WO2019231244A1 - Composition de savon et savon comprenant ladite composition - Google Patents

Composition de savon et savon comprenant ladite composition Download PDF

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Publication number
WO2019231244A1
WO2019231244A1 PCT/KR2019/006464 KR2019006464W WO2019231244A1 WO 2019231244 A1 WO2019231244 A1 WO 2019231244A1 KR 2019006464 W KR2019006464 W KR 2019006464W WO 2019231244 A1 WO2019231244 A1 WO 2019231244A1
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WIPO (PCT)
Prior art keywords
scrubber
extract
weight
parts
pineapple
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PCT/KR2019/006464
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English (en)
Korean (ko)
Inventor
박영오
Original Assignee
Park Young Oh
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Publication of WO2019231244A1 publication Critical patent/WO2019231244A1/fr

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/38—Products in which the composition is not well defined
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/10—Washing or bathing preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A61Q5/02—Preparations for cleaning the hair
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/30—Organic compounds, e.g. vitamins containing nitrogen

Definitions

  • the present invention relates to a soap composition and a soap comprising the same, and more particularly safe to sensitive skin and excellent cleaning power for contamination of body parts such as skin and hair, body odor, etc. It relates to a soap composition having an acne improving effect and a soap comprising the same.
  • Soap is one of the necessities of life that is widely used in face and face washing in daily life.
  • cosmetic soaps containing various active ingredients have been developed and released in order to help clean the skin and to anticipate moisturizing or other effects.
  • various pigments and fragrances may be added to remove the odor peculiar to oils and oils and increase the value of the product. It is a generic term for metal salts such as saturated and unsaturated higher fatty acids, tor fatty acids, resin acids, and naphthenic acids. It is a water-soluble alkali metal salt of fatty acid.
  • caproic acid to behenic acid are used.
  • Alkali is usually sodium and potassium, but there are also organic bases such as ammonia, ethanolamine and guanidine.
  • the fatty acids are caproic acid to behenic acid.
  • Alkali is generally sodium and potassium, but there are also organic bases such as ammonia, ethanolamine and guanidine. Only alkali metal salts and organic bases thereof are water and Since it melts at arbitrary ratios, it can be used for washing
  • the main fragrances used are combination fragrances and products with added natural plant aromas are also preferred.
  • plants that have been used for skin care as a folk remedy for a long time eg ginseng, cucumber, apricot, Products are being developed that are expressed by adding extracts of aloe, lemon, citron and wormwood, etc. or by combining the specific odors of these plants.
  • soaps can be expected to have cleansing power and beauty effects according to the characteristics of each product, they still do not meet consumer demand for new products. It is excellent in the ability to clean the dirt, body odor, etc., and the development of soap that has excellent effect on removing acne on the feet and improving acne without additional care is insufficient.
  • Prior documents related to the technical field of the present invention include Korean Patent Registration No. 10-0942145 (registered on February 04, 2010), 10-1496624 (registered on February 17, 2015), and 10-1533766 (2015). June 29, 2008).
  • the present invention provides a soap composition and a soap containing the same, which is safe even for sensitive skin, and has excellent cleaning power against contamination of body parts such as skin and hair, body odor, etc. have.
  • Soap composition according to the present invention comprises bromelain and scrubber extract as an active ingredient.
  • bromelain and scrubber extract may further comprise a soap base and aloe vera leaf extract.
  • bromelain and loofah extract may further include a soap base, aloe vera leaf extract and shea butter.
  • bromelain and scrubber extract may further comprise a soap base, aloe vera leaf extract, shea butter and tocopherol (vitamin E).
  • bromelain and scrubber extract may further include a soap base, aloe vera leaf extract, shea butter, tocopherol (vitamin E) and lavender oil.
  • bromelain and scrubber extract may further include a soap base, aloe vera leaf extract, shea butter, tocopherol (vitamin E), lavender oil and tea tree leaf oil.
  • bromelain and scrubber extract may further include a soap base, aloe vera leaf extract, shea butter, tocopherol (vitamin E), lavender oil, tea tree leaf oil and olive oil.
  • bromelain and loofah extract may further comprise a soap base, aloe vera leaf extract, shea butter, tocopherol (vitamin E), lavender oil, tea tree leaf oil, olive oil and jojoba seed oil.
