WO2019231244A1 - Soap composition and soap comprising same - Google Patents

Abstract

The present invention relates to a soap composition and a soap comprising same. A soap composition according to the present invention comprises bromelain and Luffa cylindrica extract as active ingredients. According to the above configuration, the present invention is safe for sensitive skin, has excellent cleansing power for contamination of body parts such as skin and hair, body odor, etc., is capable of removing keratin from feet through washing without additional care, and has acne-improving effects.

Description

Soap composition and soap comprising same

The present invention relates to a soap composition and a soap comprising the same, and more particularly safe to sensitive skin and excellent cleaning power for contamination of body parts such as skin and hair, body odor, etc. It relates to a soap composition having an acne improving effect and a soap comprising the same.

Soap is one of the necessities of life that is widely used in face and face washing in daily life. In particular, recently, cosmetic soaps containing various active ingredients have been developed and released in order to help clean the skin and to anticipate moisturizing or other effects.

In addition, various pigments and fragrances may be added to remove the odor peculiar to oils and oils and increase the value of the product. It is a generic term for metal salts such as saturated and unsaturated higher fatty acids, tor fatty acids, resin acids, and naphthenic acids. It is a water-soluble alkali metal salt of fatty acid.

As fatty acids, caproic acid to behenic acid are used. Alkali is usually sodium and potassium, but there are also organic bases such as ammonia, ethanolamine and guanidine.

The fatty acids are caproic acid to behenic acid. Alkali is generally sodium and potassium, but there are also organic bases such as ammonia, ethanolamine and guanidine. Only alkali metal salts and organic bases thereof are water and Since it melts at arbitrary ratios, it can be used for washing | cleaning. Metal salts other than those mentioned above are mostly insoluble in water and are distinguished as metal soap.

The main fragrances used are combination fragrances and products with added natural plant aromas are also preferred. Especially plants that have been used for skin care as a folk remedy for a long time (eg ginseng, cucumber, apricot, Products are being developed that are expressed by adding extracts of aloe, lemon, citron and wormwood, etc. or by combining the specific odors of these plants.

Although these soaps can be expected to have cleansing power and beauty effects according to the characteristics of each product, they still do not meet consumer demand for new products. It is excellent in the ability to clean the dirt, body odor, etc., and the development of soap that has excellent effect on removing acne on the feet and improving acne without additional care is insufficient.

Prior documents related to the technical field of the present invention include Korean Patent Registration No. 10-0942145 (registered on February 04, 2010), 10-1496624 (registered on February 17, 2015), and 10-1533766 (2015). June 29, 2008).

The present invention provides a soap composition and a soap containing the same, which is safe even for sensitive skin, and has excellent cleaning power against contamination of body parts such as skin and hair, body odor, etc. have.

Various problems to be solved by the present invention are not limited to the above-mentioned problems, and other tasks not mentioned will be clearly understood by those skilled in the art from the following description.

Soap composition according to the present invention comprises bromelain and scrubber extract as an active ingredient.

In addition to the bromelain and scrubber extract may further comprise a soap base and aloe vera leaf extract.

In addition to the bromelain and loofah extract may further include a soap base, aloe vera leaf extract and shea butter.

In addition, in addition to the bromelain and scrubber extract may further comprise a soap base, aloe vera leaf extract, shea butter and tocopherol (vitamin E).

In addition to the bromelain and scrubber extract, it may further include a soap base, aloe vera leaf extract, shea butter, tocopherol (vitamin E) and lavender oil.

Further, in addition to the bromelain and scrubber extract may further include a soap base, aloe vera leaf extract, shea butter, tocopherol (vitamin E), lavender oil and tea tree leaf oil.

Further, in addition to the bromelain and scrubber extract may further include a soap base, aloe vera leaf extract, shea butter, tocopherol (vitamin E), lavender oil, tea tree leaf oil and olive oil.

In addition to the bromelain and loofah extract may further comprise a soap base, aloe vera leaf extract, shea butter, tocopherol (vitamin E), lavender oil, tea tree leaf oil, olive oil and jojoba seed oil.

In addition to the bromelain and scrubber extract, it may further include a soap base, aloe vera leaf extract, shea butter, tocopherol (vitamin E), lavender oil, tea tree leaf oil, olive oil, jojoba seed oil and kaolin.

The bromelain and scrubber extract may be included in a weight ratio of 3-7 parts by weight of bromelline and 3-7 parts by weight of scrubber extract.

The soap base 920 to 960 parts by weight, bromelline 3 to 7 parts by weight, scrubber extract 3 to 7 parts by weight, aloe vera leaf extract 3 to 7 parts by weight, shea butter 3 to 7 parts by weight, tocopherol (vitamin E) 3 To 7 parts by weight, lavender oil 1 to 5 parts by weight, tea tree leaf oil 1 to 5 parts by weight, olive oil 1 to 5 parts by weight, jojoba seed oil 1 to 5 parts by weight, kaolin 7 to 13 parts by weight and flavoring 3 to It may be incorporated in a ratio of 7 parts by weight.

