서 50세 사이의 건강한 20명(남자 7명, 여자 13명)을 대상으로 하였는데, 상기 모발 샴푸 후 스프레이를 피험자의 모발에 분사하고, 3시간 후에 두피 상태(홍반, 부종, 구진 등)를 관찰하여 하기 [표 2]와 같은 평가표를 통한 정성적 평가를 수행하였다.First, the stimulation experiment targeted 20 healthy people (7 men, 13 women) between 10 and 50 years old.After the hair shampoo, spray was sprayed onto the hair of the subject, and after 3 hours the scalp condition (erythema, Edema, papules, etc.) were observed, and a qualitative evaluation was performed through an evaluation table as shown in [Table 2] below.
실험 항목Experiment item 주관적 점수Subjective score
자극 정도Degree of stimulation a: 두피가 많이 붉게 되고 가려움도 강하다a: The scalp becomes red and the itching is strong
b: 두피가 약간 붉게 되고 가려움이 있다b: The scalp is slightly red and itchy
c: 두피가 약간 붉게 되고 자극도 있다c: The scalp becomes slightly red and there is irritation.
d: 두피 상태는 변화 없으나 약간 자극이 있다d: There is no change in the condition of the scalp, but there is a slight irritation.
e: 두피 자극이나 두피 상태 변화 없다e: No scalp irritation or scalp condition change
상기 [표 2]의 자극 정도에 대한 실험 대상자의 평가 결과는 하기의 [표 3]와 같다.The evaluation results of the test subjects for the degree of stimulation in [Table 2] are shown in [Table 3] below.
실험 항목Experiment item 주관적 점수Subjective score 평가 결과Evaluation results
실시예 1Example 1 실시예 2Example 2 실시예 3Example 3 비교예 1Comparative Example 1 비교예 2Comparative Example 2
자극 정도Degree of stimulation aa -- -- -- -- --
bb -- -- -- -- --
cc -- -- -- 22 55
dd 1One 22 1One 66 88
ee 1919 1818 1919 1212 77
상기의 [표 3]에서 알 수 있는 바와 같이, 실시예 1 내지 3에 따른 스프레이는 자극이나 피부상태 변화가 거의 없는 안전한 물질임을 확인할 수 있었다.As can be seen from the above [Table 3], it was confirmed that the sprays according to Examples 1 to 3 were safe materials with little irritation or change in skin condition.
3. 세척 용이 실험3. Easy cleaning experiment
상기와 같이 제조된 스프레이에 대한 세척 용이 실험을 다음과 같이 실시하였다.The experiment for easy cleaning of the spray prepared as described above was conducted as follows.
먼저, 세척 용이 실험은 10세에서 50세 사이의 건강한 20명(남자 7명, 여자 13명)을 대상으로 하였는데, 모발에 스프레이를 10㎖ 분사하여 모발을 세팅하였고, 샴푸를 사용하여 세척한 경우 및 샴푸를 사용하지 않고 세척한 경우로 나누어 그 결과를 하기의 [표 4]에 나타내었다.First, the easy cleaning experiment was targeting 20 healthy people (7 men, 13 women) between the ages of 10 and 50 years, and the hair was set by spraying 10 ml of spray onto the hair, and washing with shampoo And washing without using shampoo, and the results are shown in Table 4 below.
◎: 헤어젤 성분이 거의 남아있지 않고, 세척 후 상쾌한 느낌이 난다.◎: There is almost no hair gel component left, and after washing, a fresh feeling is felt.
○: 헤어젤 성분이 어느 정도 제거되어 있고, 세척 후 상쾌한 느낌이 난다.○: The hair gel component has been removed to some extent, and after washing, a refreshing feeling is generated.
△: 헤어젤 성분이 어느 정도 제거되었으나, 세척 후 상쾌한 느낌은 나지 않는다.△: The hair gel component has been removed to some extent, but after washing, there is no refreshing feeling.
×: 헤어젤 성분이 거의 제거되지 않아, 세척 후 불쾌한 느낌이 난다.X: The hair gel component is hardly removed, and an unpleasant feeling occurs after washing.
구분division 실시예 1Example 1 실시예 2Example 2 실시예 3Example 3 비교예 1Comparative Example 1 비교예 2Comparative Example 2
샴푸를 사용한 경우When shampoo is used
샴푸를 사용하지 않은 경우When shampoo is not used
상기 [표 4]를 참조하면, 실시예 1 내지 3에 따라 제조된 스프레이는 샴푸 사용 유무에 관계없이 세척 후 스프레이 성분이 거의 남아있지 않고 상쾌한 느낌이 나는 것을 알 수 있었다.Referring to [Table 4], it was found that the sprays prepared according to Examples 1 to 3 had almost no spray components left after washing, regardless of the use of shampoo, and had a refreshing feeling.
4. 두피 자극 실험4. Scalp stimulation experiment
실시예 1에 따라 제조된 스프레이를 피험자(35세 여성)의 모발에 분사하여 피험자의 두피 상태를 관찰하였다.The spray prepared according to Example 1 was sprayed onto the hair of the subject (35 years old female) to observe the condition of the subject's scalp.
도 1a는 피험자의 두피를 보여주는 사진이고, 도 1b는 실시예 1에 따라 제조된 스프레이를 20일 동안 하루 15㎖씩 피험자의 모발에 분사 및 샴푸를 반복하였고, 20일이 경과한 후 피험자의 두피를 보여주는 사진이다.1A is a photograph showing the scalp of a subject, and FIG. 1B is a spray prepared according to Example 1 and spraying and shampooing on the subject's hair at 15 ml per day for 20 days, and after 20 days, the scalp of the subject This is a picture showing.
도 1a 및 도 1b를 참조하면, 실시예 1에 따라 제조된 스프레이는 사용 후 두피가 진정되었고 두피 건강이 개선되었음을 확인할 수 있었다.1A and 1B, it was confirmed that the spray prepared according to Example 1 calmed the scalp after use and improved scalp health.
이상, 본 발명의 바람직한 일 실시예를 설명하였지만, 본 발명이 속하는 기술분야에서 통상의 지식을 가진 자라면 본 발명이 그 기술적 사상이나 필수적인 특징을 변경하지 않고서 다른 구체적인 형태로 실시될 수 있다는 것을 이해할 수 있을 것이다. 그러므로 이상에서 기술한 일 실시예는 모든 면에서 예시적인 것이며 한정적이 아닌 것으로 이해해야만 한다.In the above, a preferred embodiment of the present invention has been described, but those of ordinary skill in the art to which the present invention pertains will understand that the present invention can be implemented in other specific forms without changing the technical spirit or essential features. I will be able to. Therefore, it should be understood that the exemplary embodiment described above is illustrative in all respects and is not limiting.

