WO2020235941A1 - Composition de pulvérisation pour améliorer la santé du cuir chevelu contenant un composant eoseongcho - Google Patents

Composition de pulvérisation pour améliorer la santé du cuir chevelu contenant un composant eoseongcho Download PDF

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WO2020235941A1
WO2020235941A1 PCT/KR2020/006632 KR2020006632W WO2020235941A1 WO 2020235941 A1 WO2020235941 A1 WO 2020235941A1 KR 2020006632 W KR2020006632 W KR 2020006632W WO 2020235941 A1 WO2020235941 A1 WO 2020235941A1
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Prior art keywords
eoseongcho
weight
parts
extract
spray
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PCT/KR2020/006632
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English (en)
Korean (ko)
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양숙현
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농업회사법인 주식회사 용추
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Priority to JP2021566333A priority Critical patent/JP7315986B2/ja
Publication of WO2020235941A1 publication Critical patent/WO2020235941A1/fr

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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9789—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04—Dispersions; Emulsions
    • A61K8/046—Aerosols; Foams
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/42—Amides
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/82—Preparation or application process involves sonication or ultrasonication

Definitions

  • the present invention relates to a spray composition for improving scalp health comprising a component of Eoseongcho, and more specifically, Eoseongcho, which can not only fix hair to express various styles, but also contain natural extracts to have healthy scalp and hair. It relates to a spray composition for improving scalp health comprising an ingredient.
  • hair spray is a liquid spray product for stably setting in a state of temporarily changing the shape of the hair.It is widely used in modern times and contains setting polymers, solvents, plasticizers, moisturizers, and fragrances. It is used to provide sufficient moisturizing effect to the skin and to keep the shape of the trimmed hair for a long time.
  • silicone plasticizers for moisturizing ingredients are added together with a neutralizing agent, but adding a plasticizing ingredient has the effect of softening the hair, but lowering the setting power to maintain the shape of the hair.
  • a cationic surfactant can be used to keep the hair flexible while exhibiting a certain level of setting effect, but the surfactant was difficult to combine due to the problem of compatibility with liquefied petroleum gases such as propane and butane, and spray products with aerosols Since it was not possible to use, the proposal of a spray product with good flexibility and setting power was urgently required.
  • Patent Document 0001 Korean Patent Publication No. 10-2011-0041023 (published on April 21, 2011)
  • Patent Document 0002 Domestic registered patent No. 10-1792747 (registered on October 26, 2017)
  • Patent Document 0003 Korean Patent Publication No. 10-2013-0010746 (published on January 29, 2013)
  • the present invention provides a spray composition for improving scalp health including Eoseongcho ingredients including Eoseongcho ingredients capable of not only fixing hair to express various styles, but also containing natural extracts to have healthy scalp and hair. .
  • the spray composition for improving scalp health comprising the Eoseongcho component according to the present invention contains Eoseongcho extract as a main component.
  • Eoseongcho extract In addition to the Eoseongcho extract, ethanol, Panthenol, Sodium Dehydroacetate, Propylene Glycol, Sulfur (surfur), Zinc Gluconate, Magnesium Gluconate, Camellia Oil, dimethicone, methacryloyl ethyl betaine (Methacryloyl Ethyl Betaine) and flavoring may be included.
  • the composition is Eoseongcho extract 1 to 5 parts by weight, ethanol 60 to 80 parts by weight, Panthenol 05 to 15 parts by weight, Sodium Dehydroacetate 01 to 1 part by weight, Propylene Glycol 03 to 08 Parts by weight, sulfur (surfur) 01 to 05 parts by weight, zinc gluconate 001 to 003 parts by weight, magnesium gluconate 005 to 01 parts by weight, camellia oil 0005 to 003 parts by weight, dimethicone ( Dimethicone) 0025 to 0055 parts by weight, methacryloyl ethyl betaine (Methacryloyl Ethyl Betaine) 005 to 01 parts by weight, and fragrance 0005 to 001 parts by weight may be included in a weight ratio.