The pineapple extract is used instead of the bromelain, the pineapple extract is prepared after the pineapple, washed to remove foreign substances, the washing of the pineapple sodium hydrogen carbonate having a concentration range of 3 to 5 (w / w)% ( NaHCO ₃ ) using purified water dissolved for 5 to 10 minutes at a temperature of 25 to 35 ℃, and crushed the washed pineapple, the grinding of the pineapple is crushed to a diameter of 0.5 to 3cm, the pineapple Steaming, the steaming of the pineapple is carried out in a first steaming step and a second steaming step, wherein the first steaming step heats the ground pineapple with steam at a temperature of 65 to 75 ° C. for 5 to 20 minutes, and In the two steaming step, the heated pineapple is heated with steam at a temperature of 85 to 95 ° C. for 0.5 to 2 hours, and the pineapple is dried, but the pineapple is dried. Steamed pineapple is carried out for 30 to 150 minutes at a temperature of 60 to 70 ℃, to extract the dried pineapple to prepare a pineapple extract, the pineapple extract is (a) dried pineapple 1000 ~ 1200g 70% (v / v) First extraction with ethanol aqueous solution 10-12L for 3-4 hours at 85 to 90 ℃, then 70% (v / v) secondary extraction for 2 to 3 hours at 85 to 90 ℃ with 4-6L of ethanol aqueous solution To complete the step, preparing an extract until the 1000 to 1200ml in a vacuum rotary evaporator; (b) adding water to the extract 2 to 3 times, centrifuging at 14,000 to 15,000 rpm for 20 to 30 minutes to completely remove polymer fibers and solids, and then collecting the collected supernatant twice with 1.2 to 1.5 times chloroform. Extracting; And (c) removing the chloroform layer and extracting the aqueous layer three times with 1.2 to 1.5 times ethyl acetate to prepare a pineapple extract.

The scrubber extract, after preparing a scrubber fruit and scrubber root, scrubber fruit and root preparation and washing step of washing and removing foreign matter attached to the scrubber fruit and scrubber root; A scrubber fruit and root drying step of removing moisture by drying the scrubber fruit and scrubber root; After cutting the dried scrubber fruit and scrubber root, scrubber fruit and root cutting and separating step to separate the scrubber fruit and scrubber root; Fermentation yeast inoculation step of inoculating the yeast cultured in the separated scrubber fruit; Honey mixing step of mixing the honey to the scrubber inoculated with the yeast; Fermentation step of ripening the loofah loofah mixed with honey; A fermentation extract preparing step of extracting the fermented scrubber fruit to prepare a scrubber fruit fermentation extract; Preparing a separated scrubber root and heating the scrubber root to prepare a leachate; A heating extract preparation step of removing the scrubber root which is a solid from the heated bath leachate and then heating the leachate to prepare a scrubber root heating extract; And a scrubber fruit fermentation extract and a scrubber root heating extract may be prepared through an extract mixing step of preparing a scrubber extract.

Drying the scrubber fruit and scrubber roots for 1 to 5 days at a temperature of 20 to 30 ℃, dried so that the content of the moisture contained in the scrubber leaves and scrubber roots to 10 to 30% by weight, the honey In the mixing step, 10 to 30 parts by weight of honey is used for 100 parts by weight of the whole of the loofah inoculated scrubber, and the fermentation may be performed at a temperature of 20 to 30 ° C. for 3 to 10 days.

In the step of preparing the fermentation extract, any one or more solvents selected from the group consisting of water, C1 or C2 lower alcohol, acetone, ethyl acetate, butyl acetate, and 1,3 butylene glycol are used as extraction solvents. 200 to 500 parts by weight of a solvent is used based on 100 parts by weight of the fermented scrubber fruit, and in the heating step of the scrubber root bath, the mixture is mixed with a weight ratio of 1000 to 1500 parts by weight of water with respect to 100 parts by weight of the whole scrubber root. It may be carried out by heating to a temperature of from 160 ℃ to 1 to 5 hours.

In the heating extract preparation step, the bath-heated leachate is added to the extractor and then heated at a temperature of 130 to 140 ° C. and a pressure of 1 to 3 kgf / cm ² for 1 to 5 hours, thereby producing 1/5 to 2 of the first leachate. Heating to obtain a scrubber root heating extract, and the scrubber extract may be mixed at a weight ratio of 70 to 90 parts by weight of a scrubber fruit fermentation extract and 10 to 30 parts by weight of a scrubber root heating extract. have.

In addition, the present invention includes a soap prepared by including the composition described above.

Specific details of other embodiments are included in the detailed description.

The soap composition according to the present invention is safe even for sensitive skin and has excellent cleaning power against contamination of body parts such as skin and hair, body odor, etc., and removes keratin of the foot only by washing without additional management and has an acne-improving effect.

It will be fully understood that embodiments of the inventive concept may provide various effects that are not specifically mentioned.

Advantages and features of the present invention and methods for achieving them will be apparent with reference to the embodiments described below in detail. However, the present invention is not limited to the embodiments described herein and may be embodied in other forms. Rather, the embodiments introduced herein are provided so that the disclosure may be made thorough and complete, and to fully convey the spirit of the present invention to those skilled in the art.

The terminology used herein is for the purpose of describing particular example embodiments only and is not intended to be limiting of the present invention. Singular expressions include plural expressions unless the context clearly indicates otherwise.

Unless defined otherwise, all terms used herein, including technical or scientific terms, have the same meaning as commonly understood by one of ordinary skill in the art. Terms such as those defined in the commonly used dictionaries should be construed as having meanings consistent with the meanings in the context of the related art and shall not be construed in ideal or excessively formal meanings unless expressly defined in this application. Do not.

Hereinafter, the soap composition according to the present invention will be described in detail.

The soap composition according to the present invention comprises a soap base, bromelain, scrubber extract, aloe vera leaf extract, shea butter, tocopherol (vitamin E), lavender oil, tea tree leaf oil, olive oil, jojoba seed oil and kaolin A fragrance may be included in the soap composition in order to emit a soft scent.

At this time, the soap composition according to the present invention includes a bromelain and flush and extract, aloe vera leaf extract, shea butter, tocopherol (vitamin E), lavender oil, tea tree leaf oil, olive oil, jojoba seed oil and kaolin And one or more combinations thereof.

In addition, the soap composition according to the present invention is 920 to 960 parts by weight of soap base, 3 to 7 parts by weight of bromelain, 3 to 7 parts by weight of scrubber extract, 3 to 7 parts by weight of aloe vera leaf extract, 3 to 7 parts by weight of shea butter. Part, 3 to 7 parts by weight of tocopherol (vitamin E), 1 to 5 parts by weight of lavender oil, 1 to 5 parts by weight of tea tree leaf oil, 1 to 5 parts by weight of olive oil, 1 to 5 parts by weight of jojoba seed oil, kaolin 7 To 13 parts by weight and 3 to 7 parts by weight of the fragrance may be combined.