Claims (6)

  1. 어성초 추출액을 주요 성분으로 포함하는 것을 특징으로 하는 어성초 성분을 포함하는 두피 건강 개선용 스프레이 조성물.A spray composition for improving scalp health comprising an Eoseongcho component, characterized in that it contains Eoseongcho extract as a main component.
  2. 제 1항에 있어서,The method of claim 1,
    상기 어성초 추출액 이외에, 에탄올, 판테놀(Panthenol), 소듐데하이드로아세테이트(Sodium Dehydroacetate), 프로필렌글리콜(Propylene Glycol), 유황(surfur), 징크 글루코네이트(Zinc Gluconate), 마그네슘 글루코네이트(Magnesium Gluconate), 동백 오일, 디메치콘(Dimethicone), 메타크릴로일에칠베타인(Methacryloyl Ethyl Betaine) 및 향료를 포함하는 것을 특징으로 하는 어성초 성분을 포함하는 두피 건강 개선용 스프레이 조성물.In addition to the Eoseongcho extract, ethanol, Panthenol, Sodium Dehydroacetate, Propylene Glycol, Sulfur (surfur), Zinc Gluconate, Magnesium Gluconate, Camellia Oil, dimethicone (Dimethicone), methacryloyl ethyl betaine (Methacryloyl Ethyl Betaine), and a spray composition for improving scalp health comprising Eoseongcho ingredients, characterized in that it comprises a fragrance.
  3. 제 2항에 있어서,The method of claim 2,
    상기 조성물은 어성초 추출액 1 내지 5 중량부, 에탄올 60 내지 80 중량부, 판테놀(Panthenol) 0.5 내지 1.5 중량부, 소듐데하이드로아세테이트(Sodium Dehydroacetate) 0.1 내지 1 중량부, 프로필렌글리콜(Propylene Glycol) 0.3 내지 0.8 중량부, 유황(surfur) 0.1 내지 0.5 중량부, 징크 글루코네이트(Zinc Gluconate) 0.01 내지 0.03 중량부, 마그네슘 글루코네이트(Magnesium Gluconate) 0.05 내지 0.1 중량부, 동백 오일 0.005 내지 0.03 중량부, 디메치콘(Dimethicone) 0.025 내지 0.055 중량부, 메타크릴로일에칠베타인(Methacryloyl Ethyl Betaine) 0.05 내지 0.1 중량부 및 향료 0.005 내지 0.01 중량부의 중량 비율로 포함되는 것을 특징으로 하는 어성초 성분을 포함하는 두피 건강 개선용 스프레이 조성물.The composition comprises 1 to 5 parts by weight of Eoseongcho extract, 60 to 80 parts by weight of ethanol, 0.5 to 1.5 parts by weight of Panthenol, 0.1 to 1 part by weight of Sodium Dehydroacetate, and 0.3 to Propylene Glycol. 0.8 parts by weight, sulfur (surfur) 0.1 to 0.5 parts by weight, zinc gluconate 0.01 to 0.03 parts by weight, magnesium gluconate 0.05 to 0.1 parts by weight, camellia oil 0.005 to 0.03 parts by weight, dimethicone (Dimethicone) 0.025 to 0.055 parts by weight, Methacryloyl Ethyl Betaine (Methacryloyl Ethyl Betaine) 0.05 to 0.1 parts by weight and a fragrance containing 0.005 to 0.01 parts by weight of the scalp health including Eoseongcho ingredients Spray composition for improvement.
  4. 제 3항에 있어서,The method of claim 3,