  • the Eoseongcho extract is washed after preparing Eoseongcho, and the washed Eoseongcho is pulverized into a certain particle size, and the crushed Eoseongcho is pulverized so that the particle diameter is in the range of 500 to 2500 ⁇ m, and the pulverized Eoseongcho is mixed with a solvent.
  • the mixture was added to an ultrasonic extractor to apply ultrasonic waves to the mixed solution to prepare an Eoseongcho extract mixture, the solvent being mixed in a weight ratio of 1000 to 2000 parts by weight based on 100 parts by weight of the pulverized Eoseongcho, and the solvent
  • any one or more solvents selected from water or alcohols having 1 to 4 carbon atoms are used, and the ultrasonic waves applied to the mixture under a temperature of 20 to 25°C and a pressure of 01 to 05kgf/cm2 are 30 to 50KHz at a vibration frequency of 30 to 50KHz. It is extracted using an output of 100 to 200 watts for 60 minutes, and may be prepared by aging for 1 to 3 hours at a temperature of 10 to 20°C after removing the solids from the Eoseongcho extract mixture.
  • a fermented wild wild ginseng extract may be further included, and the fermented wild wild ginseng extract may be included in a weight ratio of 10 to 30 parts by weight based on 100 parts by weight of the Eoseongcho extract.
  • the present invention provides a spray for improving scalp health comprising the above composition.
  • the scalp health improvement spray composition containing the Eoseongcho component according to the present invention not only fixes the hair to create a variety of styles, but also contains natural extracts to prepare a scalp health improvement spray that can have a healthy scalp and hair. can do.
  • 1A is a photograph showing a subject's scalp.
  • 1B is a photograph showing the scalp of the subject after spraying and shampooing the hair of the subject by spraying and shampooing the spray prepared according to Example 1 at 15 ml a day for 20 days.
  • providing scalp health refers to soothing the scalp and beautifying the hair to increase attractiveness and keep the hair healthy.
  • the spray composition for improving scalp health comprising the Eoseongcho component according to the present invention includes Eoseongcho extract, ethanol, Panthenol, Sodium Dehydroacetate, Propylene Glycol, sulfur (surfur), and zinc gluconate. (Zinc Gluconate), Magnesium Gluconate, Camellia Oil, Dimethicone, Methacryloyl Ethyl Betaine, and Perfume.
  • the spray composition for improving scalp health including the Eoseongcho component according to the present invention is Eoseongcho extract 1 to 5 parts by weight, ethanol 60 to 80 parts by weight, Panthenol 0.5 to 1.5 parts by weight, Sodium Dehydroacetate ) 0.1 to 1 parts by weight, propylene glycol (Propylene Glycol) 0.3 to 0.8 parts by weight, sulfur (surfur) 0.1 to 0.5 parts by weight, zinc gluconate (Zinc Gluconate) 0.01 to 0.03 parts by weight, magnesium gluconate (Magnesium Gluconate) 0.05 To 0.1 parts by weight, camellia oil 0.005 to 0.03 parts by weight, dimethicone 0.025 to 0.055 parts by weight, Methacryloyl Ethyl Betaine 0.05 to 0.1 parts by weight, and 0.005 to 0.01 parts by weight of fragrance It can be included as a percentage.
  • the Eoseongcho extract is prepared by extracting Eoseongcho, and Eoseongcho (Houttuynia cordata thunb) is an outpost of Yakmomil, a plant of the Saururaceae, and lives in Southeast Asia and particularly Japan and Korea.
  • Eoseongcho is also called Sip-Yak because it has ten medicinal effects, and the stem is like a sweet potato leaf, and it is also called Eoseongcho because it originates from the fact that when you touch the raw leaves, fish smells badly.
  • Eoseongcho is also available for medicinal and edible use. It is classified as animals and plants that can only be used in a minimum amount as an auxiliary ingredient in the classification of food raw materials in the food code. Pharmacologically, it is widely known for its strong heart, diuretic, antibacterial, detoxifying and anticancer efficacy Is used as a cosmetic and health functional food that helps detoxification and beauty.
  • Eoseongcho extract prepared by the following manufacturing method may be used as the extract of Eoseongcho.
  • the washed Eoseongcho may be pulverized into a certain particle size.