In addition, the soap composition according to the present invention may be included in the ratio of 3 to 7% by weight of the total content of the soap, when the soap composition is contained in less than 3% by weight, the effect of the soap composition according to the present invention is difficult to appear sufficiently Problems may arise, and when included in excess of 7% by weight, the increase of the effect may not be remarkable, and the problem of increasing the manufacturing cost may occur.

The soap base is a mixture of basic materials used to prepare the soap, and any soap base may be used as long as it is a soap base commonly used in the art.

The soap base includes vegetable oils, aqueous alkali solutions and natural oils. The vegetable oil (Vegetable oil, 植物性 油脂) is a fat that is taken from the plant as a liquid at room temperature, the oil (고체), the solid is called Ji (脂), ester of trihydric alcohol and fatty acid It is. Representative examples include palm oil, palm oil and palm kernel oil, and kakaoji. Since vegetable oils are extracted from natural plants, unlike animal and mineral oils that can cause skin problems, they can reduce direct irritation or troubles on the skin as much as possible, and it is effective in making skin moist and moist. Vegetable oil that can be used in the present invention can be used for all kinds of vegetable oil that can be commonly recognized by those skilled in the art, preferably olive oil, palm oil, coconut oil, etc. The vegetable oil is reacted with an aqueous alkali solution To produce soap.

The bromelain is a mixture of plant proteolytic enzymes extracted from the fruit and root of pineapple (Ananas comosus) and various compounds of other components not yet identified. It is a substance that breaks down muscle fibers well and is widely used for anticancer, antiplatelet, respiratory inflammation, indigestion, rheumatoid arthritis and mastitis. It is mainly used as an anti-inflammatory and anti-edema agent, and is known to be particularly effective for treating inflammation of soft tissues, traumatic events and post-operative tissue reactions. The inflammation treatment is known to occur by bromelain improves the nutritional supply to the inflammatory site, such as degradation of the fibrous layer of the inflammatory site, anti-edema, pain relief and improved blood circulation, and enhance immune function.

In other words, bromelain produced through the extraction and purification process of pineapple is a kind of vegetable proteinase, and it is well known that it has an excellent anti-inflammatory effect. The pharmacological action and characteristics of the bromelain, (1) the absorbed enzyme directly or indirectly through fibrinolytic enzyme system to indirectly decompose and remove the inflammatory products fibrin and denatured protein, (2) causing inflammation It is effective in the decomposition of attributable polypeptide, bradykinin, etc., (3) improves local circulation inhibited by inflammatory products, and (4) is a natural plant enzyme with no side effects. It is used as a raw material for fire extinguishing agents, and is an enzyme widely used as a meat softener or other additives in the food field.

In the present invention, the bromelain may include 3 to 7 parts by weight, and when the bromelain is included in the above range, the skin convergence, antioxidant and swelling alleviation effects may be further improved.

On the other hand, in the present invention, instead of using the bromelain, pineapple extract containing the bromelain component may be used.

The pineapple extract may be prepared by the following method.

First, the pineapple is prepared and washed to remove foreign substances.

The pineapple may be washed by using purified water in which sodium hydrogen carbonate (NaHCO ₃ ) is dissolved, and is then remaining on the surface of the pineapple by washing the surface of the pineapple using purified water in which sodium hydrogen carbonate is dissolved. It can improve the cleaning efficiency of pesticides, heavy metals and mold removal.

The sodium hydrogen carbonate (NaHCO ₃ ) is also used as a food additive, there is no toxicity and has a function of penetration, diffusion, expansion, etc. to clean the surface of the pineapple, the sodium hydrogen carbonate is 3 to 5 (w / w)% concentration range, it is preferred to wash for 5 to 10 minutes at a temperature of 25 to 35 ℃.

Next, the washed pineapple can be ground.

Grinding of the pineapple may be used by grinding the pineapple to a diameter of 0.5 to 3cm using a grinder or a blender in order to extract the active ingredient from the pineapple within a short time.

Next, the pineapple can be steamed.

Steaming of the pineapple is to steam the crushed pineapple by steaming with steam, in the present invention may be performed by the first steaming step and the second steaming step, that is, two stages of steaming in order to steam the pineapple effectively.

For example, in the steaming process of the pineapple, the first steaming step is heating the crushed pineapple with steam at a temperature of 65 to 75 ° C. for 5 to 20 minutes, and the second steaming step is heating the pineapple. Heating at 85 to 95 ° C. for 0.5 to 2 hours.

In the present invention, when the first steaming step is performed at a temperature of less than 65 ° C or less than 5 minutes, a problem may occur in that the surface and the outside of the pineapple are difficult to steam evenly by water vapor, and the temperature of more than 75 ° C or If it is performed for more than 20 minutes, the temperature of the surface and the inside of the pineapple may be uniformly preheated so that no further increase in effect may appear.

In addition, when the second steaming step is performed at a temperature of less than 85 ℃ or less than 0.5 hours, the pineapple is not sufficiently steamed, it is difficult to prepare the extract in a short time in a later process, the temperature of more than 95 ℃ or 2 hours When performed in excess, the active ingredient of the pineapple may be volatilized or the physical properties of the pineapple may be weakened.

Subsequently, the pineapple may be dried.

The drying of the pineapple may be performed for 30 to 150 minutes at the steamed pineapple at a temperature of 60 to 70 ℃, if the drying of the pineapple is performed at a temperature of less than 60 ℃ or less than 30 minutes the steamed pineapple Problems may be difficult to sufficiently remove the moisture remaining in, if the temperature is more than 70 ℃ or more than 150 minutes is carried out no further residual moisture or the physical properties of the pineapple may occur.

Next, the pineapple extract may be prepared by extracting the dried pineapple.