  • bromelain and scrubber extract may further include a soap base, aloe vera leaf extract, shea butter, tocopherol (vitamin E), lavender oil, tea tree leaf oil, olive oil, jojoba seed oil and kaolin.
  • the bromelain and scrubber extract may be included in a weight ratio of 3-7 parts by weight of bromelline and 3-7 parts by weight of scrubber extract.
  • lavender oil 1 to 5 parts by weight, tea tree leaf oil 1 to 5 parts by weight, olive oil 1 to 5 parts by weight, jojoba seed oil 1 to 5 parts by weight, kaolin 7 to 13 parts by weight and flavoring 3 to It may be incorporated in a ratio of 7 parts by weight.
  • the pineapple extract is used instead of the bromelain, the pineapple extract is prepared after the pineapple, washed to remove foreign substances, the washing of the pineapple sodium hydrogen carbonate having a concentration range of 3 to 5 (w / w)% ( NaHCO 3 ) using purified water dissolved for 5 to 10 minutes at a temperature of 25 to 35 °C, and crushed the washed pineapple, the grinding of the pineapple is crushed to a diameter of 0.5 to 3cm, the pineapple Steaming, the steaming of the pineapple is carried out in a first steaming step and a second steaming step, wherein the first steaming step heats the ground pineapple with steam at a temperature of 65 to 75 ° C.
  • the heated pineapple is heated with steam at a temperature of 85 to 95 ° C. for 0.5 to 2 hours, and the pineapple is dried, but the pineapple is dried.
  • Steamed pineapple is carried out for 30 to 150 minutes at a temperature of 60 to 70 °C, to extract the dried pineapple to prepare a pineapple extract, the pineapple extract is (a) dried pineapple 1000 ⁇ 1200g 70% (v / v) First extraction with ethanol aqueous solution 10-12L for 3-4 hours at 85 to 90 °C, then 70% (v / v) secondary extraction for 2 to 3 hours at 85 to 90 °C with 4-6L of ethanol aqueous solution To complete the step, preparing an extract until the 1000 to 1200ml in a vacuum rotary evaporator; (b) adding water to the extract 2 to 3 times, centrifuging at 14,000 to 15,000 rpm for 20 to 30 minutes to completely remove polymer fibers and solids, and then collecting the collected supernatant twice with 1.2 to 1.5
  • the scrubber extract after preparing a scrubber fruit and scrubber root, scrubber fruit and root preparation and washing step of washing and removing foreign matter attached to the scrubber fruit and scrubber root;
  • the honey drying the scrubber fruit and scrubber roots for 1 to 5 days at a temperature of 20 to 30 °C, dried so that the content of the moisture contained in the scrubber leaves and scrubber roots to 10 to 30% by weight, the honey
  • 10 to 30 parts by weight of honey is used for 100 parts by weight of the whole of the loofah inoculated scrubber, and the fermentation may be performed at a temperature of 20 to 30 ° C. for 3 to 10 days.
  • any one or more solvents selected from the group consisting of water, C1 or C2 lower alcohol, acetone, ethyl acetate, butyl acetate, and 1,3 butylene glycol are used as extraction solvents.
  • 200 to 500 parts by weight of a solvent is used based on 100 parts by weight of the fermented scrubber fruit, and in the heating step of the scrubber root bath, the mixture is mixed with a weight ratio of 1000 to 1500 parts by weight of water with respect to 100 parts by weight of the whole scrubber root. It may be carried out by heating to a temperature of from 160 °C to 1 to 5 hours.
  • the bath-heated leachate is added to the extractor and then heated at a temperature of 130 to 140 ° C. and a pressure of 1 to 3 kgf / cm 2 for 1 to 5 hours, thereby producing 1/5 to 2 of the first leachate.
  • Heating to obtain a scrubber root heating extract, and the scrubber extract may be mixed at a weight ratio of 70 to 90 parts by weight of a scrubber fruit fermentation extract and 10 to 30 parts by weight of a scrubber root heating extract. have.
  • the present invention includes a soap prepared by including the composition described above.