  • the active ingredient of the Eoseongcho may be sufficiently extracted by pulverizing the Eoseongcho to a certain particle size, and the crushing of the Eoseongcho may be pulverized so that the particle diameter is in the range of 500 to 2500 ⁇ m.
  • the particle diameter of the Eoseongcho is pulverized to less than 500 ⁇ m, it takes a long time to pulverize, and the particles are too small to cause agglomeration between particles in a later process. It may be difficult to effectively extract useful ingredients from Eoseongcho.
  • the pulverized Eoseongcho may be extracted by applying ultrasonic waves in an atmosphere of low temperature and reduced pressure to prepare a mixed solution for extracting Eoseongcho.
  • the solvent is 100 parts by weight of the pulverized Eoseongcho It is mixed at a weight ratio of 1000 to 2000 parts by weight, and any one or more solvents selected from water or an alcohol having 1 to 4 carbon atoms (C1 to C4) may be used as the solvent.
  • the ultrasonic wave applied to the mixed solution under a temperature of 20 to 25°C and a pressure of 0.1 to 0.5kgf/cm 2 outputs 100 to 200 watts for 30 to 60 minutes at a vibration frequency of 30 to 50 KHz. It can be extracted using
  • the Eoseongcho extract can be prepared by removing solids such as pulverized Eoseongcho from the Eoseongcho extract mixture and then aging for 1 to 3 hours at a temperature of 10 to 20°C.
  • the removal of solids such as crushed Eoseongcho from the Eoseongcho extract mixture may be performed by separating and removing the solids using a known sieve such as a sieve.
  • the ethanol acts as a solvent, and as the solvent evaporates, a film is formed on the surface of the hair, and the hair can be fixed by the strength of the film.
  • the panthenol is used as a conditioning agent and may improve the appearance and feel of the hair, increase flexibility, improve style, impart moisture and gloss, and improve the texture of the hair.
  • the sodium dehydroacetate is used as a bactericidal preservative and may serve to improve the storage stability of a spray composition for improving scalp health including the Eoseongcho component.
  • the chemical formula of the propylene glycol is C 3 H 8 O 2 , the specific gravity is 1.036 ⁇ 1.040, the boiling point is 185 ⁇ 189 °C.
  • the propylene glycol is well mixed with water, alcohol, acetone, ethyl acetate, chloroform, ether, and the like, has excellent solubility, and has good hygroscopicity, and can be used as a moisture evaporation barrier.
  • the propylene glycol can give a moisturizing effect to fixed hair, softly set the hair, and give a conditioning effect.
  • the sulfur occupies the eighth largest proportion of biological elements, and is particularly distributed in bones, skin, and hair.
  • the sulfur occupies the eighth largest proportion of biological elements, and is particularly distributed in bones, skin, and hair.
  • sulfur has an excellent detoxification effect against heavy metals and chemicals
  • bones become strong and bone marrow becomes full (Donguibogam)
  • Donguibogam helps yang, warms the body, and It is said that it strengthens bones (new herbal medicine), strengthens bones, strengthens muscles, and prevents hair loss.
  • this sulfur penetrates into the pores to form cystine proteins, and it is known to prevent hair loss by forming a sulfur chain together with it, and has been added as a component to various hair loss prevention products.
  • Sulfur used in the present invention refers to sulfur from which toxic components have been removed, and the sulfur can perform functions such as pain relief, inflammation removal, transport of active substances, cell regeneration, blood circulation promotion, detoxification and sterilization, etc.
  • a commercially known sulfur may be used as the sulfur, and sulfur having a particle diameter of 10 to 80 nm may be used to further improve the physiological activity and penetration into the body.
  • the zinc gluconate is used as a skin conditioning agent and is effective for inflammatory acne due to its antiviral properties.
  • the zinc gluconate is effective in soothing the irritated scalp and relieving skin itching.
  • the magnesium gluconate is a magnesium salt component of gluconic acid, the chemical formula is C 12 H 22 MgO 14 or C 12 H 22 MgO 14 2H 2 O, the molecular weight is 414.61, and the scalp state is It helps to keep it in a healthy and good condition.