Extraction of the dried pineapple may use a known extraction method such as solvent extraction, hot water extraction or supercritical extraction, for example, the preparation of the pineapple extract (a) 70% (v) in 1000 ~ 1200g dried pineapple / v) First extraction with ethanol aqueous solution 10-12L for 3-4 hours at 85 to 90 ℃, then 70% (v / v) secondary extraction for 2 to 3 hours at 85 to 90 ℃ with 4-6L of ethanol aqueous solution To complete the step, preparing an extract until the 1000 to 1200ml in a vacuum rotary evaporator; (b) adding water to the extract 2 to 3 times dilution, centrifuging at 14,000 to 15,000 rpm for 20 to 30 minutes to completely remove the polymer fibers and solids, and then collect the collected supernatant twice with 1.2 to 1.5 times chloroform Extracting; And (c) removing the chloroform layer and extracting the aqueous layer three times with 1.2 to 1.5 times ethyl acetate to prepare a pineapple extract.

The scrubber extract may be prepared using a scrubber fruit and scrubber root, and the scrubber extract may be prepared by the following preparation method.

That is, the method for producing a scrubber extract according to the present invention includes (1) scrubber fruit and root preparation and washing step, (2) scrubber fruit and root drying step, (3) scrubber fruit and root cutting and separating step, (4) fermentation Yeast inoculation step, (5) honey mixing step, (6) fermentation step, (7) fermentation extract preparation step, (8) scrubber root bath heating step, (9) heating extract preparation step and (10) extract mixing step do.

(1) preparation and washing step of scrubber fruit and root

The scrubber fruit and root preparation and washing step is to prepare the scrubber fruit and scrubber root used to prepare the scrubber extract, and then to wash and remove the foreign matter attached to the scrubber fruit and scrubber root.

Cucumber scrubber has been widely used in folk medicine since ancient times, the root is excellent in the treatment effect of eczema, starch extracted by removing the epidermis of the root is known to be effective for skin diseases. In addition, the feature of the loofah extract is absorbed by the skin to absorb moisture, has a moisturizing, moisturizing activity, and because of this effect is also used as an anti-drying agent of the lips, acting on the stratum corneum to smooth the epidermis and smooth blood circulation.

The moisturizing active ingredient in loofah is mainly composed of saponin, amino acids and sugars, and has a high content of potassium. The presence of potassium imparts an activating effect to the moisturizing action when coexisted with saponins and shows anti-inflammatory action on the skin. This action is a plant that grows in summer and has strong vitality and moisture retention even with strong sunlight. By This ability plays a role in preventing the drying of leaves and fruits. Its absorption capacity is assumed to be achieved by potassium and anti-diffusion effect is achieved by saponin.

Cucumbers contain substances called saponin-like erythericin A (cukurvitacin di) and erraterin bi (cukurvitacin i), which are also effective against transplantation cancer of Sacoma 37. Known.

The saponin molecule is composed of hydrophilic and hydrophobic moieties to exhibit surface activity, thereby trapping moisture, and present in combination with inorganic salts such as potassium, magnesium, and calcium in plants. In addition, when decomposed under the influence of sunlight, inorganic salts such as sugar and potassium are dropped and triterpanoids such as saponins, and at this time, exhibits anti-inflammatory action along with the original moisturizing action.

(2) scrubbing brush and root drying step

The scrubber fruit and root drying step is to dry the scrubber fruit and scrubber root to remove moisture.

Drying of the scrubber fruit and scrubber root may be carried out using a variety of known drying methods such as sun drying or hot air drying, by drying the scrubber fruit and scrubber root for 1 to 5 days at a temperature of 20 to 30 ℃. , The content of the moisture contained in the scrubber leaves and scrubber root may be dried to 10 to 30% by weight.

In the present invention, when the moisture content of the scrubber fruit and scrubber root is less than 10% by weight, the useful components contained in the scrubber fruit and scrubber root may not be easily extracted, and when the content exceeds 30% by weight, the later fermentation process. The problem of delayed time may occur.

(3) Cutting and Separation of Scrubber Fruits and Roots

The loofah fruit and root cutting and separating step is a step of separating the loofah fruit and the loofah root after cutting the dried loofah fruit and loofah root.

In the loofah and root cutting and separating step, the length of the dried loofah fruit and the loofah root can be cut to 1 to 3 cm, by cutting the loofah fruit and the loofah root as described above, the loofah fruit in a later process Since the contact area with the honey to be advanced is widened, the useful ingredient contained in the scrubber fruit in the fermentation process with honey can be easily extracted and the fermentation process time can be shortened, and the scrubber root is heated in the subsequent process. Useful ingredients contained in the scrubber root can be easily extracted and the heating process time can be shortened.

(4) fermentation yeast inoculation step

The fermentation yeast inoculation step is a step of inoculating the yeast cultured in the separated scrubber fruit.

The yeast may be used Saccharomyces sp., Shigasoaccharomyces sp., Etc. Specifically, Saccharomyces cerevisiae , Saccharomyces cerevisiae, Sagecharomyces Schizosaccharomyces pombe , Klureromyceslactis and Saccharomyces boulardii ), it is preferable to use any one or more selected from the group consisting of.

In the present invention, the fermentation extract can be easily obtained because the useful components contained in the scrubber leaves are extracted together by the decomposition of the yeast in the process of fermenting the yeast by inoculating and fermenting the yeast into the scrubber fruit as described above. have.

(5) honey mixing step

The honey mixing step is a step of mixing honey to the scrubber fruit inoculated with the yeast.

In the honey mixing step, 10 to 30 parts by weight of honey may be used based on 100 parts by weight of the whole of the loofah inoculated with the yeast.

In general, honey is divided into natural honey honey and artificial honey molasses. Honey is defined as honey bees gathered from honeycomb of flowers and stored and matured in honeycomb. Collected fragrant and viscous sweet substance, stored in honeycomb by bees and the like, stored in the honeycomb, which has an acidic reaction and consists of two monosaccharides, sometimes containing more complex carbohydrates, minerals, vegetable pigments, enzymes, and pollen It is defined as.