    상기 어성초 추출액은, 어성초를 준비한 후 세척하고, 상기 세척된 어성초를 일정한 입도로 분쇄하되, 상기 어성초의 분쇄는 입경이 500 내지 2500㎛의 범위가 되도록 분쇄하며, 상기 분쇄된 어성초를 용매와 혼합하여 혼합액을 제조한 후, 초음파 추출기에 투입하여 상기 혼합액에 초음파를 가함으로써 어성초 추출 혼합액을 제조하되, 상기 용매는 상기 분쇄된 어성초 100 중량부에 대해 1000 내지 2000 중량부의 중량비율로 혼합되고, 상기 용매로는 물 또는 탄소수 1 내지 4의 알코올 중에서 선택된 어느 하나 이상의 용매가 사용되고, 20 내지 25℃의 온도 및 0.1 내지 0.5kgf/cm2의 압력하에서 상기 혼합액에 가해지는 초음파는 30 내지 50KHz의 진동주파수에서 30 내지 60분 동안 100 내지 200와트(watt)의 출력을 이용하여 추출하며, 상기 어성초 추출 혼합액에서 고형물을 제거한 후 10 내지 20℃의 온도에서 1 내지 3시간 동안 숙성함으로써 제조된 것을 특징으로 하는 어성초 성분을 포함하는 두피 건강 개선용 스프레이 조성물.The Eoseongcho extract is washed after preparing Eoseongcho, and the washed Eoseongcho is pulverized into a certain particle size, and the crushed Eoseongcho is pulverized so that the particle diameter is in the range of 500 to 2500㎛, and the pulverized Eoseongcho is mixed with a solvent. After preparing the mixed solution, the mixture was added to an ultrasonic extractor to apply ultrasonic waves to the mixed solution to prepare an Eoseongcho extract mixture, the solvent being mixed in a weight ratio of 1000 to 2000 parts by weight based on 100 parts by weight of the pulverized Eoseongcho, and the solvent As the furnace, any one or more solvents selected from water or alcohols having 1 to 4 carbon atoms are used, and the ultrasonic waves applied to the mixture at a temperature of 20 to 25°C and a pressure of 0.1 to 0.5 kgf/cm 2 are at a vibration frequency of 30 to 50 KHz. Eoseongcho, characterized in that it is extracted using an output of 100 to 200 watts for 30 to 60 minutes, and is prepared by aging for 1 to 3 hours at a temperature of 10 to 20°C after removing solids from the Eoseongcho extract mixture A spray composition for improving scalp health containing ingredients.
  5. 제 4항에 있어서,The method of claim 4,
    상기 어성초 추출액 이외에 산양삼 발효 추출액을 더 포함하되, 상기 산양삼 발효 추출액은 상기 어성초 추출액 100 중량부에 대해 10 내지 30 중량부의 중량 비율로 포함되는 것을 특징으로 하는 어성초 성분을 포함하는 두피 건강 개선용 스프레이 조성물.In addition to the Eoseongcho extract, further comprising a fermented wild wild ginseng extract, wherein the fermented wild wild ginseng extract is included in a weight ratio of 10 to 30 parts by weight with respect to 100 parts by weight of the Eoseongcho extract. .
  6. 제 1항 내지 제 5항 중 어느 하나의 조성물을 포함하여 제조된 것을 특징으로 하는 어성초 성분을 포함하는 두피 건강 개선용 스프레이.A spray for improving scalp health comprising a component of Eoseongcho, characterized in that it is prepared containing the composition of any one of claims 1 to 5.
PCT/KR2020/006632 2019-05-22 2020-05-21 Spray composition for improving scalp health containing eoseongcho component WO2020235941A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2021566333A JP7315986B2 (en) 2019-05-22 2020-05-21 Spray composition for improving scalp health containing Houttuynia cordata component