  • the camellia oil is an oil containing a large amount of unsaturated fatty acids, and the oil rarely evaporates even if left unattended, and its specific gravity is about 0.916, which is similar to water.
  • the main fatty acid component is oleic acid, which accounts for about 90%. It is a yellow, clear oil with a low freezing point of 25°C, and is mainly used as a substitute for hair oil, precision machine oil, and olive oil in medicine.
  • the camellia oil prepared by the following method may be used as the camellia oil.
  • the washed camellia seeds may be immersed in grape juice and rancidity inhibitors.
  • the camellia oil produced by immersing the camellia seeds in grape juice and rancidity inhibitor can prevent discoloration or rancidity.
  • the washed camellia seeds can be immersed in a mixture of grape juice and rancidity inhibitor in a ratio of 1:1, and the rancidity inhibitor is mixed with vitamin C and salt solution in a weight ratio of 1:1. Can be manufactured.
  • the grape juice is good for preventing blood clots and preventing adult diseases such as high blood pressure, arteriosclerosis and heart disease, and can help improve memory
  • the salt solution used as the rancidity inhibitor may be a salt solution having a concentration of 1 to 2% by weight
  • the washed camellia seeds may be immersed in a weight ratio of 100 to 120 parts by weight of a mixture of grape juice and rancidity inhibitor with respect to 100 parts by weight of the washed camellia seeds, and then maintained for 10 to 40 minutes.
  • camellia seeds immersed in the mixed solution of the grape juice and rancidity inhibitor may be taken out so that the grape juice and components of the rancidity inhibitor may penetrate into the camellia seeds.
  • a mixture of grape juice and rancidity inhibitor The camellia seeds separated from may be stored at a temperature of 35 to 40° C. for 30 to 60 minutes.
  • camellia seeds into which the components of the grape juice and rancidity inhibitors have penetrated can be steamed.
  • the steaming of the camellia seeds can be performed by steaming the camellia seeds into which the grape juice and rancidity inhibitor components are infiltrated with steam for 30 to 60 minutes. If the steaming of the camellia seeds is performed below the above lower limit, sufficient There is a problem in that steaming is not performed, and when the steaming is performed beyond the upper limit range, the difference in effect according to the increase of the steaming time may be insignificant.
  • the steamed camellia seeds can be dried.
  • Drying of the steamed camellia seeds can be carried out for 10 to 20 hours at a temperature of 30 to 40°C on the steamed camellia seeds, and mechanical drying using a dryer is used to keep the drying temperature of the camellia seeds constant. Can be.
  • the dried camellia seeds may be washed with at least one acid of acetic acid or citric acid.
  • the washing of the dried camellia seeds is effective in improving the flavor and color of camellia oil to be produced through a later fermentation process by washing the surface of the dried camellia seeds with one or more acids of acetic acid or citric acid.
  • the washed camellia seed may be sprayed with a fermentation broth consisting of a culture broth and lactic acid bacteria.
  • lactic acid bacteria any one known lactic acid bacteria selected from the group consisting of lactic acid bacteria ( Lactobacillales ), Streptococcus thermophiles , and Bifidobacterium longum may be used, and the culture medium is peptone , Malt extract, sodium citrate, potassium phosphate dibasic, glucose, and distilled water, and the culture solution is 15 to 25 parts by weight of peptone, malt extract 5 to 15 It may be made by mixing in a weight ratio of 0.5 to 1.5 parts by weight of sodium citrate, 0.1 to 0.3 parts by weight of dibasic potassium phosphate, 1 to 3 parts by weight of glucose, and 100 to 200 parts by weight of distilled water.
  • the peptone is a nitrogen source that supplies protein and supplies proteins necessary for the growth of microorganisms
  • the malt extract contains various minerals, vitamin B groups, and amino acids, so that it can help the growth of microorganisms
  • the sodium citrate Silver is an inorganic substance that maintains a state optimized for the growth of microorganisms by adjusting the pH of the culture medium, and can supply nutrients, and the glucose can function as an important component by which lactic acid bacteria metabolize sugar to produce organic acids.