This honey has been used for nourishing tonic, soothing, detoxification, fatigue, gastrointestinal disorders, cough, dry skin, eczema, constipation, nervous breakdown, hangover, etc. It is good for beauty and health, and contains abundant vitamin B group, especially B6 It relieves the bitter taste of Chinese medicine and is widely used as a mating agent in oriental medicine.

In particular, honey does not change at a high temperature (30 ~ 40 ℃) because of the strong sterilization power, in the present invention fermentation using properties that do not easily deteriorate even if the aging temperature of the scrubber fruit fermented with honey due to the sterilizing power of the honey as described above Extracts can be prepared.

(6) fermentation stage

The fermentation step is a step of fermenting by aging the scrubber fruit mixed with honey.

In the fermentation step, honey and yeast are mixed in the scrubber fruit, so that the useful components of the scrubber fruit can be micronized to a small size by decomposing the yeast without deteriorating the scrubber fruit.

In the present invention, the fermentation step may be carried out for 3 to 10 days at a temperature of 20 to 30 ℃, if the fermentation step is carried out below the lower limit, the scrubber fruit is not sufficiently fermented so that the active ingredient of the scrubber fruit A problem may occur that is not sufficiently extracted, and when performed beyond the above upper limit range, a problem of increasing the process cost may not occur without further significant effect increase over time.

(7) Fermentation Extract Preparation Step

The fermentation extract preparation step is to extract the fermented scrubber fruit to prepare a scrubber fruit fermentation extract.

In the step of preparing the fermentation extract, any one or more solvents selected from the group consisting of water, C1 or C2 lower alcohol, acetone, ethyl acetate, butyl acetate and 1,3 butylene glycol may be used as the extraction solvent. The solvent may be used in an amount of 200 to 500 parts by weight based on 100 parts by weight of the fermented scrubber fruit.

In addition, as the extraction method in the fermentation extract preparation step may be used, such as heat extraction, cold needle extraction, reflux cooling extraction and ultrasonic extraction, it can be used to extract once or multiple times, the extraction method is the art In the art, it is well known to those skilled in the art a detailed description thereof will be omitted.

(8) scrubber root bath heating step

The scrubber root bath heating step is to prepare a separated scrubber root and then heated the bath to prepare a leachate.

In the heating step of the scrubber root bath may be performed by putting the water in the bath so that the container containing the scrubber root does not directly touch the fire, and then heated the water, 1000 to 1500 weight of water based on 100 parts by weight of the whole scrubber root After mixing in a negative weight ratio, it may be carried out by heating to a temperature of 150 to 160 ℃ for 1 to 5 hours.

When the heating in the scrubber root bath heating step is carried out below the lower limit range, the useful components contained in the scrubber root may not be sufficiently leached, if the time is performed over the above upper limit range The problem of increasing the process cost may occur without further significant increase in effect.

(9) heating extract preparation step

The heating extract preparation step is a step of preparing a scrubber root heating extract by removing the scrubber root which is a solid from the heated bath leaching solution and then heating the leaching solution.

In the heating extract preparation step, the bath-heated leachate is added to the extractor and then heated at a temperature of 130 to 140 ° C. and a pressure of 1 to 3 kgf / cm ² for 1 to 5 hours, thereby producing 1/5 to 2 of the first leachate. The scrubber root heated extract can be prepared by heating until it reaches / 5.

When the heating of the heating extract preparation step is carried out below the lower limit, the moisture contained in the leachate may not be sufficiently removed, the viscosity of the extract may be too low, if performed above the upper limit The viscosity of the extract is too high, and the physical properties of the extract may be modified by excessive heating.

(10) Extract Mixing Step

The extract mixing step is to prepare a scrubber extract by mixing the scrubber fruit fermentation extract and scrubber root heating extract.

In the step of mixing the extract may be prepared scrubber extract by mixing the scrubber fruit fermentation extract and scrubber root heating extract, the scrubber extract is 70 to 90 parts by weight of scrubber fruit fermentation extract and 10 to 30 parts by weight of scrubber root heating extract Can be mixed in proportions.

In the present invention, the scrubber extract may include 3 to 7 parts by weight, when the scrubber extract is included in less than 3 parts by weight, the moisturizing, skin irritation preventing effect is not great, and when included in excess of 7 parts by weight soap unique May cause poor cleaning power and discoloration.

The aloe vera leaf extract is extracted from aloe vera, the aloe vera (Aloe Vera, Barbados aloe) is native to the Mediterranean region and Africa. Gel-containing sap contained in the leaves is known to be effective in treating burns and arthritis.

The aloe vera is a perennial perennial herb, the stem is 30-60 cm high, short and grows up to 100 cm. Long, hard leaves come out of this stem in rosette form. Leaves are 15-40cm long, 2-7cm wide, light green with white spots, thick, fleshy and succulent. It is wider at the bottom and narrower at the top. The back is round and the front is slightly indented. There is a serrated small gray spine on the edge. At the end of the leaves there are some grooves and the ends are sharp. Flowers like small coffins bloom in winter and spring. The flower is bright yellow or orange, and grows downward in the shape of gunshot inflorescence. It is easy to cultivate, resistant to pests, and has good oxygen production at night. It is also suitable for planting indoors such as bedrooms, living rooms, and offices, and is also widely used as a medicinal plant. It is used for various purposes such as raw materials of cosmetics and pharmaceuticals, edible, etc., and it has been found to be effective in disinfecting toxin, relieving fatigue and neutralizing skin, antipyretic, constipation and ulcer. Vitamin A, C, D, E, B12, fatty acids, amino acids, selenium, calcium and aloin (aloin), aloesin (aloesin) and contains about 300 different components. The distribution area of India, North Africa, and Manila is very wide. In the present invention, the aloe vera leaf extract may include 3 to 7 parts by weight.