  • the soap composition according to the present invention is safe even for sensitive skin and has excellent cleaning power against contamination of body parts such as skin and hair, body odor, etc., and removes keratin of the foot only by washing without additional management and has an acne-improving effect.
  • the soap composition according to the present invention comprises a soap base, bromelain, scrubber extract, aloe vera leaf extract, shea butter, tocopherol (vitamin E), lavender oil, tea tree leaf oil, olive oil, jojoba seed oil and kaolin
  • a fragrance may be included in the soap composition in order to emit a soft scent.
  • the soap composition according to the present invention includes a bromelain and flush and extract, aloe vera leaf extract, shea butter, tocopherol (vitamin E), lavender oil, tea tree leaf oil, olive oil, jojoba seed oil and kaolin And one or more combinations thereof.
  • the soap composition according to the present invention is 920 to 960 parts by weight of soap base, 3 to 7 parts by weight of bromelain, 3 to 7 parts by weight of scrubber extract, 3 to 7 parts by weight of aloe vera leaf extract, 3 to 7 parts by weight of shea butter.
  • Part, 3 to 7 parts by weight of tocopherol (vitamin E), 1 to 5 parts by weight of lavender oil, 1 to 5 parts by weight of tea tree leaf oil, 1 to 5 parts by weight of olive oil, 1 to 5 parts by weight of jojoba seed oil, kaolin 7 To 13 parts by weight and 3 to 7 parts by weight of the fragrance may be combined.
  • the soap composition according to the present invention may be included in the ratio of 3 to 7% by weight of the total content of the soap, when the soap composition is contained in less than 3% by weight, the effect of the soap composition according to the present invention is difficult to appear sufficiently Problems may arise, and when included in excess of 7% by weight, the increase of the effect may not be remarkable, and the problem of increasing the manufacturing cost may occur.
  • the soap base is a mixture of basic materials used to prepare the soap, and any soap base may be used as long as it is a soap base commonly used in the art.
  • the soap base includes vegetable oils, aqueous alkali solutions and natural oils.
  • the vegetable oil (Vegetable oil, ⁇ ⁇ ) is a fat that is taken from the plant as a liquid at room temperature, the oil ( ⁇ ), the solid is called Ji ( ⁇ ), ester of trihydric alcohol and fatty acid It is.
  • Representative examples include palm oil, palm oil and palm kernel oil, and kakaoji. Since vegetable oils are extracted from natural plants, unlike animal and mineral oils that can cause skin problems, they can reduce direct irritation or troubles on the skin as much as possible, and it is effective in making skin moist and moist.
  • Vegetable oil that can be used in the present invention can be used for all kinds of vegetable oil that can be commonly recognized by those skilled in the art, preferably olive oil, palm oil, coconut oil, etc. The vegetable oil is reacted with an aqueous alkali solution To produce soap.
  • the bromelain is a mixture of plant proteolytic enzymes extracted from the fruit and root of pineapple (Ananas comosus) and various compounds of other components not yet identified. It is a substance that breaks down muscle fibers well and is widely used for anticancer, antiplatelet, respiratory inflammation, indigestion, rheumatoid arthritis and mastitis. It is mainly used as an anti-inflammatory and anti-edema agent, and is known to be particularly effective for treating inflammation of soft tissues, traumatic events and post-operative tissue reactions.
  • the inflammation treatment is known to occur by bromelain improves the nutritional supply to the inflammatory site, such as degradation of the fibrous layer of the inflammatory site, anti-edema, pain relief and improved blood circulation, and enhance immune function.
  • bromelain produced through the extraction and purification process of pineapple is a kind of vegetable proteinase, and it is well known that it has an excellent anti-inflammatory effect.
  • the pharmacological action and characteristics of the bromelain (1) the absorbed enzyme directly or indirectly through fibrinolytic enzyme system to indirectly decompose and remove the inflammatory products fibrin and denatured protein, (2) causing inflammation It is effective in the decomposition of attributable polypeptide, bradykinin, etc., (3) improves local circulation inhibited by inflammatory products, and (4) is a natural plant enzyme with no side effects. It is used as a raw material for fire extinguishing agents, and is an enzyme widely used as a meat softener or other additives in the food field.