  • camellia seeds sprayed with the fermentation broth may be fermented.
  • Fermentation of the camellia seeds may be fermented by storing the camellia seeds sprayed with the fermentation broth in a storage container maintaining a temperature of 45 to 50° C. and a humidity of 60 to 65% for 3 to 6 days.
  • the fermented camellia seeds may be dried in cold air.
  • Cold air drying of the fermented camellia seeds may be performed by drying the fermented camellia seeds with cold air at a temperature of 3 to 6° C. for 5 to 10 hours and maintaining the fermented camellia seeds at a temperature of 55 to 60° C. for 1 to 3 days.
  • camellia seed oil (camellia seed oil).
  • the dimethicone is used as an emulsifier, and it can improve the mixing properties of the spray composition for improving scalp health including the Eoseongcho component according to the present invention so as to exhibit homogeneous physical properties.
  • the methacryloyl ethyl betaine (Methacryloyl Ethyl Betaine) may be so as to be well dissolved in an ethanol solvent ( ⁇ ), a transparent aromatic alcohol.
  • the fragrance provides the fragrance of the spray composition, and various kinds of known fragrances can be used.
  • natural fragrances extracted from plants can be used to consider the health of the hair or scalp. have.
  • the spray composition for improving scalp health comprising the Eoseongcho component according to the present invention may further include a fermented wild ginseng extract in addition to the composition, wherein the fermented wild wild ginseng extract is 10 to 30 parts by weight based on 100 parts by weight of the Eoseongcho extract. It can be included as a percentage.
  • the fermented wild wild ginseng extract can be prepared using wild wild ginseng roots and wild wild ginseng leaves.
  • the wild wild ginseng contains 10 times more saponin than ginseng and 4 to 5 times more than red ginseng, which has great efficacy in enhancing immunity. , Diabetes prevention, digestion, stress relief, energy enhancement, etc. are effective.
  • the wild wild ginseng fermented extract may be used wild wild ginseng fermented extract prepared by the following manufacturing method.
  • the wild mountain ginseng root and the fresh mountain mountain leaves can be separated and prepared, and then washed.
  • the wild ginseng root can be heated with steam to increase steam and then fumigate with sulfur.
  • the wild ginseng roots are heated with steam for 30 to 100 minutes at a temperature of 130 to 140°C and a pressure of 1 to 3kgf/cm 2 , and then sulfur fumigation is performed on the wild ginseng roots heated with steam for 1 to 3 minutes. I can.
  • the sulfur fumigated wild ginseng roots may be dried for 1 to 3 days at a temperature of 25 to 30°C.
  • the dried wild ginseng root may be cut in units of a predetermined length, for example, the dried wild ginseng root may be cut in a length unit of 0.1 to 1.0 cm.
  • the aging can be aged by maintaining the wild ginseng root mixed with the lactic acid bacteria for 10 to 30 hours at a temperature of 20 to 25 °C.
  • lactic acid bacteria any one known lactic acid bacteria selected from the group consisting of lactic acid bacteria ( Lactobacillales ), Streptococcus thermophiles , and Bifidobacterium longum may be used.
  • the washed wild wild ginseng leaves may be heated with steam.
  • step it may be carried out by heating the wild wild ginseng leaves at 110 to 120°C and a pressure of 1 to 3kgf/cm 2 with steam for 10 to 30 minutes.
  • the fresh wild wild ginseng leaves heated with the steam may be dried.
  • the wild wild wild ginseng leaves may be dried for 5 to 10 hours at a temperature of 25 to 30°C.
  • the dried wild wild ginseng leaves can be heated to roast.
  • the dried wild wild ginseng leaves are put into a heating container (for example, a cauldron) and then first roasted at a temperature of 90 to 95°C for 3 to 5 minutes, and the first roasted wild wild wild ginseng leaves are 130 to 140 At a temperature of °C 30 to 60 seconds may proceed to the step of the second abrasion.
  • a heating container for example, a cauldron
  • the washed wild wild ginseng leaves may be fermented by spraying the Bacteria leachate into the washed wild wild ginseng leaves.