The shea butter is a vegetable oil obtained from the fruit of the shea tree, which has been used for a long time as a folk remedy in Africa, to moisturize rough and dry skin to moisturize the skin, and it is very effective in regenerating wounds. It is known to be high and is widely used as a moisturizer and softener in cosmetics. In French, the sheer tree, called karite, grows in Mali, Cameroon, Congo, Ghana, Guinea, Senegal, Sudan, Nigeria, Burkina Faso, Uganda, and Cote d'Ivoire in Africa. Also known as Vitellaria paradoxa. In particular, the fruit of the shea tree is called shea butter because its appearance looks like butter. Shea butter is yellow-green fat, which has a good aroma and taste, and is used for food in West Africa. It is used as a substitute for cocoa butter when used with cocoa or chocolate. Shea butter is known to have antioxidant and anti-inflammatory effects in addition to skin moisturizing and regenerative effects. In addition, shea butter also has a sunscreen effect, which is approximately sun protection factor (SPF) of about 6. In addition, it stimulates the capillaries to make hair and scalp shine, increase nutrition and regeneration, so it is also used as a hair conditioner.

The tocopherol (vitamin E) has a natural moisturizing function to moisturize and hydrate dry skin and protects skin cell membranes from external invasion. That is, the skin prevents damage due to UV rays, pollutants, and aging, and it moisturizes deep into the skin, which helps skin respiration and metabolism, which is good for preventing wrinkles. In addition, the strong antioxidant action when used in natural soaps or cosmetics to prevent rancidity, increase the shelf life and protect cells and cell membranes from oxidative factors.

The lavender oil not only improves the fragrance of the soap, lavender oil helps to relieve stress and prevent and cure skin diseases, and is effective in alleviating skin allergies.

The tea tree leaf oil is effective for skin diseases caused by bacteria, acne, eczema, oily skin, athlete's foot, warts, insect bites, dandruff, wounds and effective in improving the immune system.

The olive oil is widely used in the Mediterranean region where olive trees are grown and used for cooking as well as makeup and treatment, and it is effective in treating various dermatitis and ulcers and improving skin and preventing and treating high blood pressure, diabetes and heart disease. It is rich in vitamin E and unsaturated fatty acids, so it is good for skin beauty. Massage makes skin moist and troubles, prevents skin aging, discharges waste and toxins, makes skin clear and glossy, and soothes skin troubles. . In the present invention, the olive oil may include 1 to 50 parts by weight.

The jojoba seed oil is an oil extracted by compressing a seed of a plant called jojoba growing in the desert, and is an oil extracted in the form of a liquid wax. The jojoba seed oil is well absorbed by the skin and delivers moisture to the skin without blocking pores, which is effective in balancing the skin. The jojoba seed oil is good for dry skin or aging skin, and forms a moisture film on the skin, thereby showing an excellent moisturizing effect that helps to prevent moisture from being deprived. In the present invention, the jojoba seed oil may include 1 to 5 parts by weight.

Kaolin (高嶺土, kaolin) is also known as kaolin, kaolin, and white clay (白 陶土: china clay), the main components are kaolinite and halosite. Feldspar, such as feldspar, feldspar, soda feldspar, and feldspar in rock, is produced by weathering, which is chemically decomposed by carbonic acid or water. Usually, several m thick layers are formed on the rocks of Wonseong soil. It is used as a raw material for porcelain, and it is called kaolin because it was produced a lot in China's Gao Ling. High-quality kaolin is light and bright because it does not contain iron, making it suitable for making thin bowls. It is commonly called white clay in Korea, and many fine white clay is produced in Hadong, Gyeongnam.

The kaolin serves as a white pigment to make the color of the soap clear and clean, and to serve to make the coloring well even if the pigment is added later. Therefore, if it is lower than the lower limit, it will not function properly as a white pigment, and if it is added above the upper limit, it will appear excessively white, and since it does not occur in harmony with other components, 7 to 13 parts by weight is used. It is desirable to.

The fragrance is added so as to emit a gentle scent to the soap, it is preferable to use a natural fragrance so as not to overdo the skin. The fragrance is a technique known in the art, the fragrance in the present invention is preferably used 3 to 7 parts by weight.

In the present invention, when the fragrance is included in less than 3 parts by weight, the effect that the fragrance is dissipated in the soap is insufficient, and when included in excess of 7 parts by weight, the fragrance is too strong to give the user an uncomfortable use of the soap For this reason, 3 to 7 parts by weight is preferably included.

Hereinafter, a preferred embodiment of the soap according to the present invention will be described in detail. However, the following examples are for illustrating the technical idea of the present invention, and the present invention is not limited to the following examples.

<Example>

94.95 parts by weight of soap base, 0.5 parts by weight of bromelain, 0.5 parts by weight of loofah extract, 0.5 parts by weight of aloe vera leaf extract, 0.5 parts by weight of shea butter, 0.3 parts by weight of tocopherol (vitamin E), 0.3 parts by weight of lavender oil, tea tree A soap was prepared by blending 0.3 parts by weight of leaf oil, 0.3 parts by weight of olive oil, 0.3 parts by weight of jojoba seed oil, 1 part by weight of kaolin and 0.5 parts by weight of perfume.

<Comparative Example>

A commercially available soap (manufactured by L Company) was prepared and used as a soap according to a comparative example.

1. Stimulation experiment of soap

Stimulation experiment on the soap prepared as described above was carried out as follows.

First, clinical trials were conducted on healthy 20 people (7 men, 13 women) between 10 and 50 years old. After washing the soap, skin condition (erythema, edema) after 3 hours without applying cosmetics or moisturizers , Papules, etc.) were observed to perform a qualitative evaluation through the evaluation table as shown in Table 1 below.

Experiment item	Subjective score
Stimulation degree	a: The skin is very red and itchy
	b: skin becomes slightly red and itchy
	c: skin is slightly red and irritated
	d: skin condition remains unchanged but slightly irritating
	e: No irritation or skin condition change

Evaluation results of the test subjects for the degree of stimulation of the [Table 1] are as shown in the following [Table 2].