  • the bromelain may include 3 to 7 parts by weight, and when the bromelain is included in the above range, the skin convergence, antioxidant and swelling alleviation effects may be further improved.
  • pineapple extract containing the bromelain component may be used instead of using the bromelain.
  • the pineapple extract may be prepared by the following method.
  • the pineapple is prepared and washed to remove foreign substances.
  • the pineapple may be washed by using purified water in which sodium hydrogen carbonate (NaHCO 3 ) is dissolved, and is then remaining on the surface of the pineapple by washing the surface of the pineapple using purified water in which sodium hydrogen carbonate is dissolved. It can improve the cleaning efficiency of pesticides, heavy metals and mold removal.
  • NaHCO 3 sodium hydrogen carbonate
  • the sodium hydrogen carbonate (NaHCO 3 ) is also used as a food additive, there is no toxicity and has a function of penetration, diffusion, expansion, etc. to clean the surface of the pineapple, the sodium hydrogen carbonate is 3 to 5 (w / w)% concentration range, it is preferred to wash for 5 to 10 minutes at a temperature of 25 to 35 °C.
  • the washed pineapple can be ground.
  • Grinding of the pineapple may be used by grinding the pineapple to a diameter of 0.5 to 3cm using a grinder or a blender in order to extract the active ingredient from the pineapple within a short time.
  • the pineapple can be steamed.
  • Steaming of the pineapple is to steam the crushed pineapple by steaming with steam, in the present invention may be performed by the first steaming step and the second steaming step, that is, two stages of steaming in order to steam the pineapple effectively.
  • the first steaming step is heating the crushed pineapple with steam at a temperature of 65 to 75 ° C. for 5 to 20 minutes
  • the second steaming step is heating the pineapple. Heating at 85 to 95 ° C. for 0.5 to 2 hours.
  • the first steaming step when the first steaming step is performed at a temperature of less than 65 ° C or less than 5 minutes, a problem may occur in that the surface and the outside of the pineapple are difficult to steam evenly by water vapor, and the temperature of more than 75 ° C or If it is performed for more than 20 minutes, the temperature of the surface and the inside of the pineapple may be uniformly preheated so that no further increase in effect may appear.
  • the second steaming step is performed at a temperature of less than 85 °C or less than 0.5 hours, the pineapple is not sufficiently steamed, it is difficult to prepare the extract in a short time in a later process, the temperature of more than 95 °C or 2 hours When performed in excess, the active ingredient of the pineapple may be volatilized or the physical properties of the pineapple may be weakened.
  • the pineapple may be dried.
  • the drying of the pineapple may be performed for 30 to 150 minutes at the steamed pineapple at a temperature of 60 to 70 °C, if the drying of the pineapple is performed at a temperature of less than 60 °C or less than 30 minutes the steamed pineapple Problems may be difficult to sufficiently remove the moisture remaining in, if the temperature is more than 70 °C or more than 150 minutes is carried out no further residual moisture or the physical properties of the pineapple may occur.
  • the pineapple extract may be prepared by extracting the dried pineapple.
  • Extraction of the dried pineapple may use a known extraction method such as solvent extraction, hot water extraction or supercritical extraction, for example, the preparation of the pineapple extract (a) 70% (v) in 1000 ⁇ 1200g dried pineapple / v) First extraction with ethanol aqueous solution 10-12L for 3-4 hours at 85 to 90 °C, then 70% (v / v) secondary extraction for 2 to 3 hours at 85 to 90 °C with 4-6L of ethanol aqueous solution To complete the step, preparing an extract until the 1000 to 1200ml in a vacuum rotary evaporator; (b) adding water to the extract 2 to 3 times dilution, centrifuging at 14,000 to 15,000 rpm for 20 to 30 minutes to completely remove the polymer fibers and solids, and then collect the collected supernatant twice with 1.2 to 1.5 times chloroform Extracting; And (c) removing the chloroform layer and extracting the aqueous layer three times with 1.2 to 1.5 times ethyl acetate to prepare a pineapple
  • the scrubber extract may be prepared using a scrubber fruit and scrubber root, and the scrubber extract may be prepared by the following preparation method.