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR10-2019-0059879 2019-05-22
KR1020190059879A KR102063889B1 (en) 2019-05-22 2019-05-22 Spray composition for improving head skin comprising houttuynia cordata ingredient

Publications (1)

Publication Number Publication Date
WO2020235941A1 true WO2020235941A1 (en) 2020-11-26

Family

ID=69154082

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/KR2020/006632 WO2020235941A1 (en) 2019-05-22 2020-05-21 Spray composition for improving scalp health containing eoseongcho component

Country Status (3)

Country Link
JP (1) JP7315986B2 (en)
KR (1) KR102063889B1 (en)
WO (1) WO2020235941A1 (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102063889B1 (en) * 2019-05-22 2020-01-08 양숙현 Spray composition for improving head skin comprising houttuynia cordata ingredient
KR102174199B1 (en) * 2020-01-29 2020-11-04 양숙현 Manufacturing method for fermented oil of houttuynia cordata comprising wood-cultivated ginseng ingredient and fermented oil of houttuynia cordata manufactured by the same
KR102287369B1 (en) * 2021-04-12 2021-08-06 (주)배리어스랩 Composition for preventing hair loss

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20110112019A (en) * 2010-04-06 2011-10-12 전도용 Cosmetic composition for preventing hair loss and stimulating hair growth and method for preparing the same
KR20160043698A (en) * 2014-10-14 2016-04-22 주식회사 더네이처 Composition for treating hair or scalp to prevent hair loss
KR20170037694A (en) * 2015-09-25 2017-04-05 주식회사 씨앤비코스메틱 Cosmetic composition for protecting scalp and hair comprising wood cultivated ginseng extract
KR20170050222A (en) * 2015-10-30 2017-05-11 김인숙 The manufacturing method of shampoo composition for caring scalp and promoting hair growth, and shampoo composition thereof
KR102063889B1 (en) * 2019-05-22 2020-01-08 양숙현 Spray composition for improving head skin comprising houttuynia cordata ingredient

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH09241137A (en) * 1996-03-07 1997-09-16 Hoyu Co Ltd Hair crowing and restoring agent
JPH1017440A (en) * 1996-07-02 1998-01-20 Hoyu Co Ltd Hair growing and restoring agent
JP4883261B2 (en) * 2005-06-27 2012-02-22 ライオン株式会社 Hair cosmetics
JP2008001628A (en) * 2006-06-22 2008-01-10 Ichimaru Pharcos Co Ltd Hair cosmetic
JP5235049B2 (en) * 2006-07-25 2013-07-10 株式会社 資生堂 Aerosol hair cosmetics
KR20110041023A (en) 2009-10-15 2011-04-21 전창순 Hair spray food juice
KR20130010746A (en) 2011-07-19 2013-01-29 윤영준 A composition
JP2014162738A (en) * 2013-02-22 2014-09-08 Kracie Home Products Ltd Cosmetics and perspiration promoter
CN104547210B (en) * 2014-12-30 2017-09-29 广西百利乐生物科技有限公司 A kind of tcm product prevented and cure Car-sickness
KR101792747B1 (en) 2016-03-15 2017-11-07 (주) 컨템포 Composition for hair spray containing salt