Experiment item	Subjective score	Evaluation results
		Example	Comparative example
Stimulation degree	a: The skin is very red and itchy	-	-
	b: skin becomes slightly red and itchy	-	-
	c: skin is slightly red and irritated	-	-
	d: skin condition remains unchanged but slightly irritating	One	5
	e: No irritation or skin condition change	19	15

As can be seen from the above [Table 2], the soap according to the embodiment was confirmed that it is a safe substance with little irritation or stimulation, such as erythema, edema, almost no change in irritation or skin condition.

Soap according to the embodiment does not use synthetic surfactants, artificial colors, triclosan, preservatives (parabes), chemical moisturizers, microplastics, coagulants, thickeners, synthetic emulsifiers, etc. used in conventional conventional soaps safely used on sensitive skin Could confirm.

2. Skin irritation test of soap

Ten women aged 20 to 50 years after facial washing with soap according to the Examples and Comparative Examples, evaluated the facial skin irritation after 3 hours without applying cosmetics or moisturizers, the results are shown in Table 3 below Indicated.

The following evaluation was performed using a 5-point scale method, which was divided into 0 points-none, 1 points-very mild symptoms, 2 points-obvious symptoms, 3 points-slightly severe symptoms, 4 points-severe symptoms.

division	Example	Comparative example
Erythema formation	0	0
Crust formation	0	0
Edema formation	0	0
Itching	0	0
Acne formation	0	0

Referring to [Table 3], after washing with soap according to the Examples and Comparative Examples, it was reported that no symptoms such as erythema, itching, edema.

3. Skin elasticity, moisturizing and exfoliation experiment

In a survey of 10 women aged 20 to 50 years after washing the soap prepared according to the example three times a day for 2 weeks, the skin elasticity, moisturizing improvement and exfoliation were evaluated. Is shown in Table 4 below.

The evaluation was evaluated by a five-point scale method of 1 to 5 point scale, and the higher the score, the better.

division	Before use	after use
Skin moisturizer	2.1	3.4
Skin elasticity	2.3	3.4
Skin wrinkles	2.0	2.9
Skin blemishes, pigmentation	2.2	2.8
Skin tone	2.3	2.9
Exfoliation	2.4	3.7

Referring to [Table 4], in the survey conducted after washing the soap prepared according to the embodiment three times a day for two weeks, seven of the experimenters responded that the skin elasticity, moisturizing improvement and exfoliation improved Three of the respondents said they had improved significantly.

4. Formulation Stability Experiment

Formulation degree of the soap prepared according to the above example and the soap according to the comparative example was evaluated.

Evaluation of the formulation stabilization was carried out by confirming the phase stability by storing the soap samples according to the Examples and soap samples according to the comparative example for 30 days at a temperature of 40 ℃, room temperature, -20 ℃, respectively, the results It is shown in Table 5 below.

division	Example	Comparative example
40 ℃	Good	Good
Room temperature	Good	Good
-20 ℃	Good	Good

Referring to Table 6, soaps prepared according to Examples and soaps according to Comparative Examples were found to have good formulation stability.

5. Antibacterial activity evaluation experiment

In order to evaluate the antimicrobial activity of the soap prepared according to the embodiment was carried out the following experiment. In the antimicrobial activity evaluation experiment, propionibacterium acnes (Propionibacterium acnes ATCC 6919) was used as a test bacterium.

After acne bacteria were inoculated in BHI broth and preincubated, 100 ml of sterilized new BHI broth containing 5% of each composition was inoculated at a concentration of 1%, followed by incubation for 2 days in an anaerobic incubator. It was.

	P. acnes
	Inoculation bacteria concentration (cfu / ml)	Bacterial concentration after incubation (cfu / ml)
Example	2.15 x 10 6	2.32 x 10 4
Comparative example	2.15 x 10 6	5.89 x 10 5

Referring to [Table 6], it can be seen that the soap prepared according to the embodiment has greatly improved the antibacterial activity against acne bacteria.

Although one preferred embodiment of the present invention has been described above, those skilled in the art to which the present invention pertains understand that the present invention may be embodied in other specific forms without changing the technical spirit or essential features thereof. Could be. Therefore, it should be understood that one embodiment described above is illustrative in all respects and not restrictive.

Claims (17)

1. Soap composition, characterized in that it comprises bromelain and scrubber extract as an active ingredient.
2. The method of claim 1,

   Soap composition, characterized in that it further comprises a soap base and aloe vera leaf extract in addition to the bromelain and scrubber extract.
3. The method of claim 1,

   Soap composition, characterized in that it further comprises a soap base, aloe vera leaf extract and shea butter in addition to the bromelain and scrubber extract.
4. The method of claim 1,

   Soap composition, characterized in that it further comprises a soap base, aloe vera leaf extract, shea butter and tocopherol (vitamin E) in addition to the bromelain and scrubber extract.
5. The method of claim 1,

   Soap composition, characterized in that it further comprises a soap base, aloe vera leaf extract, shea butter, tocopherol (vitamin E) and lavender oil in addition to the bromelain and scrubber extract.
6. The method of claim 1,

   Soap composition, characterized in that it further comprises a soap base, aloe vera leaf extract, shea butter, tocopherol (vitamin E), lavender oil and tea tree leaf oil in addition to the bromelain and scrubber extract.
7. The method of claim 1,

   Soap composition, characterized in that it further comprises a soap base, aloe vera leaf extract, shea butter, tocopherol (vitamin E), lavender oil, tea tree leaf oil and olive oil in addition to the bromelain and scrubber extract.
8. The method of claim 1,

   Soap composition, characterized in that it further comprises a soap base, aloe vera leaf extract, shea butter, tocopherol (vitamin E), lavender oil, tea tree leaf oil, olive oil and jojoba seed oil in addition to the bromelain and scrubber extract.
9. The method of claim 1,