  • the method for producing a scrubber extract according to the present invention includes (1) scrubber fruit and root preparation and washing step, (2) scrubber fruit and root drying step, (3) scrubber fruit and root cutting and separating step, (4) fermentation Yeast inoculation step, (5) honey mixing step, (6) fermentation step, (7) fermentation extract preparation step, (8) scrubber root bath heating step, (9) heating extract preparation step and (10) extract mixing step do.
  • the scrubber fruit and root preparation and washing step is to prepare the scrubber fruit and scrubber root used to prepare the scrubber extract, and then to wash and remove the foreign matter attached to the scrubber fruit and scrubber root.
  • Cucumber scrubber has been widely used in folk medicine since ancient times, the root is excellent in the treatment effect of eczema, starch extracted by removing the epidermis of the root is known to be effective for skin diseases.
  • the feature of the loofah extract is absorbed by the skin to absorb moisture, has a moisturizing, moisturizing activity, and because of this effect is also used as an anti-drying agent of the lips, acting on the stratum corneum to smooth the epidermis and smooth blood circulation.
  • the moisturizing active ingredient in loofah is mainly composed of saponin, amino acids and sugars, and has a high content of potassium.
  • the presence of potassium imparts an activating effect to the moisturizing action when coexisted with saponins and shows anti-inflammatory action on the skin.
  • This action is a plant that grows in summer and has strong vitality and moisture retention even with strong sunlight. By This ability plays a role in preventing the drying of leaves and fruits. Its absorption capacity is assumed to be achieved by potassium and anti-diffusion effect is achieved by saponin.
  • Cucumbers contain substances called saponin-like erythericin A (cukurvitacin di) and erraterin bi (cukurvitacin i), which are also effective against transplantation cancer of Sacoma 37. Known.
  • the saponin molecule is composed of hydrophilic and hydrophobic moieties to exhibit surface activity, thereby trapping moisture, and present in combination with inorganic salts such as potassium, magnesium, and calcium in plants.
  • inorganic salts such as sugar and potassium are dropped and triterpanoids such as saponins, and at this time, exhibits anti-inflammatory action along with the original moisturizing action.
  • the scrubber fruit and root drying step is to dry the scrubber fruit and scrubber root to remove moisture.
  • Drying of the scrubber fruit and scrubber root may be carried out using a variety of known drying methods such as sun drying or hot air drying, by drying the scrubber fruit and scrubber root for 1 to 5 days at a temperature of 20 to 30 °C. , The content of the moisture contained in the scrubber leaves and scrubber root may be dried to 10 to 30% by weight.
  • the moisture content of the scrubber fruit and scrubber root when the moisture content of the scrubber fruit and scrubber root is less than 10% by weight, the useful components contained in the scrubber fruit and scrubber root may not be easily extracted, and when the content exceeds 30% by weight, the later fermentation process. The problem of delayed time may occur.
  • the loofah fruit and root cutting and separating step is a step of separating the loofah fruit and the loofah root after cutting the dried loofah fruit and loofah root.
  • the length of the dried loofah fruit and the loofah root can be cut to 1 to 3 cm, by cutting the loofah fruit and the loofah root as described above, the loofah fruit in a later process Since the contact area with the honey to be advanced is widened, the useful ingredient contained in the scrubber fruit in the fermentation process with honey can be easily extracted and the fermentation process time can be shortened, and the scrubber root is heated in the subsequent process. Useful ingredients contained in the scrubber root can be easily extracted and the heating process time can be shortened.
  • the fermentation yeast inoculation step is a step of inoculating the yeast cultured in the separated scrubber fruit.
  • the yeast may be used Saccharomyces sp., Shigasoaccharomyces sp., Etc. Specifically, Saccharomyces cerevisiae , Saccharomyces cerevisiae, Sagecharomyces Schizosaccharomyces pombe , Klureromyceslactis and Saccharomyces boulardii ), it is preferable to use any one or more selected from the group consisting of.
  • the fermentation extract can be easily obtained because the useful components contained in the scrubber leaves are extracted together by the decomposition of the yeast in the process of fermenting the yeast by inoculating and fermenting the yeast into the scrubber fruit as described above. have.
  • the honey mixing step is a step of mixing honey to the scrubber fruit inoculated with the yeast.