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20110112019A (en) * 2010-04-06 2011-10-12 전도용 Cosmetic composition for preventing hair loss and stimulating hair growth and method for preparing the same
KR20160043698A (en) * 2014-10-14 2016-04-22 주식회사 더네이처 Composition for treating hair or scalp to prevent hair loss
KR20170037694A (en) * 2015-09-25 2017-04-05 주식회사 씨앤비코스메틱 Cosmetic composition for protecting scalp and hair comprising wood cultivated ginseng extract
KR20170050222A (en) * 2015-10-30 2017-05-11 김인숙 The manufacturing method of shampoo composition for caring scalp and promoting hair growth, and shampoo composition thereof
KR102063889B1 (en) * 2019-05-22 2020-01-08 양숙현 Spray composition for improving head skin comprising houttuynia cordata ingredient

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
NUBLY: "I Was Curious about All the Ingredients in the TS Shampoo", /BLOG.NAVER, 12 February 2018 (2018-02-12), XP055762867, Retrieved from the Internet <URL:https://blog.naver.com/PostView.nhn?blogId=ginam500&logNo=221207196655&redirect=Dlog> *

Also Published As

Publication number Publication date
KR102063889B1 (en) 2020-01-08
JP7315986B2 (en) 2023-07-27
JP2022533930A (en) 2022-07-27

Similar Documents

Publication Publication Date Title
WO2020235941A1 (en) Spray composition for improving scalp health containing eoseongcho component
KR102016002B1 (en) Cosmetic composition for improving skin-whitening, anti-wrinkle and head skin
WO2015133710A1 (en) Shampoo composition containing extracts of wild plants and natural medicinal herbs
WO2017115970A1 (en) Pack composition containing illite extract as active ingredient and pack containing same
WO2021137677A1 (en) Composition containing plant extract
WO2020226442A1 (en) Soap composition using mountain-cultivated ginseng, and soap comprising same
JP2008201773A (en) External preparation for skin
WO2021261975A1 (en) Vegetable extract comprising vegetable collagen and vegetable mucin, and method for preparing same
KR20200065339A (en) Manufacturing method using Dendropanax morbifera Lev and young barley leaves extraction fluid having whitening and anti-wrinkle activity
WO2017146414A1 (en) Composition for skin moisturization and skin wrinkle alleviation, containing α-terpineol as active ingredient
WO2024049120A1 (en) Cosmetic composition containing extract extracted by means of eco-friendly natural eutectic solvent
CN111228162A (en) Cosmetic composition containing Cucurbita pepo extract for whitening, resisting oxidation and keeping moisture, and its preparation method
JP3586321B2 (en) Cosmetics
WO2014168433A2 (en) Material composition for promoting hair growth, gray hair melanin regeneration and skin regeneration
KR20210068366A (en) A composition for skin whitening comprising enzymatic hydrolysates of protaetia brevitarsis larva
KR102127254B1 (en) Cosmetic composition for skin whitening and moisturing comprising natural extracts
WO2017142265A1 (en) Composition containing adipic acid as active ingredient for skin wrinkle alleviation and skin elasticity enhancement
WO2020032460A1 (en) Skin care cosmetic composition comprising onion extract
WO2019231244A1 (en) Soap composition and soap comprising same
KR20210006603A (en) Manufacturing method for cosmetics or improving condition of damaged hair
WO2020032296A1 (en) Functional composition
KR100628518B1 (en) Extract of Glycine Semen Germinatum and functional cosmetics for the skin-aging protection containing the same
KR102258166B1 (en) Hair shampoo composition for improving head skin
KR102266968B1 (en) Treatment composition for dyeing
CN109498469B (en) Walnut green seedcase hair blackening sunscreen spray and preparation method and application thereof

Legal Events

Date Code Title Description
121 Ep: the epo has been informed by wipo that ep was designated in this application

Ref document number: 20810246

Country of ref document: EP

Kind code of ref document: A1

ENP Entry into the national phase

Ref document number: 2021566333

Country of ref document: JP

Kind code of ref document: A

NENP Non-entry into the national phase

Ref country code: DE

122 Ep: pct application non-entry in european phase

Ref document number: 20810246

Country of ref document: EP

Kind code of ref document: A1