   Soap base, aloe vera leaf extract, shea butter, tocopherol (vitamin E), lavender oil, tea tree leaf oil, olive oil, jojoba seed oil and kaolin in addition to the bromelain and scrubber extract Composition.
10. The method of claim 1,

    The bromelain and scrubber extract is a soap composition, characterized in that it is blended in a weight ratio of 3 to 7 parts by weight of bromelline and 3 to 7 parts by weight of scrubber extract.
11. The method of claim 9,

    920 to 960 parts by weight of the soap base, 3 to 7 parts by weight of bromelain, 3 to 7 parts by weight of scrubber extract, 3 to 7 parts by weight of aloe vera leaf extract, 3 to 7 parts by weight of shea butter, tocopherol (vitamin E) 3 To 7 parts by weight, 1 to 5 parts by weight of lavender oil, 1 to 5 parts by weight of tea tree leaf oil, 1 to 5 parts by weight of olive oil, 1 to 5 parts by weight of jojoba seed oil and 7 to 13 parts by weight of kaolin Soap composition, characterized in that it is included.
12. The method of claim 11,

    Instead of the bromelain using pineapple extract,

    The pineapple extract,

    After the pineapple is prepared and washed to remove foreign substances, the pineapple is washed at a temperature of 25 to 35 ℃ using purified water in which sodium hydrogen carbonate (NaHCO ₃ ) having a concentration range of 3 to 5 (w / w)% dissolved Wash for 5-10 minutes,

    Grind the washed pineapple, the grinding of the pineapple is ground to a diameter of 0.5 to 3cm,

    Steaming the pineapple, the steaming of the pineapple is carried out in the first steaming step and the second steaming step, the first steaming step is to heat the crushed pineapple with steam of 65 to 75 ℃ temperature for 5 to 20 minutes The second steaming step is to heat the heated pineapple with steam at a temperature of 85 to 95 ℃ for 0.5 to 2 hours,

    Drying the pineapple, the pineapple is dried for 30 to 150 minutes at a temperature of 60 to 70 ℃ steamed pineapple,

    Pineapple extract is prepared by extracting the dried pineapple, but the pineapple extract is (a) dried pineapple 1000 ~ 1200g 70% (v / v) ethanol aqueous solution 10-12L for 3-4 hours at 85 ~ 90 ℃ After the first extraction, 70% (v / v) ethanol aqueous solution of 4-6 l to complete the second extraction for 2 to 3 hours at 85 to 90 ℃, to prepare an extract until the 1000 to 1200ml in a vacuum rotary evaporator Doing; (b) adding water to the extract 2 to 3 times dilution, centrifuging at 14,000 to 15,000 rpm for 20 to 30 minutes to completely remove the polymer fibers and solids, and then collect the collected supernatant twice with 1.2 to 1.5 times chloroform Extracting; And (c) removing the chloroform layer, and extracting the aqueous layer three times with 1.2 to 1.5 times ethyl acetate to prepare a pineapple extract.
13. The method of claim 1,

    The loofah extract,

    Preparing a scrubber fruit and a scrubber root, and preparing and washing a scrubber fruit and root to wash and remove foreign substances attached to the scrubber fruit and the scrubber root;

    A scrubber fruit and root drying step of removing moisture by drying the scrubber fruit and scrubber root;

    After cutting the dried scrubber fruit and scrubber root, scrubber fruit and root cutting and separating step to separate the scrubber fruit and scrubber root;

    Fermentation yeast inoculation step of inoculating the yeast cultured in the separated scrubber fruit;

    Honey mixing step of mixing the honey to the scrubber inoculated with the yeast;

    Fermentation step of ripening the loofah loofah mixed with honey;

    A fermentation extract preparing step of extracting the fermented scrubber fruit to prepare a scrubber fruit fermentation extract;

    Preparing a separated scrubber root and heating the scrubber root to prepare a leachate;

    A heating extract preparation step of removing the scrubber root which is a solid from the heated bath leachate and then heating the leachate to prepare a scrubber root heating extract; And

    Soap composition, characterized in that it is prepared through an extract mixture step of preparing a scrubber extract by mixing the scrubber fruit fermentation extract and scrubber root heating extract.
14. The method of claim 13,

    Drying the scrubber fruit and scrubber roots for 1 to 5 days at a temperature of 20 to 30 ℃, dried so that the content of the moisture contained in the scrubber leaves and scrubber root is 10 to 30% by weight,

    In the honey mixing step, 10 to 30 parts by weight of honey is used for 100 parts by weight of the whole of the loofah inoculated with the yeast,

    The fermentation step is a soap composition, characterized in that proceed for 3 to 10 days at a temperature of 20 to 30 ℃.
15. The method of claim 14,

    In the step of preparing the fermentation extract, any one or more solvents selected from the group consisting of water, C1 or C2 lower alcohol, acetone, ethyl acetate, butyl acetate, and 1,3 butylene glycol are used as extraction solvents. 200 to 500 parts by weight of the solvent is used based on 100 parts by weight of the whole of the fermented scrubber fruit,

    In the heating step of the scrubber root bath soap soap composition characterized in that it is carried out by mixing at a weight ratio of 1000 to 1500 parts by weight of water with respect to 100 parts by weight of the whole scrubber root and then heated to a temperature of 150 to 160 ℃ for 1 to 5 hours .
16. The method of claim 15,

    In the heating extract preparation step, the bath-heated leachate is added to the extractor and then heated at a temperature of 130 to 140 ° C. and a pressure of 1 to 3 kgf / cm ² for 1 to 5 hours, thereby producing 1/5 to 2 of the first leachate. Heat until it reaches / 5 to prepare a scrubbed root heating extract,

    In the extract mixing step, the scrubber extract is a soap composition, characterized in that the mixture of 70 to 90 parts by weight of the scrubber fruit fermentation extract and 10 to 30 parts by weight of the scrubber root heating extract.
17. A soap comprising the composition of any one of claims 1 to 16.