  • honey mixing step 10 to 30 parts by weight of honey may be used based on 100 parts by weight of the whole of the loofah inoculated with the yeast.
  • honey is divided into natural honey honey and artificial honey molasses.
  • Honey is defined as honey bees gathered from honeycomb of flowers and stored and matured in honeycomb. Collected fragrant and viscous sweet substance, stored in honeycomb by bees and the like, stored in the honeycomb, which has an acidic reaction and consists of two monosaccharides, sometimes containing more complex carbohydrates, minerals, vegetable pigments, enzymes, and pollen It is defined as.
  • This honey has been used for nourishing tonic, soothing, detoxification, fatigue, gastrointestinal disorders, cough, dry skin, eczema, constipation, nervous breakdown, hangover, etc. It is good for beauty and health, and contains abundant vitamin B group, especially B6 It relieves the bitter taste of Chinese medicine and is widely used as a mating agent in oriental medicine.
  • honey does not change at a high temperature (30 ⁇ 40 °C) because of the strong sterilization power
  • fermentation using properties that do not easily deteriorate even if the aging temperature of the scrubber fruit fermented with honey due to the sterilizing power of the honey as described above Extracts can be prepared.
  • the fermentation step is a step of fermenting by aging the scrubber fruit mixed with honey.
  • honey and yeast are mixed in the scrubber fruit, so that the useful components of the scrubber fruit can be micronized to a small size by decomposing the yeast without deteriorating the scrubber fruit.
  • the fermentation step may be carried out for 3 to 10 days at a temperature of 20 to 30 °C, if the fermentation step is carried out below the lower limit, the scrubber fruit is not sufficiently fermented so that the active ingredient of the scrubber fruit A problem may occur that is not sufficiently extracted, and when performed beyond the above upper limit range, a problem of increasing the process cost may not occur without further significant effect increase over time.
  • the fermentation extract preparation step is to extract the fermented scrubber fruit to prepare a scrubber fruit fermentation extract.
  • any one or more solvents selected from the group consisting of water, C1 or C2 lower alcohol, acetone, ethyl acetate, butyl acetate and 1,3 butylene glycol may be used as the extraction solvent.
  • the solvent may be used in an amount of 200 to 500 parts by weight based on 100 parts by weight of the fermented scrubber fruit.
  • the extraction method in the fermentation extract preparation step may be used, such as heat extraction, cold needle extraction, reflux cooling extraction and ultrasonic extraction, it can be used to extract once or multiple times, the extraction method is the art In the art, it is well known to those skilled in the art a detailed description thereof will be omitted.
  • the scrubber root bath heating step is to prepare a separated scrubber root and then heated the bath to prepare a leachate.
  • the heating step of the scrubber root bath may be performed by putting the water in the bath so that the container containing the scrubber root does not directly touch the fire, and then heated the water, 1000 to 1500 weight of water based on 100 parts by weight of the whole scrubber root After mixing in a negative weight ratio, it may be carried out by heating to a temperature of 150 to 160 °C for 1 to 5 hours.
  • the heating extract preparation step is a step of preparing a scrubber root heating extract by removing the scrubber root which is a solid from the heated bath leaching solution and then heating the leaching solution.
  • the bath-heated leachate is added to the extractor and then heated at a temperature of 130 to 140 ° C. and a pressure of 1 to 3 kgf / cm 2 for 1 to 5 hours, thereby producing 1/5 to 2 of the first leachate.
  • the scrubber root heated extract can be prepared by heating until it reaches / 5.
  • the heating of the heating extract preparation step When the heating of the heating extract preparation step is carried out below the lower limit, the moisture contained in the leachate may not be sufficiently removed, the viscosity of the extract may be too low, if performed above the upper limit The viscosity of the extract is too high, and the physical properties of the extract may be modified by excessive heating.
  • the extract mixing step is to prepare a scrubber extract by mixing the scrubber fruit fermentation extract and scrubber root heating extract.
  • the extract may be prepared scrubber extract by mixing the scrubber fruit fermentation extract and scrubber root heating extract, the scrubber extract is 70 to 90 parts by weight of scrubber fruit fermentation extract and 10 to 30 parts by weight of scrubber root heating extract Can be mixed in proportions.