  • the Bacillus leachate is capable of accelerating the fermentation of the dried wild wild ginseng leaves, sprayed at a weight ratio of 30 to 50 parts by weight of the dried wild wild ginseng leaves, and a temperature of 55 to 60°C and 60 to 65 After allowing the% humidity to be maintained, it can be fermented for 2 to 4 days.
  • the Bacillus Bacillus culture medium is produced by mixing Bacillus bacillus and water, and the Bacillus bacillus is grown twice a day at 25°C after mixing 10 to 12% by weight of brown sugar in godubap, placing eco-friendly rice husks on the prepared medium and covering a cloth. It can be cultured for one week while spraying water on the plant to generate Bacillus bacteria, which are re-inoculated in a medium mixed with rice bran and brown sugar at a weight ratio of 50:50, and cultured at 25°C for one week to be used as the Bacillus bacteria leachate used in the present invention. have.
  • Bacillus subtilis Bacillus subtilis
  • Bacillus subtilis spjijepiyi Bacillus subtilis
  • Bacillus megaterium Bacillus megaterium
  • Bacillus licheniformis Bacillus licheniformis
  • Bacillus fulmis Any one or more selected from the group consisting of ( Bacillus pumilus ) may be used.
  • the fermented wild wild ginseng root and the fermented wild wild ginseng leaves are mixed and fermented to prepare a fermented wild wild ginseng mixture.
  • the fermented wild wild ginseng leaves are mixed at a weight ratio of 200 to 400 parts by weight with respect to 100 parts by weight of the aged wild ginseng roots, and then fermented for 3 to 5 days at a temperature of 60 to 65°C and a humidity of 55 to 60%.
  • a fermented wild ginseng mixture is prepared.
  • the fermented wild wild ginseng fermentation broth may be prepared by mixing a solvent with the fermented wild wild ginseng mixture and applying ultrasonic waves.
  • the fermented wild ginseng mixture may be mixed with a solvent to prepare a mixture, and then added to an ultrasonic extractor to apply ultrasonic waves to the mixture to prepare a wild wild ginseng fermentation broth. It is included in a weight ratio of 300 to 500 parts by weight based on parts, and water may be used as the solvent.
  • the ultrasonic wave applied to the mixed solution to prepare the fermented wild ginseng may be extracted using an output of 100 to 200 watts for 50 to 100 minutes at a vibration frequency of 60 to 80 KHz.
  • solids such as wild wild ginseng roots and fresh wild wild ginseng leaves can be removed from the fermented wild ginseng broth.
  • Separation of solids such as wild wild ginseng roots and fresh wild wild ginseng leaves in the above step may be performed using a known strainer such as a sieve.
  • the fermented wild ginseng broth from which the solid content has been removed may be centrifuged.
  • the fermented wild ginseng broth from which solids have been removed by centrifuging the fermented wild ginseng broth from which solids have been removed, it can be separated into a lower layer in which fine particles of wild ginseng roots and fresh leaves are located, and a middle layer and a supernatant located above the lower layer. .
  • the useful ingredient of sanyangsam may prepare a fermented sanyangsam extract.
  • the fermented wild wild ginseng extract is first extracted with 10 to 15 l of a 70% (v/v) ethanol aqueous solution in 2000 to 3000 g of wild wild ginseng fermentation broth at 85 to 90°C for 3 to 4 hours, and then 70% (v/v) ethanol Completing the secondary extraction for 2 to 3 hours at 85 to 90 °C with 4 to 6 l of aqueous solution, and preparing an extract until it becomes 1000 to 1500 ml in a vacuum rotary evaporator; And ethanol is added to the extract, diluted to 2 to 3 times by weight, centrifuged at 18,000 to 20,000 rpm for 30 to 40 minutes to completely remove polymer fibers and solids that may be included in the fermented wild ginseng, and then the collected supernatant is 1.5 to It can be prepared by extracting twice with 2.0 times the weight of acetic acid.
  • the spray composition for improving scalp health comprising the Eoseongcho component according to the present invention may further include an onion extract in addition to the composition, wherein the onion extract is in a weight ratio of 5 to 15 parts by weight based on 100 parts by weight of the Eoseongcho extract. Can be included.