  • the scrubber extract may include 3 to 7 parts by weight, when the scrubber extract is included in less than 3 parts by weight, the moisturizing, skin irritation preventing effect is not great, and when included in excess of 7 parts by weight soap unique May cause poor cleaning power and discoloration.
  • the aloe vera leaf extract is extracted from aloe vera, the aloe vera (Aloe Vera, Barbados aloe) is native to the Mediterranean region and Africa. Gel-containing sap contained in the leaves is known to be effective in treating burns and arthritis.
  • the aloe vera is a perennial perennial herb, the stem is 30-60 cm high, short and grows up to 100 cm. Long, hard leaves come out of this stem in rosette form. Leaves are 15-40cm long, 2-7cm wide, light green with white spots, thick, fleshy and succulent. It is wider at the bottom and narrower at the top. The back is round and the front is slightly indented. There is a serrated small gray spine on the edge. At the end of the leaves there are some grooves and the ends are sharp. Flowers like small coffins bloom in winter and spring. The flower is bright yellow or orange, and grows downward in the shape of gunshot inflorescence. It is easy to cultivate, resistant to pests, and has good oxygen production at night.
  • the distribution area of India, North Africa, and Manila is very wide.
  • the aloe vera leaf extract may include 3 to 7 parts by weight.
  • the shea butter is a vegetable oil obtained from the fruit of the shea tree, which has been used for a long time as a folk remedy in Africa, to moisturize rough and dry skin to moisturize the skin, and it is very effective in regenerating wounds. It is known to be high and is widely used as a moisturizer and softener in cosmetics.
  • the sheer tree called karite, grows in Mali, Cameroon, Congo, Ghana, Guinea, Senegal, Sudan, Nigeria, Burkina Faso, Kenya, and Cote d'Ivoire in Africa. Also known as Vitellaria paradoxa.
  • the fruit of the shea tree is called shea butter because its appearance looks like butter.
  • Shea butter is yellow-green fat, which has a good aroma and taste, and is used for food in West Africa. It is used as a substitute for cocoa butter when used with cocoa or chocolate. Shea butter is known to have antioxidant and anti-inflammatory effects in addition to skin moisturizing and regenerative effects. In addition, shea butter also has a sunscreen effect, which is approximately sun protection factor (SPF) of about 6. In addition, it stimulates the capillaries to make hair and scalp shine, increase nutrition and regeneration, so it is also used as a hair conditioner.
  • SPDF sun protection factor
  • the tocopherol (vitamin E) has a natural moisturizing function to moisturize and hydrate dry skin and protects skin cell membranes from external invasion. That is, the skin prevents damage due to UV rays, pollutants, and aging, and it moisturizes deep into the skin, which helps skin respiration and metabolism, which is good for preventing wrinkles.
  • the strong antioxidant action when used in natural soaps or cosmetics to prevent rancidity increase the shelf life and protect cells and cell membranes from oxidative factors.
  • the lavender oil not only improves the fragrance of the soap, lavender oil helps to relieve stress and prevent and cure skin diseases, and is effective in alleviating skin allergies.
  • the tea tree leaf oil is effective for skin diseases caused by bacteria, acne, eczema, oily skin, athlete's foot, warts, insect bites, dandruff, wounds and effective in improving the immune system.
  • the olive oil is widely used in the Mediterranean region where olive trees are grown and used for cooking as well as makeup and treatment, and it is effective in treating various dermatitis and ulcers and improving skin and preventing and treating high blood pressure, diabetes and heart disease. It is rich in vitamin E and unsaturated fatty acids, so it is good for skin beauty. Massage makes skin moist and troubles, prevents skin aging, discharges waste and toxins, makes skin clear and glossy, and soothes skin troubles. .
  • the olive oil may include 1 to 50 parts by weight.
  • the jojoba seed oil is an oil extracted by compressing a seed of a plant called jojoba growing in the desert, and is an oil extracted in the form of a liquid wax.
  • the jojoba seed oil is well absorbed by the skin and delivers moisture to the skin without blocking pores, which is effective in balancing the skin.
  • the jojoba seed oil is good for dry skin or aging skin, and forms a moisture film on the skin, thereby showing an excellent moisturizing effect that helps to prevent moisture from being deprived.