  • the onion extract is prepared by extracting the useful ingredients of onion, and the onion (Allium cepa) is a perennial plant belonging to the lily family, and is used as food, spices and medicinal materials to which a unique taste and aroma are applied along with a long cultivation history.
  • 100g of onion contains 90g of moisture, about 72g of carbohydrates, 11g of protein, 10 to 20mg of vitamin C, calcium, phosphorus, and iron.
  • the onion skin contains 504% sugar, 2924% fiber, 148% fat, and 499% ash. Contains.
  • onions The efficacy of onions is known for antioxidant, lowering blood lipids, antihypertension, anti-inflammatory, antibacterial, anti-tumor, and lowering blood sugar.
  • the main physiologically active substances contained in onions include organic sulfur compounds and flavonoid compounds.
  • onions contain very high quercetin, which exhibits antioxidant activity, compared to other vegetables and fruits.
  • Quercetin is a plant-derived flavonoid-based phenolic compound that is not only a powerful antioxidant, but also has anti-arteriosclerosis, antibacterial activity, cholesterol lowering, anti-cancer, anti-viral and anti-allergic activities, but little toxicity. It is known. Therefore, eating foods containing a lot of quercetin is effective in improving blood circulation, lowering blood pressure and dieting such as diabetes and weight loss, strengthening immune function, inhibiting DNA damage, and inhibiting lipid peroxidation of red blood cell membranes.
  • the onion extract can be prepared by the following manufacturing method.
  • the onion is collected and 1 to 5 minutes with purified water in which sodium hydrogen carbonate (NaHCO 3 ) having a concentration range of 1 to 3 (w/w)% and a temperature of 33 to 37°C is dissolved During washing to remove foreign substances adhering to the onion, the peel of the onion can be separated and separated into onion flesh and onion peel.
  • NaHCO 3 sodium hydrogen carbonate
  • the onion pulp is dried in a dryer, but drying of the onion pulp is performed in a dryer in which a constant temperature and humidity are maintained in order to prevent the chlorophyll of the onion pulp from being destroyed and the inherent flavor of the onion pulp from disappearing when drying in sunlight.
  • the onion flesh may be dried for 3 to 7 hours in a dryer maintained at a temperature of 20 to 25° C. and a humidity of 33 to 40%.
  • the dried onion pulp is mixed with purified water and heated to prepare the onion pulp extract.
  • the onion pulp extract may be prepared by mixing 500 to 1000 parts by weight of purified water with respect to 100 parts by weight of the dried onion pulp and heating at a temperature of 95 to 105°C for 5 to 15 hours.
  • the onion peel can be dried to remove moisture contained in the onion peel, and the onion peel can be dried for 3 to 7 hours in a dryer maintained at 30 to 35°C and 35 to 45% humidity.
  • the moisture contained in the onion skin is gradually and evenly evaporated, so that the inherent aroma and useful ingredients of the onion skin can be more easily extracted.
  • By destroying the cell tissue of the onion skin it facilitates the penetration of air and promotes the fermentation, so that the useful components of the onion skin can be enriched.
  • the dried onion peel is mixed with purified water and then heated to prepare the onion peel extract.
  • the onion peel extract is mixed with 200 to 400 parts by weight of purified water based on 100 parts by weight of the dried onion peel. After immersing for 1 to 3 hours at a temperature of 60 to 70°C, the purified water immersed in the onion skin is added to a heater, and purified water in which the onion skin is immersed in the heater is added to a temperature of 110 to 120°C and inside a pressure vessel
  • the onion peel extract can be prepared by heating for 3 to 5 hours in a pressure range of 2.5 to 3.5kgf/cm 2 .
  • the onion peel is immersed in purified water and then extracted as described above, thereby weakening the plant wall of the onion peel to increase extraction efficiency.
  • an onion extract can be prepared by mixing the onion flesh extract and the onion peel extract, wherein the onion extract is prepared by mixing the onion flesh extract and the onion peel extract in a weight ratio of 7:3 to 6:4. I can.
  • the onion extract may be aged by storing it for 1 to 5 hours at a temperature of 3 to 7°C.
  • the onion extract may be uniformly mixed and the flavor may be enhanced.
  • a spray was prepared using a spray composition included in a weight ratio of 0.008 parts by weight and a fragrance.
  • a spray was prepared using the same composition as in Example 1, but in Example 2, a spray was prepared by further including 20 parts by weight of the fermented wild ginseng extract with respect to 100 parts by weight of the Eoseongcho extract.
  • Soap was prepared using the same composition as in Example 1, and in Example 3, a spray was prepared by further including 10 parts by weight of onion extract with respect to 100 parts by weight of the Eoseongcho extract.
  • a spray was prepared using the same composition as in Example 1, but in Comparative Example 1, Eoseongcho extract and camellia oil were not included.
  • a commercially available spray (manufactured by W company, using a chemical substance) was prepared, and it was used as a spray according to Comparative Example 2.
  • the experiment was conducted on 20 healthy subjects (7 males and 13 females) between the ages of 10 and 50, and the spray was used 15 ml per day for 20 days, and the result was measured by a 5-point scale method. I did.
  • the spray according to Examples 1 to 3 included natural extracts such as Eoseongcho extract, fermented wild ginseng extract, and onion extract, thereby contributing to the improvement of the user's scalp and hair.
  • the stimulation test for the spray prepared as described above was conducted as follows.
  • the stimulation experiment targeted 20 healthy people (7 men, 13 women) between 10 and 50 years old.After the hair shampoo, spray was sprayed onto the hair of the subject, and after 3 hours the scalp condition (erythema, Edema, papules, etc.) were observed, and a qualitative evaluation was performed through an evaluation table as shown in [Table 2] below.
  • the easy cleaning experiment was targeting 20 healthy people (7 men, 13 women) between the ages of 10 and 50 years, and the hair was set by spraying 10 ml of spray onto the hair, and washing with shampoo And washing without using shampoo, and the results are shown in Table 4 below.
  • ⁇ The hair gel component has been removed to some extent, and after washing, a refreshing feeling is generated.
  • ⁇ The hair gel component has been removed to some extent, but after washing, there is no refreshing feeling.
  • the hair gel component is hardly removed, and an unpleasant feeling occurs after washing.
  • the spray prepared according to Example 1 was sprayed onto the hair of the subject (35 years old female) to observe the condition of the subject's scalp.
  • FIG. 1A is a photograph showing the scalp of a subject
  • FIG. 1B is a spray prepared according to Example 1 and spraying and shampooing on the subject's hair at 15 ml per day for 20 days, and after 20 days, the scalp of the subject This is a picture showing.

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Abstract

La présente invention concerne une composition de pulvérisation qui est destinée à améliorer la santé du cuir chevelu et comprend un composant Eoseongcho. Une composition de pulvérisation, qui est destinée à améliorer la santé du cuir chevelu et comprend un composant Eoseongcho selon la présente invention, comprend : un extrait d'Eoseongcho ; de l'éthanol ; du panthénol ; du déhydroacétate de sodium ; du propylène glycol ; du soufre ; du gluconate de zinc ; du gluconate de magnésium ; de l'huile de camellia ; de la diméthicone ; de la méthacryloyl éthyl bétaïne ; et un parfum. Du fait de la configuration susmentionnée, la présente invention peut produire une pulvérisation pour améliorer la santé du cuir chevelu, la pulvérisation permettant d'arborer une variété de coiffures par fixation des cheveux, et permettant également d'obtenir un cuir chevelu et des cheveux sains grâce à la présence d'un extrait naturel.
PCT/KR2020/006632 2019-05-22 2020-05-21 Composition de pulvérisation pour améliorer la santé du cuir chevelu contenant un composant eoseongcho WO2020235941A1 (fr)

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KR102174199B1 (ko) * 2020-01-29 2020-11-04 양숙현 산양삼 성분이 포함된 어성초 발효 오일의 제조방법 및 이에 의해 제조된 어성초 발효 오일
KR102287369B1 (ko) * 2021-04-12 2021-08-06 (주)배리어스랩 탈모방지용 조성물

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