  • the jojoba seed oil may include 1 to 5 parts by weight.
  • Kaolin ( ⁇ , kaolin) is also known as kaolin, kaolin, and white clay ( ⁇ ⁇ : china clay), the main components are kaolinite and halosite.
  • Feldspar such as feldspar, feldspar, soda feldspar, and feldspar in rock, is produced by weathering, which is chemically decomposed by carbonic acid or water. Usually, several m thick layers are formed on the rocks of Wonseong soil. It is used as a raw material for porcelain, and it is called kaolin because it was produced a lot in China's Gao Ling. High-quality kaolin is light and bright because it does not contain iron, making it suitable for making thin bowls. It is commonly called white clay in Korea, and many fine white clay is produced in Hadong, Gyeongnam.
  • the kaolin serves as a white pigment to make the color of the soap clear and clean, and to serve to make the coloring well even if the pigment is added later. Therefore, if it is lower than the lower limit, it will not function properly as a white pigment, and if it is added above the upper limit, it will appear excessively white, and since it does not occur in harmony with other components, 7 to 13 parts by weight is used. It is desirable to.
  • the fragrance is added so as to emit a gentle scent to the soap, it is preferable to use a natural fragrance so as not to overdo the skin.
  • the fragrance is a technique known in the art, the fragrance in the present invention is preferably used 3 to 7 parts by weight.
  • the fragrance when the fragrance is included in less than 3 parts by weight, the effect that the fragrance is dissipated in the soap is insufficient, and when included in excess of 7 parts by weight, the fragrance is too strong to give the user an uncomfortable use of the soap For this reason, 3 to 7 parts by weight is preferably included.
  • soap base 0.5 parts by weight of bromelain, 0.5 parts by weight of loofah extract, 0.5 parts by weight of aloe vera leaf extract, 0.5 parts by weight of shea butter, 0.3 parts by weight of tocopherol (vitamin E), 0.3 parts by weight of lavender oil, tea tree A soap was prepared by blending 0.3 parts by weight of leaf oil, 0.3 parts by weight of olive oil, 0.3 parts by weight of jojoba seed oil, 1 part by weight of kaolin and 0.5 parts by weight of perfume.
  • a commercially available soap (manufactured by L Company) was prepared and used as a soap according to a comparative example.
  • the soap according to the embodiment was confirmed that it is a safe substance with little irritation or stimulation, such as erythema, edema, almost no change in irritation or skin condition.
  • Soap according to the embodiment does not use synthetic surfactants, artificial colors, triclosan, preservatives (parabes), chemical moisturizers, microplastics, coagulants, thickeners, synthetic emulsifiers, etc. used in conventional conventional soaps safely used on sensitive skin could confirm.
  • the following evaluation was performed using a 5-point scale method, which was divided into 0 points-none, 1 points-very mild symptoms, 2 points-obvious symptoms, 3 points-slightly severe symptoms, 4 points-severe symptoms.
  • the evaluation was evaluated by a five-point scale method of 1 to 5 point scale, and the higher the score, the better.
  • propionibacterium acnes Propionibacterium acnes ATCC 6919 was used as a test bacterium.
  • the soap prepared according to the embodiment has greatly improved the antibacterial activity against acne bacteria.

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Abstract

La présente invention concerne une composition de savon et un savon comprenant ladite composition. Selon la présente invention, la composition de savon comprend de la bromélaïne et un extrait de Luffa cylindrica en tant que principes actifs. Selon la configuration ci-dessus, la présente invention est sûre pour la peau sensible, possède un excellent pouvoir nettoyant pour la contamination de parties corporelles telles que la peau et les cheveux, pour une odeur corporelle, etc., est apte à éliminer la kératine des pieds par lavage sans soins supplémentaires et possède des effets d'atténuation de l'acné.
PCT/KR2019/006464 2018-05-29 2019-05-29 Composition de savon et savon comprenant ladite composition WO2019231244A1 (fr)

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WO2023085959A1 (fr) * 2021-11-12 2023-05-19 Aflofarm Farmacja Polska Sp Z Oo Composition cosmétique pour l'exfoliation enzymatique trichologique du cuir chevelu et son procédé d'obtention

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